CN103656553A - Traditional Chinese medicine preparation for treating arthralgia of bones and joints and soft tissue injuries and preparation method thereof - Google Patents
Traditional Chinese medicine preparation for treating arthralgia of bones and joints and soft tissue injuries and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a traditional Chinese medicine, and particularly relates to a traditional Chinese medicine preparation for treating arthralgia of bones and joints and soft tissue injuries and a preparation method thereof. The traditional Chinese medicine preparation is prepared from the following raw materials in parts by weight: 1-5 parts of venenum bufonis, 10-15 parts of nux vomica, 20-60 parts of asarum, 20-60 parts of Chinese prickly ash, 12-25 parts of fructus evodiae, 12-25 parts of radix aconiti agrestis, 12-25 parts of semen brassicae, 12-20 parts of fructus gleditsiae offieinalis, 12-20 parts of pseudo-ginseng, 15-26 parts of camphor, 10-15 parts of rhizoma zingiberis, 10-15 parts of pepper, 2-8 parts of menthol, 10-15 parts of root of yellow monkshood, 12-15 parts of girald daphne barks, 12-15 parts of syzygium aromaticum, 12-15 parts of jasmine cape jasmine and 12-15 parts of galangal. The preparation has the beneficial effects of relaxing tendons and activating collaterals, promoting blood circulation to remove blood stasis and decreasing swelling to relieve pains, and is used for treating arthralgia of bones and joints and soft tissue and muscle injuries as well as pains caused by scapulohumeral periarthritis, osteoproliferation, traumatic injury, chronic strain, protrusion of lumbar intervertebral disc and the like.
Description
Technical field
The present invention relates to the field of Chinese medicines, relate in particular to a kind of Chinese medicine preparation for the treatment of muscles and bones arthralgia and soft tissue injury and preparation method thereof.
Background technology
Muscles and bones arthralgia and soft tissue, muscle injury, and scapulohumeral periarthritis, hyperosteogeny, traumatic injury, chronic strain, prolapse of lumbar intervertebral disc etc. all can cause pain.These pain have greatly affected daily life, and daily life is brought inconvenience.
Western medicine is due to highly purified molecule cluster, and concentrated absorption is unavoidably in evil case, to the heart, brain, liver, the equal toxic side effect of kidney.
There is no at present a kind of pure Chinese medicine preparation that can effectively alleviate this series symptom.
Summary of the invention
The object of invention: for treatment muscles and bones arthralgia and soft tissue injury being provided, can alleviating Chinese medicine preparation of sufferer pain and preparation method thereof.
In order to reach as above object, the present invention takes following technical scheme: a kind of Chinese medicine preparation for the treatment of muscles and bones arthralgia and soft tissue injury, it is characterized in that, and its raw material by following components by weight percent is prepared from: Venenum Bufonis 1-5 part; Semen Strychni 10-15 part; Herba Asari 20-60 part; Pericarpium Zanthoxyli 20-60 part; Fructus Evodiae 12-25 part; Radix Aconiti Kusnezoffii 12-25 part; Semen Sinapis Albae 12-25 part; Fructus Gleditsiae Abnormalis 12-20 part; Radix Notoginseng 12-20 part; Camphora 15-26 part; Rhizoma Zingiberis 10-15 part; Fructus Piperis 10-15 part; Mentholum 2-8 part; Radix aconiti szechenyiani 10-15 part; Daphne giraldii Nitsche 12-15 part; Flos Caryophylli 12-15 part; Fructus Gardeniae 12-15 part; Rhizoma Alpiniae Officinarum 12-15 part.
