CN103665460B - A kind of Abrasion-resistant base for liftmobile solid tyre - Google Patents
A kind of Abrasion-resistant base for liftmobile solid tyre Download PDFInfo
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- CN103665460B CN103665460B CN201310620416.9A CN201310620416A CN103665460B CN 103665460 B CN103665460 B CN 103665460B CN 201310620416 A CN201310620416 A CN 201310620416A CN 103665460 B CN103665460 B CN 103665460B
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- carbon black
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Abstract
The invention belongs to the technical field of rubber production, be specifically related to a kind of Abrasion-resistant base for liftmobile solid tyre.This kind is for the Abrasion-resistant base of liftmobile solid tyre, be made up of following raw materials in parts by weight proportioning: natural rubber, liquid polybutadiene rubber, carbon black N234, white carbon black, silicone couplet, poly-2,3,4-trimethylammonium-1,2-dihydroquinoline, N-(1,3-dimethyl)-N '-phenyl-pphenylenediamine, zinc oxide, Zinic stearas, N-tertiary butyl benzothiazole-2-sulphenamide, tetramethyl--thiuramsulfides, Sulfur, N-ring ethylenebis dithiocarbamate phthalic imidine, tynex.This described base rubber not only has higher modulus and good wear resistance, and reversion-resistant is also better simultaneously, and hysteresis loss is also very low.
Description
Technical field
The invention belongs to the technical field of rubber production, be specifically related to a kind of Abrasion-resistant base for liftmobile solid tyre.
Background technology
Liftmobile solid tyre requires lower rolling resistance, object is to ensure that the speed of vehicle and working hour reach greatest limit, although tire tread shape, crown radius of the radian, tread design and tread thickness and these performances of acquisition have much relations, best effect be obtained and also must adopt suitable sizing compound formula.Liftmobile in use overloads work often, and the distortion and the creep effect which results in tire increase, and along with distortion and creep effect increase, the rolling resistance of tire also can increase thereupon, and consequently Vehicle Speed reduces, energy expenditure acceleration.Although the good high-module sizing material of reinforcing property can be obtained by selecting suitable kind of carbon black and consumption, the distortion of tire can be reduced simultaneously, but the increase of hysteresis loss also can affect rolling resistance, therefore will average out between high-module and low hysteresis loss, solid tyre also must have good wear resistance and tear strength.
Solid tyre needs longer curing time guarantee tread rubber centre to reach desirable state of vulcanization, the performance of this long-time sulfuration to tire has a significant impact, can cause in tread surface and tyre surface bottom certain depth and produce over cure, although reversion there is no obvious decline at look-up table surface hardness usually, but in tire used process namely in a dynamic condition, hardness and modulus rapidly decline can cause abrasion to be accelerated, rolling resistance increases and heat-dissipating increases, and heat-dissipating can make modulus and hardness decline further.
In sum, if the requirement that solid tyre will meet low-rolling-resistance must have following performance: 1. good reversion-resistant; 2, high-module and low hysteresis loss; 3, good wear resistant.
Summary of the invention
The object of the invention is to the defect for above-mentioned existence and provide a kind of Abrasion-resistant base for liftmobile solid tyre, this base rubber not only has higher modulus and good wear resistance, and reversion-resistant is also better simultaneously, and hysteresis loss is also very low.
Technical scheme of the present invention is: a kind of Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 90 ~ 100 parts
Liquid polybutadiene rubber 6 ~ 11 parts
Carbon black N234 25 ~ 35 parts
White carbon black 5 ~ 8 parts
Silicone couplet 0.2 ~ 0.5 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.0 ~ 1.5 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.0 ~ 1.5 parts
5 ~ 9 parts, zinc oxide
Zinic stearas 6 ~ 8 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.2 ~ 2.1 parts
Tetramethyl--thiuramsulfides 0.3 ~ 0.7 part
Sulfur 1.5 ~ 2.0 parts
N-cyclohexylthiophthalimide 0.15 ~ 0.25 part
Tynex 3 ~ 6 parts.
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 92.8 parts
Liquid polybutadiene rubber 6.7 parts
Carbon black N234 25.5 parts
White carbon black 5.8 parts
Silicone couplet 0.25 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.1 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.1 parts
5.9 parts, zinc oxide
Zinic stearas 6.8 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.25 parts
Tetramethyl--thiuramsulfides 0.37 part
Sulfur 1.6 parts
N-cyclohexylthiophthalimide 0.16 part
Tynex 3.6 parts.
