CN103741002A - Preparation method of superhard composite material - Google Patents

Preparation method of superhard composite material Download PDF

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Publication number
CN103741002A
CN103741002A CN201310264043.6A CN201310264043A CN103741002A CN 103741002 A CN103741002 A CN 103741002A CN 201310264043 A CN201310264043 A CN 201310264043A CN 103741002 A CN103741002 A CN 103741002A
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China
Prior art keywords
metal adhesive
boron nitride
cubic boron
nitride powder
powder
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CN201310264043.6A
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Chinese (zh)
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CN103741002B (en
Inventor
王琰弟
李英爱
张铁臣
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CHANGCHUN AERMASI SCIENCE & TECHNOLOGY Co Ltd
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CHANGCHUN AERMASI SCIENCE & TECHNOLOGY Co Ltd
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Priority to CN201310264043.6A priority Critical patent/CN103741002B/en
Publication of CN103741002A publication Critical patent/CN103741002A/en
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Abstract

The invention provides a preparation method of superhard composite material, and belongs to the field of material manufacture technology, and the method comprises the following steps: selecting a TiCu alloy whose Ti content is 30-75% from Fe, Ni, Co system, mixing the grinded TiCu alloy and Al powder, pressing into a plate shaped metal binder; placing a plate shaped metal binder into the bottom of a cylindrical heating block which is prepared from graphite material, injecting cubic boron nitride powder into the cylindrical heating block, placing the heating block into a high temperature high pressure apparatus, gradually pressurizing to 30 kPa, simultaneously heating, after naturally cooling, forming a cutlery material from the metal binder and the cubic boron nitride powder. When the cutter cuts a steel member whose quenching hardness is 40 HRC with linear velocity 90 meter/min, the usage life of the cutter produced by the method reaches to 90 minutes, and the yield reaches to 85-90%.

Description

A kind of preparation method of super-hard compound material
Technical field
The invention belongs to material manufacturing technology field, is a kind of method of preparing cutlery material.
Background technology
Existing cutlery material preparation method is mainly that cutlery is in use easy to wear by several metallic substance Hybrid Heating, and the life-span is short.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of preparation method of super-hard compound material.
The scheme of technical solution problem of the present invention is to complete by following steps:
1, prepare metal adhesive
From Fe, Ni, Co system, choose the TiCu alloy that Ti content is 30-75%, after TiCu alloy is pulverized, mix with Al powder, be pressed into plates metal adhesive, wherein TiCu alloy accounts for the 95-80% of total mass, and the content of Al powder accounts for 5-20%;
2, early-stage preparations
Plates metal adhesive is put into the tubular heat block bottom that graphite material is made, in tubular heat block, inject cubic boron nitride powder, the quality of cubic boron nitride powder is 3-5 times of metal adhesive quality;
3, preparation
The heat block that metal adhesive and cubic boron nitride powder are housed is put into high temperature high pressure device, progressively pressurizeing and making pressure is 30 kPas, heat up simultaneously, guarantee that metal adhesive can melt completely, after naturally cooling, the alloy of metal adhesive and cubic boron nitride powder forms cutlery material.
The cutter that the present invention produces is when cutting the steel part that quenching hardness is 40HRC, and in the situation that linear velocity is 90 ms/min, the life-span can reach 90 minutes, yield rate 85%-90%.
Embodiment
1, choose Ti content and be respectively 50% TiCuNi alloy, after TiCuNi alloy is pulverized, mix with Al powder, be pressed into plates metal adhesive, wherein TiCuNi alloy accounts for 95% of total mass, and the content of Al powder accounts for 5%; Plates metal adhesive is put into the tubular heat block bottom that graphite material is made, in tubular heat block, inject cubic boron nitride powder, the quality of cubic boron nitride powder is 5 times of metal adhesive quality; The heat block that metal adhesive and cubic boron nitride powder are housed is put into high temperature high pressure device, progressively pressurizeing and making pressure is 30 kPas, heat up simultaneously, guarantee that metal adhesive can melt completely, after naturally cooling, the alloy of metal adhesive and cubic boron nitride powder forms cutlery material.
2, choose Ti content and be respectively 30% TiCuFe alloy, after TiCuFe alloy is pulverized, mix with Al powder, be pressed into plates metal adhesive, wherein TiCuFe alloy accounts for 80% of total mass, and the content of Al powder accounts for 20%; Plates metal adhesive is put into the tubular heat block bottom that graphite material is made, in tubular heat block, inject cubic boron nitride powder, the quality of cubic boron nitride powder is 3 times of metal adhesive quality; The heat block that metal adhesive and cubic boron nitride powder are housed is put into high temperature high pressure device, progressively pressurizeing and making pressure is 30 kPas, heat up simultaneously, guarantee that metal adhesive can melt completely, after naturally cooling, the alloy of metal adhesive and cubic boron nitride powder forms cutlery material.
3, choose Ti content and be respectively 50% TiCu Chrome metal powder, after TiCu Chrome metal powder is pulverized, mix with Al powder, be pressed into plates metal adhesive, wherein TiCu Chrome metal powder accounts for 88% of total mass, and the content of Al powder accounts for 12%; Plates metal adhesive is put into the tubular heat block bottom that graphite material is made, in tubular heat block, inject cubic boron nitride powder, the quality of cubic boron nitride powder is 4 times of metal adhesive quality; The heat block that metal adhesive and cubic boron nitride powder are housed is put into high temperature high pressure device, progressively pressurizeing and making pressure is 30 kPas, heat up simultaneously, guarantee that metal adhesive can melt completely, after naturally cooling, the alloy of metal adhesive and cubic boron nitride powder forms cutlery material.