The further technical scheme of the present invention is, its raw material by following components by weight percent is prepared from: 2.7 parts of Venenum Bufoniss; 13.3 parts of Semen Strychni; 41.4 parts of Herba Asaris; 41.4 parts, Pericarpium Zanthoxyli; 13.8 parts of Fructus Evodiaes; 13.8 parts of Radix Aconiti Kusnezoffii; 13.8 parts of Semen Sinapis Albaes; 13.8 parts of Fructus Gleditsiae Abnormalis; 13.8 parts of Radix Notoginseng; 20.7 parts of Camphoras; 13.8 parts of Rhizoma Zingiberiss; 13.8 parts, Fructus Piperis; 6.9 parts of Mentholums; 13.8 parts of Radix aconiti szechenyiani; 13.8 parts of Daphne giraldii Nitsche; 13.8 parts of Flos Caryophyllis; 13.8 parts of Fructus Gardeniaes; 13.8 parts of Rhizoma Alpiniae Officinarums.
3. the method for preparation as preparation as above, is characterized in that, comprises following steps:
Powder process: Venenum Bufonis is ground into fine powder, crosses 100 mesh sieves; Semen Strychni, Flos Caryophylli, Pericarpium Zanthoxyli, Fructus Piperis, Rhizoma Zingiberis, Rhizoma Alpiniae Officinarum, Semen Sinapis Albae, Herba Asari are ground into coarse powder, cross 60 mesh sieves;
Extraction: add 80% alcohol reflux three times, each 3 hours, medicinal residues were standby;
Preliminary mixing: merge extractive liquid,, filter, Camphora, Mentholum are added in filtrate and mixed, stir, standby;
Second extraction: Fructus Evodiae, Radix Aconiti Kusnezoffii, Fructus Gleditsiae Abnormalis, Radix Notoginseng, Fructus Piperis, Radix aconiti szechenyiani, Daphne giraldii Nitsche, Fructus Gardeniae medicament disintegrating are become to powder, mix with above-mentioned medicinal residues, add 60% ethanol, reflux secondary, each 1 hour;
Produce: merge extractive liquid,, filter, Venenum Bufonis powder is added in filtrate, mix, standing, filter, filtrate and above-mentioned ethanol extract merge, and adjusting concentration of alcohol is 55%, obtains.
Adopt as above the present invention of technical scheme, there is following beneficial effect: relaxing muscles and tendons and activating QI and blood in the collateral, blood circulation promoting and blood stasis dispelling, reducing swelling and alleviating pain.For muscles and bones arthralgia and soft tissue, muscle injury, and the pain that causes such as scapulohumeral periarthritis, hyperosteogeny, traumatic injury, chronic strain, prolapse of lumbar intervertebral disc.Through clinical trial, find that there is fabulous therapeutic effect.
The specific embodiment
Below embodiments of the invention are described, embodiment is not construed as limiting the invention:
Be below embodiments of the invention 1, i.e. optimum embodiment:
13.8 parts of 13.8 portions of Rhizoma Alpiniae Officinarums of 13.8 portions of Fructus Gardeniaes of 13.8 portions of Flos Caryophyllis of 13.8 parts of Daphne giraldii Nitsche of 6.9 parts of Radix aconiti szechenyiani of 13.8 parts of Mentholums of 13.8 portions of Fructus Piperiss of 20.7 portions of Rhizoma Zingiberiss of 13.8 parts of Camphoras of 13.8 portions of Radix Notoginseng of 13.8 parts of Fructus Gleditsiae Abnormalis of 13.8 parts of Semen Sinapis Albaes of 13.8 portions of Radix Aconiti Kusnezoffii of 41.4 parts of Fructus Evodiaes of 41.4 portions of Pericarpium Zanthoxylies of 13.3 parts of Herba Asaris of 2.7 parts of Semen Strychni of [prescription] Venenum Bufonis
[method for making] Venenum Bufonis is ground into fine powder; Semen Strychni, Flos Caryophylli, Pericarpium Zanthoxyli, Fructus Piperis, Rhizoma Zingiberis, Rhizoma Alpiniae Officinarum, Semen Sinapis Albae, Herba Asari are ground into coarse powder, add 80% alcohol reflux three times, each 3 hours, medicinal residues are standby, and merge extractive liquid, filters, Camphora, Mentholum are added to dissolved in filtrate, stir, standby; Seven tastes such as all the other Daphne giraldii Nitsche, are ground into coarse powder, mix with above-mentioned medicinal residues, add 60% ethanol, reflux secondary, each 1 hour, merge extractive liquid,, filters, and Venenum Bufonis fine powder is added in filtrate, mix, standing, filter, filtrate and above-mentioned ethanol extract merge, adjusting concentration of alcohol is 55%, obtains.