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 94.2 parts
Liquid polybutadiene rubber 7.3 parts
Carbon black N234 26.2 parts
White carbon black 6.3 parts
Silicone couplet 0.31 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.23 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.23 parts
6.2 parts, zinc oxide
Zinic stearas 7.1 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.34 parts
Tetramethyl--thiuramsulfides 0.41 part
Sulfur 1.65 parts
N-cyclohexylthiophthalimide 0.18 part
Tynex 4.1 parts.
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 96.5 parts
Liquid polybutadiene rubber 9.8 parts
Carbon black N234 31.3 parts
White carbon black 7.4 parts
Silicone couplet 0.43 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.38 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.38 parts
7.73 parts, zinc oxide
Zinic stearas 7.5 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.98 parts
Tetramethyl--thiuramsulfides 0.58 part
Sulfur 1.75 parts
N-cyclohexylthiophthalimide 0.21 part
Tynex 5.5 parts.
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 99.4 parts
Liquid polybutadiene rubber 10.7 parts
Carbon black N234 34.9 parts
White carbon black 7.85 parts
Silicone couplet 0.48 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.47 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.47 parts
8.7 parts, zinc oxide
Zinic stearas 7.82 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 2.0 parts
Tetramethyl--thiuramsulfides 0.68 part
Sulfur 1.93 parts
N-cyclohexylthiophthalimide 0.24 part
Tynex 5.8 parts.
Beneficial effect of the present invention is: the Abrasion-resistant base for liftmobile solid tyre of the present invention, and 100% fixed stretching strength is 2.7 ~ 3.2MPa, and conservation rate is 94% ~ 96%; 300% fixed stretching strength is 14 ~ 17MPa, and conservation rate is 98% ~ 99%; Tensile strength is 28 ~ 30MPa, and conservation rate is 97.5% ~ 98.6%; Tensile yield is 500% ~ 510%, and conservation rate is 96.5% ~ 98.8%; At 25 DEG C, rebound resilience is 70% ~ 73%, and conservation rate is 96% ~ 98%; Hardness is 66 ~ 68; Wear index 97 ~ 99, conservation rate is 100%, C shape of the mouth as one speaks tear strength is 110 ~ 122N/mm, and conservation rate is 80% ~ 85%.At 160 DEG C, sulfuration is after 60 minutes, and reversion percentage drops to 4 ~ 5%.
In sum, this described base rubber not only has higher modulus and good wear resistance, and reversion-resistant is also better simultaneously, and hysteresis loss is also very low.
Embodiment
Below by specific embodiment, the present invention will be described in detail.
Embodiment 1
For an Abrasion-resistant base for liftmobile solid tyre, be made up of following raw materials in parts by weight proportioning:
Natural rubber 90 parts
Liquid polybutadiene rubber 6 parts
Carbon black N234 25 parts
White carbon black 5 parts
Silicone couplet 0.2 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.0 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.0 parts
5 parts, zinc oxide
Zinic stearas 6 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.2 parts
Tetramethyl--thiuramsulfides 0.3 part
Sulfur 1.5 parts
N-cyclohexylthiophthalimide 0.15 part
Tynex 3 parts.
Adopt the Abrasion-resistant base for liftmobile solid tyre described in embodiment 1,100% fixed stretching strength is 2.7MPa, and conservation rate is 94%; 300% fixed stretching strength is 14MPa, and conservation rate is 98%; Tensile strength is 28MPa, and conservation rate is 97.5%; Tensile yield is 500%, and conservation rate is 96.5%; At 25 DEG C, rebound resilience is 70%, and conservation rate is 96%; Hardness is 66; Wear index 97, conservation rate is 100%, C shape of the mouth as one speaks tear strength is 110N/mm, and conservation rate is 80%.At 160 DEG C, sulfuration is after 60 minutes, and reversion percentage drops to 4%.
Embodiment 2
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 92.8 parts
Liquid polybutadiene rubber 6.7 parts
Carbon black N234 25.5 parts
White carbon black 5.8 parts
Silicone couplet 0.25 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.1 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.1 parts
5.9 parts, zinc oxide
Zinic stearas 6.8 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.25 parts
Tetramethyl--thiuramsulfides 0.37 part
Sulfur 1.6 parts
N-cyclohexylthiophthalimide 0.16 part
Tynex 3.6 parts.
Adopt the Abrasion-resistant base for liftmobile solid tyre described in embodiment 2,100% fixed stretching strength is 2.82MPa, and conservation rate is 94.6%; 300% fixed stretching strength is 15.7MPa, and conservation rate is 98.9%; Tensile strength is 28.30MPa, and conservation rate is 97.86%; Tensile yield is 506%, and conservation rate is 96.8%; At 25 DEG C, rebound resilience is 70.3%, and conservation rate is 96.8%; Hardness is 66.8; Wear index 97.9, conservation rate is 100%, C shape of the mouth as one speaks tear strength is 112N/mm, and conservation rate is 81.5%.At 160 DEG C, sulfuration is after 60 minutes, and reversion percentage drops to 4.5%.
