CN103666237A - Aqueous UV top-varnish product for kitchen cabinet - Google Patents
Aqueous UV top-varnish product for kitchen cabinet Download PDFInfo
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- CN103666237A CN103666237A CN201310652490.9A CN201310652490A CN103666237A CN 103666237 A CN103666237 A CN 103666237A CN 201310652490 A CN201310652490 A CN 201310652490A CN 103666237 A CN103666237 A CN 103666237A
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Abstract
The present invention relates to a high chemical resistance aqueous ultraviolet light-curable (UV) top-varnish, which is characterized by comprising, by weight, 60-70 parts of an aqueous dispersion, 4-6 parts of a matting agent, 3-6 parts of a film forming auxiliary agent, 1-2 parts of a leveling agent, 1-2 parts of an antifoaming agent, 1-2 parts of a thickening agent, 4-6 parts of a photoinitiator, and 26-6 parts of water. The high chemical resistance aqueous ultraviolet light-curable (UV) top-varnish has good chemical resistance based on requirements of kitchen cabinet plates, can provide resistance for coffee stains, tomato sauce, olive oil and other commonly used basic kitchen articles, has characteristics of good adhesion and adjustable and appropriate shear viscosity, and is suitable for plant spray coating products. In addition, the high chemical resistance aqueous ultraviolet light-curable (UV) top-varnish is in the domestic leading level.
Description
Technical field
The present invention relates to a kind of UV-curable waterborne (UV) coating, particularly a kind of UV-curable waterborne clear finish that is applicable to the high resistance to chemicals moral character of cabinet product.
Background technology
UV cure wood coatings is a kind of environmental protection and energy saving coating of succeeding in developing over nearly 20 years.UV cure wood coatings has advantages of that many traditional woodwork coatings are incomparable: save the energy, capacity usage ratio is high; Solvent-free discharge, safety non-pollution; Curing speed is fast, and production efficiency is high; Can application to heat sensitive base material; Film quality is high, coating performance is excellent.And UV-curable waterborne coatings is the international product of the future that just started in recent years exploitation, aspect environment protection, curing efficiency, there iing impayable advantage, under the promotion of national policy, will become the main force of coating industry.
Cabinet product also needs to be able to take the dipping tests such as coffee stain, tomato-sauce, sweet oil, vinegar, ethanol, water except requiring the requirement of the furniture items such as common application property, paint film planarization, sticking power, hardness.
Summary of the invention
The object of the invention is, for adapting to the requirement of client to cabinet application high-performance, environmental protection, efficient, high resistance to chemicals product performance, provides a kind of UV-curable waterborne clear finish product of high resistance to chemicals moral character.The present invention designs a kind of water-based UV clear finish product that is applicable to cabinet, it is characterized in that: by following constituent and weight part, formed,
60 ~ 70 parts of aqueous dispersion,
4 ~ 6 parts of matting agents,
3 ~ 6 parts of film coalescence aid,
1 ~ 2 part of flow agent,
1 ~ 2 part of defoamer,
1 ~ 2 part of thickening material,
4 ~ 6 parts of light triggers,
26 ~ 6 parts, water,
Described aqueous dispersion is a kind of or its mixture of water-based aliphatics UV curing acrylic polyurethane dispersions and water soluble acrylic acid polyurethane dispersions.Matting agent adopts silicon-dioxide or organic wax.Film coalescence aid is dipropylene glycol methyl ether (DPM), dipropylene glycol butyl ether (DPNB).Flow agent is polyether-modified polydimethylsiloxane interpolymer.Defoamer is polyether silicone co-polymer emulsion, containing aerosil.Thickening material is associative thickener.Light trigger is the mixture of TMDPO and benzophenone.Being dried need be through two step, and pre-volatile dry and UV curing cross-linked film forming are dry.