Embodiment 2; Method for making is with embodiment 1; Its formula is as follows:
1 part of Venenum Bufonis; 10 parts of Semen Strychni; 20 parts of Herba Asaris; 20 parts, Pericarpium Zanthoxyli; 12 parts of Fructus Evodiaes; 12 parts of Radix Aconiti Kusnezoffii; 12 parts of Semen Sinapis Albaes; 12 parts of Fructus Gleditsiae Abnormalis; 12 parts of Radix Notoginseng; 15 parts of Camphoras; 10 parts of Rhizoma Zingiberiss; 10 parts, Fructus Piperis; 2 parts of Mentholums; 10 parts of Radix aconiti szechenyiani; 12 parts of Daphne giraldii Nitsche; 12 parts of Flos Caryophyllis; 12 parts of Fructus Gardeniaes; 12 parts of Rhizoma Alpiniae Officinarums.
Embodiment 3; Method for making is with embodiment 1; Its formula is as follows:
5 parts of Venenum Bufoniss; 15 parts of Semen Strychni; 60 parts of Herba Asaris; 60 parts, Pericarpium Zanthoxyli; 25 parts of Fructus Evodiaes; 25 parts of Radix Aconiti Kusnezoffii; 25 parts of Semen Sinapis Albaes; 20 parts of Fructus Gleditsiae Abnormalis; 20 parts of Radix Notoginseng; 26 parts of Camphoras; 15 parts of Rhizoma Zingiberiss; 15 parts, Fructus Piperis; 8 parts of Mentholums; 15 parts of Radix aconiti szechenyiani; 15 parts of Daphne giraldii Nitsche; 15 parts of Flos Caryophyllis; 15 parts of Fructus Gardeniaes; 15 parts of Rhizoma Alpiniae Officinarums.
[character] this product is henna supernatant liquid; Gas is fragrant.
This product 60ml is got in [discriminating] 1, be concentrated into thick paste shape, add chloroform-ethanol (10:1) mixed solution 30ml and strong ammonia solution 5ml, close plug, jolting 5 minutes, place 2 hours, filter filtrate evaporate to dryness, residue adds chloroform 1ml to be made to dissolve, as need testing solution, separately get Semen Strychni control medicinal material 0.5g, add chloroform-ethanol (10:1) mixed solution 30ml and strong ammonia solution 5ml, with legal system, obtain control medicinal material solution.The peace strychnine reference substance of choosing scholars as officials again, chlorination is copied into every 1ml and is respectively contained the mixed solution of 1mg, in contrast product solution.According to thin layer chromatography test, draw each 10 μ l of above-mentioned three kinds of solution,
Put respectively in same and take on the silica gel g thin-layer plate that carboxymethyl cellulose sodium is adhesive, the upper solution of toluene-acetone-ethanol-strong ammonia solution (4:6:0.6:1) of take is developing solvent, launch, take out, dry, spray is with rare bismuth potassium iodide test solution, in test sample chromatograph, with control medicinal material and the corresponding position of reference substance chromatograph on, the speckle of aobvious same color.
2. get this product 20ml, be concentrated into thick paste shape, add ethanol 25ml, supersound process 20 minutes, filters, filtrate evaporate to dryness, and residue adds ethanol 2ml to be made to dissolve, as need testing solution.Separately get Fructus Evodiae control medicinal material 0.5g, add ethanol 20ml, be made in the same way of control medicinal material solution.According to thin layer chromatography, test, draw above-mentioned need testing solution 1 μ l, control medicinal material solution 2 μ l, put respectively in same and take on the silica gel g thin-layer plate that sodium carboxymethyl cellulose is adhesive, n-butyl alcohol-glacial acetic acid-the water (5:1:1) of take is developing solvent, launches, and takes out, dry, put under ultra-violet lamp (365nm) and inspect.In test sample chromatograph, with the corresponding position of control medicinal material chromatograph on, the fluorescence speckle of aobvious same color.