Embodiment 3
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 94.2 parts
Liquid polybutadiene rubber 7.3 parts
Carbon black N234 26.2 parts
White carbon black 6.3 parts
Silicone couplet 0.31 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.23 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.23 parts
6.2 parts, zinc oxide
Zinic stearas 7.1 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.34 parts
Tetramethyl--thiuramsulfides 0.41 part
Sulfur 1.65 parts
N-cyclohexylthiophthalimide 0.18 part
Tynex 4.1 parts.
Adopt the Abrasion-resistant base for liftmobile solid tyre described in embodiment 3,100% fixed stretching strength is 2.96MPa, and conservation rate is 95.6%; 300% fixed stretching strength is 16.4MPa, and conservation rate is 98.7%; Tensile strength is 28.9MPa, and conservation rate is 98%; Tensile yield is 505%, and conservation rate is 97.3%; At 25 DEG C, rebound resilience is 72.4%, and conservation rate is 97.1%; Hardness is 67.5; Wear index 98.1, conservation rate is 100%, C shape of the mouth as one speaks tear strength is 119N/mm, and conservation rate is 83.6%.At 160 DEG C, sulfuration is after 60 minutes, and reversion percentage drops to 4.7%.
Embodiment 4
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 96.5 parts
Liquid polybutadiene rubber 9.8 parts
Carbon black N234 31.3 parts
White carbon black 7.4 parts
Silicone couplet 0.43 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.38 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.38 parts
7.73 parts, zinc oxide
Zinic stearas 7.5 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.98 parts
Tetramethyl--thiuramsulfides 0.58 part
Sulfur 1.75 parts
N-cyclohexylthiophthalimide 0.21 part
Tynex 5.5 parts.
Adopt the Abrasion-resistant base for liftmobile solid tyre described in embodiment 4,100% fixed stretching strength is 3.0MPa, and conservation rate is 95.31%; 300% fixed stretching strength is 16.32MPa, and conservation rate is 98.75%; Tensile strength is 29.12MPa, and conservation rate is 98.35%; Tensile yield is 506.3%, and conservation rate is 97.71%; At 25 DEG C, rebound resilience is 72.56%, and conservation rate is 97.63%; Hardness is 66.98; Wear index 98.67, conservation rate is 100%, C shape of the mouth as one speaks tear strength is 121.98N/mm, and conservation rate is 83.57%.At 160 DEG C, sulfuration is after 60 minutes, and reversion percentage drops to 4.87%.
Embodiment 5
The described Abrasion-resistant base for liftmobile solid tyre, is made up of following raw materials in parts by weight proportioning:
Natural rubber 99.4 parts
Liquid polybutadiene rubber 10.7 parts
Carbon black N234 34.9 parts
White carbon black 7.85 parts
Silicone couplet 0.48 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.47 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.47 parts
8.7 parts, zinc oxide
Zinic stearas 7.82 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 2.0 parts
Tetramethyl--thiuramsulfides 0.68 part
Sulfur 1.93 parts
N-cyclohexylthiophthalimide 0.24 part
Tynex 5.8 parts
Adopt the Abrasion-resistant base for liftmobile solid tyre described in embodiment 5,100% fixed stretching strength is 3.184MPa, and conservation rate is 95.62%; 300% fixed stretching strength is 16.89MPa, and conservation rate is 98.76%; Tensile strength is 29.94MPa, and conservation rate is 98.56%; Tensile yield is 509.7%, and conservation rate is 98.77%; At 25 DEG C, rebound resilience is 72.9%, and conservation rate is 97.63%; Hardness is 67.85; Wear index 98.36, conservation rate is 100%, C shape of the mouth as one speaks tear strength is 121.3N/mm, and conservation rate is 84.73%.At 160 DEG C, sulfuration is after 60 minutes, and reversion percentage drops to 4.59%.
Embodiment 6
For an Abrasion-resistant base for liftmobile solid tyre, be made up of following raw materials in parts by weight proportioning:
Natural rubber 100 parts
Liquid polybutadiene rubber 11 parts
Carbon black N234 35 parts
White carbon black 8 parts
Silicone couplet 0.5 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.5 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.5 parts
9 parts, zinc oxide
Zinic stearas 8 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 2.1 parts
Tetramethyl--thiuramsulfides 0.7 part
Sulfur 2.0 parts
N-cyclohexylthiophthalimide 0.25 part
Tynex 6 parts.