It is the photocuring PUA water dispersion of UVLS2282 that described aqueous dispersion can adopt Beyer Co., Ltd's trade mark, and the water dispersion of the acroleic acid polyurethane that the trade mark that also can add DSM N. V. is E-129, improves product performance.
Described matting agent can adopt the silicon-dioxide of the trade mark SY7000 of GRACE company or organic wax of goldschmidt chemical corporation trade mark OK500.
Dipropylene glycol methyl ether (DPM), dipropylene glycol butyl ether (DPNB) that described film coalescence aid can adopt DOW company to produce.
Described flow agent can adopt the polyether-modified polydimethylsiloxane interpolymer of the trade mark BYK333 of BYK company.
Described defoamer can adopt one or more in the trade mark BYK022 of BYK company, BYK093, the trade mark TEGO810 of TEGO company, TEGO901W, TEGO902W.
Described thickening material can adopt the RM-12W of Rhom and Hass and one or both in RM-2050D.
Described light trigger can adopt the benzophenone that TMDPO that the trade mark of Hubei Gu Run is TPO and Changzhou Hua Tai company trade mark are BP to mix.
Advantage of the present invention is to have good chemical resistance, the collocation of preferred aliphat UV curing acrylic polyurethane dispersions and water soluble acrylic acid polyaminoester emulsion, is doing balance aspect chemical resistance and the basic film forming of paint film, snappiness, hardness, sticking power.The first physical constraints of dry employing is dry, then uses uv cure machine to impel free radical to cause the drying principles of rear crosslinked film forming.Reaction principle as shown in Figure 1.
The present invention sets about from formula, from formula source, be conceived to the requirement of client to smell, VOC, and factory's construction requirement high-level efficiency, high performance requirement, adopt UV sodified water dispersion, add the seldom film coalescence aid of amount, VOC is controlled at extremely low-level, and has improved greatly the shortcoming that aqueous product hardness, fullness ratio, mechanical property etc. exist always.
Accompanying drawing explanation
The drying principles figure of crosslinked film forming after accompanying drawing 1 use uv cure machine of the present invention impels free radical to cause.
Below in conjunction with example, the present invention is elaborated:
When prepared by product, should note:
Film coalescence aid add fashionable should with water latting drown, during middling speed stirs, slowly add, prevent from adding the too fast localized agglomeration breakdown of emulsion that causes.
2. powder adds the fashionable middling speed of should opening and stirs and slowly to add, and prevents agglomerate, and the rear application clear water that fed intake cleans casing wall, and high speed dispersion is qualified to fineness.
3. defoamer must high speed dispersion after adding, otherwise easily there is shrinkage cavity, goes rancid.
4. necessary lucifuge while producing, light trigger also needs to keep in Dark Place, and finished product is used black plastic bucket packing.
During construction, adopt the form of construction work of spraying, can adopt heating according to room temperature height situation, add sailor's section and carry out adjusting coating viscosity.Dry two steps that are divided into: pre-volatile dry and the photocured cross-linked film forming of UV.Forced drying method is used in suggestion, and (50 ℃, 15min) re-use UV light irradiation (300-350mj/m first to use infrared drying
2).
The present invention mainly utilizes UV curing urethane dispersion in formula, film coalescence aid, flow agent, defoamer, thickening material, light trigger, water etc. in plate fitment coating process, there are good sticking power, hardness, curing speed is fast, environmental protection, low cost, the most important thing is excellent chemical resistance.
According to recommend to meet < < KCMA A161.1-2000 cabinet after construction technology making sheet and bathe the performance of cabinet and construction standard > > in related request to paint film.
Detection data are as follows:
The test of detected result conformance with standard to the test of chemical resistance and other fundamental propertys, it is qualified to be judged to.
Embodiment
Finished product significant parameter of the present invention is as follows:
Embodiment 1
Formula:
70 kilograms of water-based UV curing acrylic polyurethane dispersions, 5 kilograms, mute powder, 6 kilograms of film coalescence aid, 1 kilogram of flow agent, 1 kilogram of defoamer, 2 kilograms of thickening materials, 4 kilograms of light triggers, 11 kilograms, water, add up to double centner.