[inspection] 1 amount of alcohol: should be 50%～60%.
2. total solid: it is appropriate to get this product, filters, and precision measures filtrate 25ml, measures in accordance with the law, leaves over residue and must not be less than 3.0%(g/ml).
3. limit test of microbe:
Bacterial population≤100/ml yeast and mold number≤100/ml
Pseudomonas aeruginosa, staphylococcus aureus all must not detect.
[assay] is according to high effective liquid chromatography for measuring.
chromatographic condition and system suitability testwith silica gel, it is filler; Normal hexane-methylene chloride-methanol-strong ammonia solution (45:40:5:0.35) is mobile phase; Detection wavelength is 254nm; Number of theoretical plate calculates and should be not less than 4000 by strychnine peak.
the preparation of reference substance solutionit is appropriate that precision takes strychnine reference substance, adds ethyl acetate and make every 1ml containing the solution of 50 μ g, shake up, both.
the preparation of need testing solutionaccurate this product 2ml that draws, put in water-bath and steam extremely without alcohol taste, add water 10ml and strong ammonia solution 2ml, put in separatory funnel, add 5 (15ml of chloroform extraction, 15ml, 15ml, 10ml, 10ml), chloroform solution merges, wave to about 15ml, put in separatory funnel, add sulfuric acid solution (3-100ml) and extract 5 (15ml, 15ml, 15ml, 10ml, 10ml), sulphuric acid liquid merges, adding strong ammonia solution adjusts pH value to 9-10, add 5 (20ml of chloroform extraction, 20ml, 20ml, 10ml, 10ml), chloroform solution merges, put in water-bath and steam to about 5ml, be added on processed good alkali alumina post (100 orders, 3g, interior through 10-15mm) on, with chloroform 60ml eluting, collect eluent, put evaporate to dryness in water-bath, residue adds ethyl acetate to be made to dissolve, and be quantitatively transferred in 25ml measuring bottle, add ethyl acetate to scale, shake up, microporous filter membrane with 0.45 μ m filters, getting subsequent filtrate both obtained.
algoscopyprecision is drawn above-mentioned two kinds of each 10ul of solution respectively, and injection liquid chromatography is measured, and obtains.
The every 1ml of this product contains Semen Strychni with strychnine (C
21h
22n
2o
2) meter, should be 20 μ g-50 μ g.
[function cures mainly] relaxing muscles and tendons and activating QI and blood in the collateral, blood circulation promoting and blood stasis dispelling, reducing swelling and alleviating pain.For muscles and bones arthralgia and soft tissue, muscle injury, and the pain that causes such as scapulohumeral periarthritis, hyperosteogeny, traumatic injury, chronic strain, prolapse of lumbar intervertebral disc.
Usage and dosage: affected part is smeared in external, every day 2～4 times, pain spot and acupuncture point are smeared and are massaged.
[taboo] (1) medicine for external use is avoided for oral administration, must not be applied to the positions such as eye, mucosa.
(2) wound forbidding.(3) anemia of pregnant woman's forbidding.
[points for attention] this product, should not large area life-time service containing toxicity medicines such as Semen Strychni, Venenum Bufoniss.
[storage] sealing, lucifuge, put shady and cool place.[effect duration] 1.5 years.