Adopt the Abrasion-resistant base for liftmobile solid tyre described in embodiment 6,100% fixed stretching strength is 3.2MPa, and conservation rate is 96%; 300% fixed stretching strength is 17MPa, and conservation rate is 99%; Tensile strength is 30MPa, and conservation rate is 98.6%; Tensile yield is 510%, and conservation rate is 98.8%; At 25 DEG C, rebound resilience is 73%, and conservation rate is 98%; Hardness is 68; Wear index 99, conservation rate is 100%, C shape of the mouth as one speaks tear strength is 122N/mm, and conservation rate is 85%.At 160 DEG C, sulfuration is after 60 minutes, and reversion percentage drops to 5%.
Claims (5)
1. for an Abrasion-resistant base for liftmobile solid tyre, it is characterized in that, be made up of following raw materials in parts by weight proportioning:
Natural rubber 90 ~ 100 parts
Liquid polybutadiene rubber 6 ~ 11 parts
Carbon black N234 25 ~ 35 parts
White carbon black 5 ~ 8 parts
Silicone couplet 0.2 ~ 0.5 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.0 ~ 1.5 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.0 ~ 1.5 parts
5 ~ 9 parts, zinc oxide
Zinic stearas 6 ~ 8 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.2 ~ 2.1 parts
Tetramethyl--thiuramsulfides 0.3 ~ 0.7 part
Sulfur 1.5 ~ 2.0 parts
N-cyclohexylthiophthalimide 0.15 ~ 0.25 part
Tynex 3 ~ 6 parts.
2. according to claim 1 for the Abrasion-resistant base of liftmobile solid tyre, it is characterized in that, be made up of following raw materials in parts by weight proportioning:
Natural rubber 92.8 parts
Liquid polybutadiene rubber 6.7 parts
Carbon black N234 25.5 parts
White carbon black 5.8 parts
Silicone couplet 0.25 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.1 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.1 parts
5.9 parts, zinc oxide
Zinic stearas 6.8 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.25 parts
Tetramethyl--thiuramsulfides 0.37 part
Sulfur 1.6 parts
N-cyclohexylthiophthalimide 0.16 part
Tynex 3.6 parts.
3. according to claim 1 for the Abrasion-resistant base of liftmobile solid tyre, it is characterized in that, be made up of following raw materials in parts by weight proportioning:
Natural rubber 94.2 parts
Liquid polybutadiene rubber 7.3 parts
Carbon black N234 26.2 parts
White carbon black 6.3 parts
Silicone couplet 0.31 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.23 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.23 parts
6.2 parts, zinc oxide
Zinic stearas 7.1 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.34 parts
Tetramethyl--thiuramsulfides 0.41 part
Sulfur 1.65 parts
N-cyclohexylthiophthalimide 0.18 part
Tynex 4.1 parts.
4. according to claim 1 for the Abrasion-resistant base of liftmobile solid tyre, it is characterized in that, be made up of following raw materials in parts by weight proportioning:
Natural rubber 96.5 parts
Liquid polybutadiene rubber 9.8 parts
Carbon black N234 31.3 parts
White carbon black 7.4 parts
Silicone couplet 0.43 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.38 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.38 parts
7.73 parts, zinc oxide
Zinic stearas 7.5 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 1.98 parts
Tetramethyl--thiuramsulfides 0.58 part
Sulfur 1.75 parts
N-cyclohexylthiophthalimide 0.21 part
Tynex 5.5 parts.
5. according to claim 1 for the Abrasion-resistant base of liftmobile solid tyre, it is characterized in that, be made up of following raw materials in parts by weight proportioning:
Natural rubber 99.4 parts
Liquid polybutadiene rubber 10.7 parts
Carbon black N234 34.9 parts
White carbon black 7.85 parts
Silicone couplet 0.48 part
Poly-2,2,4-trimethylammonium-1,2-dihydroquinoline 1.47 parts
N-(1,3-dimethylbutyl)-N '-phenyl-pphenylenediamine 1.47 parts
8.7 parts, zinc oxide
Zinic stearas 7.82 parts
N-tertiary butyl-2-[4-morpholinodithio sulphenamide 2.0 parts
Tetramethyl--thiuramsulfides 0.68 part
Sulfur 1.93 parts
N-cyclohexylthiophthalimide 0.24 part
Tynex 5.8 parts.
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CN110183744A (en) * | 2019-04-26 | 2019-08-30 | 中策橡胶集团有限公司 | A kind of mixing method of snowfield tire and snowfield tire tread rubber composition and rubber composition |
CN110628091A (en) * | 2019-09-06 | 2019-12-31 | 芜湖集拓实心胎有限公司 | Puncture-resistant engineering solid tire |
CN117447794B (en) * | 2023-12-26 | 2024-03-12 | 河北技投机械设备有限公司 | Ternary olefin copolymer composition for slurry pump, and preparation method and application thereof |
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