Water-based UV curing acrylic polyurethane dispersions is Beyer Co., Ltd's product, and the trade mark is UVLS2282
Ya Fenwei GRACE company product, the trade mark is SY7000
Film coalescence aid WeiDOW company product, the trade mark is DPNB, DPM
Flow agent WeiBYK company product, the trade mark is BYK333
Defoamer is TEGO company product, and the trade mark is TEGO901W
Thickening material is Rhom and Hass's product, and the trade mark is RM-12W, RM-2050D
Light trigger is that Hubei Gu Run company product grade is TPO, and Changzhou Hua Tai company product grade is BP.
Manufacture craft is as follows: first drop into UVLS2282, will after DPM, DPNB premix, slowly drip, then add successively SY7000, BYK333, TEGO901W under middling speed stirs, after high speed dispersion 15 minutes is qualified to fineness, with RM12W and RM-2050D, adjust viscosity.
Construction proportioning: adding water, to adjust in right amount paint temperature be 25 ℃, is used T-4 cup test working viscosity at 40-50S.
Form of construction work: hand spray
Drying conditions: 50 ℃ infrared leveling machine upper 15 minutes again after spraying, then carry out UV photocuring, photocuring energy 300-350mj/cm
2.
According to limits of harmful substances > > in < < GB 24410-2009 indoor decorating and refurnishing materials water-borne wood coating and < < Q/TOLD 30-2011 aquosity ultraviolet light (UV) solidified carpentry coating > >, detect, actual detection numerical value is as follows:
1, after condition in container parameter stirs evenly without lump
2, fineness 35 μ m
3, appearance of film is normal
4, gloss (60 ° of angles) is decided through consultation (30%)
5, pencil hardness (scratch) 2H
6, sticking power (drawing compartment apart from 2mm) is 1 grade
7, water tolerance (24h) non-foaming, wrinkle resistant, do not come off
8, alcohol resistance (50% ethanol, 2h) non-foaming, wrinkle resistant, do not come off
9, dry heat resistance (90 ± 2) ℃, 1 grade of level
10, volatile organic compounds (VOC) 219g/L
11, benzene,toluene,xylene, ethylbenzene, mg/kg does not detect
12, halohydrocarbon, mg/kg does not detect
13, formaldehyde, mg/kg does not detect
Embodiment 2
Formula:
50 kilograms of water-based UV curing acrylic polyurethane dispersions, 20 kilograms of water soluble acrylic acid polyurethane dispersions, 5 kilograms, mute powder, 6 kilograms of film coalescence aid, 1 kilogram of flow agent, 1 kilogram of defoamer, 2 kilograms of thickening materials, 4 kilograms of light triggers, 11 kilograms, water, add up to double centner.
Water-based UV curing acrylic polyurethane dispersions is Beyer Co., Ltd's product, and the trade mark is UVLS2282
Water soluble acrylic acid polyurethane dispersions is DSM N. V.'s product, and the trade mark is E-129
Ya Fenwei GRACE company product, the trade mark is SY7000
Film coalescence aid WeiDOW company product, the trade mark is DPNB, DPM
Flow agent WeiBYK company product, the trade mark is BYK333
Defoamer is TEGO company product, and the trade mark is TEGO901W
Thickening material is Rhom and Hass's product, and the trade mark is RM-12W, RM-2050D
Light trigger is that Hubei Gu Run company product grade is TPO, and Changzhou Hua Tai company product grade is BP.
Manufacture craft is as follows: first drop into UVLS2282, under middling speed stirs, will after DPM, DPNB premix, slowly drip, then add successively SY7000, BYK333, TEGO901W, after high speed dispersion 15 minutes is qualified to fineness, drop into E-129, stir evenly rear by RM12W and RM-2050D adjustment viscosity.