Claims (1)

1. a preparation method for super-hard compound material, is characterized in that being completed by following steps:
(1) prepare metal adhesive
From Fe, Ni, Co system, choose the TiCu alloy that Ti content is 30-75%, after TiCu alloy is pulverized, mix with Al powder, be pressed into plates metal adhesive, wherein TiCu alloy accounts for the 95-80% of total mass, and the content of Al powder accounts for 5-20%;
(2) early-stage preparations
Plates metal adhesive is put into the tubular heat block bottom that graphite material is made, in tubular heat block, inject cubic boron nitride powder, the quality of cubic boron nitride powder is 3-5 times of metal adhesive quality;
(3) preparation
The heat block that metal adhesive and cubic boron nitride powder are housed is put into high temperature high pressure device, progressively pressurizeing and making pressure is 30 kPas, heat up simultaneously, guarantee that metal adhesive can melt completely, after naturally cooling, the alloy of metal adhesive and cubic boron nitride powder forms cutlery material.
CN201310264043.6A 2013-06-28 2013-06-28 A kind of preparation method of super-hard compound material Active CN103741002B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201310264043.6A CN103741002B (en) 2013-06-28 2013-06-28 A kind of preparation method of super-hard compound material

Publications (2)

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CN103741002A true CN103741002A (en) 2014-04-23
CN103741002B CN103741002B (en) 2016-07-06

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106566973A (en) * 2016-10-14 2017-04-19 洛阳鼎威材料科技有限公司 Preparation method for cutting tool composite
CN114672683A (en) * 2022-03-30 2022-06-28 陕西理工大学 Self-lubricating alloy cutter material and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1059138A (en) * 1991-08-30 1992-03-04 机械电子工业部郑州磨料磨具磨削研究所 Agglomerate of composite superhard material and manufacture method thereof
CN101031525A (en) * 2004-10-28 2007-09-05 京瓷株式会社 Cubic boron nitride sintered material and cutting tool using the same
CN101168229A (en) * 2006-10-27 2008-04-30 河南富耐克超硬材料有限公司 Method for manufacturing ultra-hard composite blade
CN101627139A (en) * 2006-12-11 2010-01-13 六号元素(产品)(控股)公司 Cubic boron nitride compact
EP2420483A1 (en) * 2009-04-17 2012-02-22 Tungaloy Corporation Cubic boron nitride sintered compact and coated cubic boron nitride sintered compact

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1059138A (en) * 1991-08-30 1992-03-04 机械电子工业部郑州磨料磨具磨削研究所 Agglomerate of composite superhard material and manufacture method thereof
CN101031525A (en) * 2004-10-28 2007-09-05 京瓷株式会社 Cubic boron nitride sintered material and cutting tool using the same
CN101168229A (en) * 2006-10-27 2008-04-30 河南富耐克超硬材料有限公司 Method for manufacturing ultra-hard composite blade
CN101627139A (en) * 2006-12-11 2010-01-13 六号元素(产品)(控股)公司 Cubic boron nitride compact
EP2420483A1 (en) * 2009-04-17 2012-02-22 Tungaloy Corporation Cubic boron nitride sintered compact and coated cubic boron nitride sintered compact

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106566973A (en) * 2016-10-14 2017-04-19 洛阳鼎威材料科技有限公司 Preparation method for cutting tool composite
CN114672683A (en) * 2022-03-30 2022-06-28 陕西理工大学 Self-lubricating alloy cutter material and preparation method thereof

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