Enclose clinical experiment report of the present invention, take ten days as a course for the treatment of;
| Name | Sex | Age | Address | Sick time | Control front symptom | With this medicine treatment time | Curative effect |
| Poplar | Female | 27 years old | Shenyang-Dalian | 2006.10 | Scapulohumeral periarthritis | 2 courses for the treatment of | Recovery from illness |
| Jiang Mei | Female | 33 years old | Yingkou, Shenyang | 2007.10 | Hyperosteogeny | 4 courses for the treatment of | Recovery from illness |
| Li Yusong | Man | 26 years old | Tonghua, Jilin Province | 2004.5 | Traumatic injury | 2 courses for the treatment of | Recovery from illness |
| Pan | Man | 25 years old | Liaoyuan | 2003.8 | Traumatic injury | 2 courses for the treatment of | Recovery from illness |
| Wang Yunqian | Female | 45 years old | Su County, Anhui | 2003.8 | Chronic strain | 4 courses for the treatment of | Recovery from illness |
| Qu little Juan | Female | 40 years old | Zhengzhou, henan | 2004.10 | Chronic strain | 4 courses for the treatment of | Recovery from illness |
| Chen Qingqing | Female | 29 years old | Qingdao | 2006.12 | It is outstanding that waist pushes away intercalated disc | 3 courses for the treatment of | Recovery from illness |
| Liu Zehua | Man | 40 years old | Siping | 2005.3 | Muscle injury | 3 courses for the treatment of | Recovery from illness |
| Yang Zhiyong | Man | 43 years old | Xuchang, Henan | 2005.4 | Muscle injury | 2 courses for the treatment of | Recovery from illness |
| Zhang Mingtao | Man | 35 years old | Hua County, Guangdong | 2006.3 | Scapulohumeral periarthritis | 2 courses for the treatment of | Recovery from illness |
| Yan Haoyi | Man | 39 years old | Yichang | 2007.1 | Arthralgia | 2 courses for the treatment of | Recovery from illness |
| Business | Female | 25 years old | From Anshun of Guizhou | 2008.5 | Soft tissue injury | 3 courses for the treatment of | Recovery from illness |
| Chen Jianping | Man | 38 years old | Shangxian county, Shaanxi | 2005.10 | Arthralgia | 1 course for the treatment of | Recovery from illness |
| Luo Shangyu | Man | 29 years old | District of Nanzheng, Shaanxi | 2007.12 | Arthralgia | 4 courses for the treatment of | Recovery from illness |
| Wang Jingye | Man | 46 years old | Beihai Fisheries Base Guangxi Province | 2005.3 | It is outstanding that waist pushes away intercalated disc | 4 courses for the treatment of | Recovery from illness |
| Zhao Zhonghui | Man | 56 years old | Xi'an | 2003.4 | Arthralgia | 2 courses for the treatment of | Recovery from illness |
| Hao Zongxiao | Man | 42 | Xi'an | 2003.11 | The long bleb of the palm of the hand | 1 course for the treatment of | Recovery from illness |
| Wang Guanchao | Man | 18 | Yan-an | 2004.2 | Extremity pain | 4 courses for the treatment of | Recovery from illness |
known by above analysis, drug effect of the present invention is outstanding, has the splendid effect of curing the disease.
more than show and described ultimate principle of the present invention, principal character and advantage of the present invention.Those skilled in the art should understand the present invention and not be restricted to the described embodiments; that in above-described embodiment and description, describes just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in claimed scope.
Claims (3)
1. a Chinese medicine preparation for the treatment of muscles and bones arthralgia and soft tissue injury, is characterized in that, its raw material by following components by weight percent is prepared from: Venenum Bufonis 1-5 part; Semen Strychni 10-15 part; Herba Asari 20-60 part; Pericarpium Zanthoxyli 20-60 part; Fructus Evodiae 12-25 part; Radix Aconiti Kusnezoffii 12-25 part; Semen Sinapis Albae 12-25 part; Fructus Gleditsiae Abnormalis 12-20 part; Radix Notoginseng 12-20 part; Camphora 15-26 part; Rhizoma Zingiberis 10-15 part; Fructus Piperis 10-15 part; Mentholum 2-8 part; Radix aconiti szechenyiani 10-15 part; Daphne giraldii Nitsche 12-15 part; Flos Caryophylli 12-15 part; Fructus Gardeniae 12-15 part; Rhizoma Alpiniae Officinarum 12-15 part.