Construction proportioning: add the appropriate 25 ℃/T-4 of adjustment of water viscosity at 40-50 ",
Form of construction work: hand spray,
Drying conditions: 50 ℃ infrared leveling machine upper 15 minutes again after spraying, then carry out UV photocuring, photocuring energy 300-350mj/cm
2.
According to limits of harmful substances > > in < < GB 24410-2009 indoor decorating and refurnishing materials water-borne wood coating and < < Q/TOLD 30-2011 aquosity ultraviolet light (UV) solidified carpentry coating > >, detect, actual detection numerical value is as follows:
1, after condition in container parameter stirs evenly without lump
2, fineness 35 μ m
3, appearance of film is normal
4, gloss (60 ° of angles) is decided through consultation (30%)
5, pencil hardness (scratch) 2H
6, sticking power (drawing compartment apart from 2mm) is 1 grade
7, water tolerance (24h) non-foaming, wrinkle resistant, do not come off
8, alcohol resistance (50% ethanol, 2h) non-foaming, wrinkle resistant, do not come off
9, dry heat resistance (90 ± 2) ℃, 1 grade of level
10, volatile organic compounds (VOC) 225g/L
11, benzene,toluene,xylene, ethylbenzene, mg/kg does not detect
12, halohydrocarbon, mg/kg does not detect
13, formaldehyde, mg/kg does not detect
Embodiment 3
Formula:
60 kilograms of water soluble acrylic acid polyurethane dispersions, 6 kilograms, mute powder, 6 kilograms of film coalescence aid, 2 kilograms of flow agents, 2 kilograms of defoamers, 2 kilograms of thickening materials, 6 kilograms of light triggers, 16 kilograms, water, add up to double centner.
Water-based UV curing acrylic polyurethane dispersions is Beyer Co., Ltd's product, and the trade mark is UVLS2282
Water soluble acrylic acid polyurethane dispersions is DSM N. V.'s product, and the trade mark is E-129
Ya Fenwei GRACE company product, the trade mark is SY7000
Film coalescence aid WeiDOW company product, the trade mark is DPNB, DPM
Flow agent WeiBYK company product, the trade mark is BYK333
Defoamer is TEGO company product, and the trade mark is TEGO901W
Thickening material is Rhom and Hass's product, and the trade mark is RM-12W, RM-2050D
Light trigger is that Hubei Gu Run company product grade is TPO, and Changzhou Hua Tai company product grade is BP.
Make, construct, be dried, detect the same embodiment.
Embodiment 4
Formula:
60 kilograms of water soluble acrylic acid polyurethane dispersions, 4 kilograms, mute powder, 3 kilograms of film coalescence aid, 1 kilogram of flow agent, 1 kilogram of defoamer, 1 kilogram of thickening material, 4 kilograms of light triggers, 26 kilograms, water, add up to double centner.
Water-based UV curing acrylic polyurethane dispersions is Beyer Co., Ltd's product, and the trade mark is UVLS2282
Water soluble acrylic acid polyurethane dispersions is DSM N. V.'s product, and the trade mark is E-129
Ya Fenwei GRACE company product, the trade mark is SY7000
Film coalescence aid WeiDOW company product, the trade mark is DPNB, DPM
Flow agent WeiBYK company product, the trade mark is BYK333
Defoamer is TEGO company product, and the trade mark is TEGO901W
Thickening material is Rhom and Hass's product, and the trade mark is RM-12W, RM-2050D
Light trigger is that Hubei Gu Run company product grade is TPO, and Changzhou Hua Tai company product grade is BP.
Make, construct, be dried, detect the same embodiment.
Claims (9)
1. a water-based UV clear finish product that is applicable to cabinet, is characterized in that: by following constituent and weight part, formed,
60 ~ 70 parts of aqueous dispersion,
4 ~ 6 parts of matting agents,
3 ~ 6 parts of film coalescence aid,
1 ~ 2 part of flow agent,
1 ~ 2 part of defoamer,
1 ~ 2 part of thickening material,
4 ~ 6 parts of light triggers,
26 ~ 6 parts, water.
2. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: described aqueous dispersion is a kind of or its mixture of water-based aliphatics UV curing acrylic polyurethane dispersions and water soluble acrylic acid polyurethane dispersions.
3. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: matting agent adopts silicon-dioxide or organic wax.
4. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: film coalescence aid is dipropylene glycol methyl ether (DPM), dipropylene glycol butyl ether (DPNB).
5. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: flow agent is polyether-modified polydimethylsiloxane interpolymer.
6. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: defoamer is polyether silicone co-polymer emulsion, containing aerosil.
7. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: thickening material is associative thickener.
8. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: light trigger is the mixture of TMDPO and benzophenone.
9. a kind of water-based UV clear finish product that is applicable to cabinet claimed in claim 1, is characterized in that: being dried need be through two step, and pre-volatile dry and UV curing cross-linked film forming are dry.
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| CN201310652490.9A CN103666237A (en) | 2013-12-06 | 2013-12-06 | Aqueous UV top-varnish product for kitchen cabinet |
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| CN201310652490.9A CN103666237A (en) | 2013-12-06 | 2013-12-06 | Aqueous UV top-varnish product for kitchen cabinet |
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| CN201310652490.9A Pending CN103666237A (en) | 2013-12-06 | 2013-12-06 | Aqueous UV top-varnish product for kitchen cabinet |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104497845A (en) * | 2014-12-26 | 2015-04-08 | 成都展辰化工有限公司 | Open type aqueous UV shower-coating clear primer |
| CN105419623A (en) * | 2015-12-29 | 2016-03-23 | 河北晨阳工贸集团有限公司 | Multifunctional aqueous UV varnish, and preparation and usage method |
| CN107573830A (en) * | 2017-10-18 | 2018-01-12 | 北京展辰新材料有限公司 | A kind of nanometer water UV ultraviolet light cured varnish and preparation method and application |
| CN109354994A (en) * | 2018-09-30 | 2019-02-19 | 佛山阳光逸采涂料科技有限公司 | A kind of UV LED UV-curable waterborne mahogany furniture coating and preparation method thereof |
| CN109486388A (en) * | 2018-09-30 | 2019-03-19 | 佛山阳光逸采涂料科技有限公司 | UV LED UV-curable waterborne timber coatings for furniture and preparation method thereof |
| CN109535284A (en) * | 2017-07-31 | 2019-03-29 | 广东华润涂料有限公司 | Photoinitiator composite suitable for UV-LED light radiation and the water-based paint compositions by its preparation |
| CN109627959A (en) * | 2018-11-06 | 2019-04-16 | 青岛展辰新材料有限公司 | Plentiful high thoroughly clear priming paint of a kind of aqueous UV high and its preparation method and application |
| CN111073494A (en) * | 2019-12-20 | 2020-04-28 | 珠海展辰新材料股份有限公司 | Water-based ultraviolet-curing solid-color coating and preparation method thereof |
| CN113512315A (en) * | 2021-07-06 | 2021-10-19 | 江苏海田技术有限公司 | UV-no skin feel coating |
| CN115746694A (en) * | 2022-11-24 | 2023-03-07 | 中华制漆(新丰）有限公司 | Water-based UV wood lacquer and preparation method thereof |