2. a kind of Chinese medicine preparation for the treatment of muscles and bones arthralgia and soft tissue injury as claimed in claim 1, is characterized in that, its raw material by following components by weight percent is prepared from: 2.7 parts of Venenum Bufoniss; 13.3 parts of Semen Strychni; 41.4 parts of Herba Asaris; 41.4 parts, Pericarpium Zanthoxyli; 13.8 parts of Fructus Evodiaes; 13.8 parts of Radix Aconiti Kusnezoffii; 13.8 parts of Semen Sinapis Albaes; 13.8 parts of Fructus Gleditsiae Abnormalis; 13.8 parts of Radix Notoginseng; 20.7 parts of Camphoras; 13.8 parts of Rhizoma Zingiberiss; 13.8 parts, Fructus Piperis; 6.9 parts of Mentholums; 13.8 parts of Radix aconiti szechenyiani; 13.8 parts of Daphne giraldii Nitsche; 13.8 parts of Flos Caryophyllis; 13.8 parts of Fructus Gardeniaes; 13.8 parts of Rhizoma Alpiniae Officinarums.
3. the method for the preparation of preparation as described in claim 1 or 2, is characterized in that, comprises following steps:
Powder process: Venenum Bufonis is ground into fine powder, crosses 100 mesh sieves; Semen Strychni, Flos Caryophylli, Pericarpium Zanthoxyli, Fructus Piperis, Rhizoma Zingiberis, Rhizoma Alpiniae Officinarum, Semen Sinapis Albae, Herba Asari are ground into coarse powder, cross 60 mesh sieves;
Extraction: add 80% alcohol reflux three times, each 3 hours, medicinal residues were standby;
Preliminary mixing: merge extractive liquid,, filter, Camphora, Mentholum are added in filtrate and mixed, stir, standby;
Second extraction: Fructus Evodiae, Radix Aconiti Kusnezoffii, Fructus Gleditsiae Abnormalis, Radix Notoginseng, Fructus Piperis, Radix aconiti szechenyiani, Daphne giraldii Nitsche, Fructus Gardeniae medicament disintegrating are become to powder, mix with above-mentioned medicinal residues, add 60% ethanol, reflux secondary, each 1 hour;
Produce: merge extractive liquid,, filter, Venenum Bufonis powder is added in filtrate, mix, standing, filter, filtrate and above-mentioned ethanol extract merge, and adjusting concentration of alcohol is 55%, obtains.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210337783.3A CN103656553A (en) | 2012-09-13 | 2012-09-13 | Traditional Chinese medicine preparation for treating arthralgia of bones and joints and soft tissue injuries and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210337783.3A CN103656553A (en) | 2012-09-13 | 2012-09-13 | Traditional Chinese medicine preparation for treating arthralgia of bones and joints and soft tissue injuries and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105535921A (en) * | 2016-03-03 | 2016-05-04 | 姜爱民 | Tendon setting and soft tissue injury healing plaster |
| CN105770847A (en) * | 2016-05-18 | 2016-07-20 | 程敬轩 | Traditional Chinese medicine composition for relieving or treating joint swelling and pain and preparation method and application of traditional Chinese medicine composition |
| CN106267080A (en) * | 2016-08-31 | 2017-01-04 | 唐秀宗 | For Chinese herbal medicine sticking acupuncture point and preparation method thereof, using method |
-
2012
- 2012-09-13 CN CN201210337783.3A patent/CN103656553A/en active Pending
Non-Patent Citations (1)
| Title |
|---|
| 一叶沙寒: "蟾马正痛酊", 《HTTP://BAIKE.BAIDU.COM/HISTORY/13636904》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105535921A (en) * | 2016-03-03 | 2016-05-04 | 姜爱民 | Tendon setting and soft tissue injury healing plaster |
| CN105770847A (en) * | 2016-05-18 | 2016-07-20 | 程敬轩 | Traditional Chinese medicine composition for relieving or treating joint swelling and pain and preparation method and application of traditional Chinese medicine composition |
| CN106267080A (en) * | 2016-08-31 | 2017-01-04 | 唐秀宗 | For Chinese herbal medicine sticking acupuncture point and preparation method thereof, using method |
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Application publication date: 20140326 |