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Cited By (17)
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| CN104497845A (en) * | 2014-12-26 | 2015-04-08 | 成都展辰化工有限公司 | Open type aqueous UV shower-coating clear primer |
| CN105419623A (en) * | 2015-12-29 | 2016-03-23 | 河北晨阳工贸集团有限公司 | Multifunctional aqueous UV varnish, and preparation and usage method |
| CN105419623B (en) * | 2015-12-29 | 2017-07-07 | 河北晨阳工贸集团有限公司 | A kind of multifunctional aqueous UV varnish and its preparation and application method |
| US11814546B2 (en) | 2017-07-31 | 2023-11-14 | Guangdong Huarun Paints Co., Ltd | Photoinitiating composition suitable for UV-LED light irradiation and an aqueous coating composition prepared therefrom |
| CN109535284A (en) * | 2017-07-31 | 2019-03-29 | 广东华润涂料有限公司 | Photoinitiator composite suitable for UV-LED light radiation and the water-based paint compositions by its preparation |
| CN109535284B (en) * | 2017-07-31 | 2021-07-06 | 广东华润涂料有限公司 | Photoinitiator composition suitable for UV-LED light radiation and water-based coating composition prepared from same |
| CN107573830B (en) * | 2017-10-18 | 2020-05-05 | 青岛展辰新材料有限公司 | Nano water-based UV ultraviolet curing varnish, and preparation method and application thereof |
| CN107573830A (en) * | 2017-10-18 | 2018-01-12 | 北京展辰新材料有限公司 | A kind of nanometer water UV ultraviolet light cured varnish and preparation method and application |
| CN109354994A (en) * | 2018-09-30 | 2019-02-19 | 佛山阳光逸采涂料科技有限公司 | A kind of UV LED UV-curable waterborne mahogany furniture coating and preparation method thereof |
| CN109354994B (en) * | 2018-09-30 | 2020-11-03 | 佛山阳光逸采涂料科技有限公司 | UV LED water-based ultraviolet-curing redwood furniture coating and preparation method thereof |
| CN109486388B (en) * | 2018-09-30 | 2020-12-29 | 佛山阳光逸采涂料科技有限公司 | UV LED water-based ultraviolet-curing wooden door and furniture coating and preparation method thereof |
| CN109486388A (en) * | 2018-09-30 | 2019-03-19 | 佛山阳光逸采涂料科技有限公司 | UV LED UV-curable waterborne timber coatings for furniture and preparation method thereof |
| CN109627959A (en) * | 2018-11-06 | 2019-04-16 | 青岛展辰新材料有限公司 | Plentiful high thoroughly clear priming paint of a kind of aqueous UV high and its preparation method and application |
| CN111073494A (en) * | 2019-12-20 | 2020-04-28 | 珠海展辰新材料股份有限公司 | Water-based ultraviolet-curing solid-color coating and preparation method thereof |
| CN113512315A (en) * | 2021-07-06 | 2021-10-19 | 江苏海田技术有限公司 | UV-no skin feel coating |
| CN115746694A (en) * | 2022-11-24 | 2023-03-07 | 中华制漆(新丰）有限公司 | Water-based UV wood lacquer and preparation method thereof |
| CN115746694B (en) * | 2022-11-24 | 2024-03-01 | 中华制漆(新丰）有限公司 | Water-based UV wood paint and preparation method thereof |
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Address after: 8555 No. 201707 Shanghai city Qingpu District Songze Avenue Applicant after: Shanghai Zhanchen Paint Co., Ltd. Applicant after: Zhanchen Coatings Group Co., Ltd. Applicant after: Beijing Zhanchen Chemical Industry Co., Ltd. Applicant after: Qingdao Zhan Chen novel material company limited Applicant after: Chengdu Zhanchen Chemical Co., Ltd. Address before: 8555 No. 201707 Shanghai city Qingpu District Songze Avenue Applicant before: Shanghai Fuchen Chemical Co., Ltd. Applicant before: Zhanchen Coatings Group Co., Ltd. Applicant before: Beijing Zhanchen Chemical Industry Co., Ltd. Applicant before: Qingdao Fuchen Chemical Co., Ltd. Applicant before: Chengdu Zhanchen Chemical Co., Ltd. |
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