CN103616264B - A kind of device that manually traps gas gas-phase objects in main flume by mouth solvent - Google Patents
A kind of device that manually traps gas gas-phase objects in main flume by mouth solvent Download PDFInfo
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- CN103616264B CN103616264B CN201310660635.XA CN201310660635A CN103616264B CN 103616264 B CN103616264 B CN 103616264B CN 201310660635 A CN201310660635 A CN 201310660635A CN 103616264 B CN103616264 B CN 103616264B
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Abstract
The invention discloses a kind ofly manually by the device of gas gas-phase objects in mouth solvent trapping main flume, comprise the tracheae with the cigarette clamper of cambridge filter, smoking machine suction source, solvent trapping bottle, the above-mentioned parts of manual three-way valve and UNICOM; Wherein, solvent trapping bottle connects respectively manual three-way valve, after manual three-way valve series connection, is connected with smoking machine suction source, after the parallel connection of solvent trapping bottle, is connected with cigarette clamper, realizes the control to suction airstream direction by manual control triple valve. Device of the present invention can, manually by the chemical composition in mouth solvent trapping main flume gas phase, be analyzed different gaseous substances by selecting different solution to trap, and is beneficial to the character of analysis of cigarette flue gas. This apparatus structure is simple, easy to use, is applicable to straight line smoking machine, applies this device and is conducive to analyze the gas gas-phase objects in main flume by mouth, for the character of analysing in depth cigarette mainstream flue gas provides technical support.
Description
Technical field
The present invention relates to production of cigarettes technical field, be specifically related to one manually by mouth solvent trapping main flumeThe device of middle gas gas-phase objects.
Background technology
Cigarette smoke is a kind of very complicated body thing, has therefrom identified at present several thousand kinds of materials. ForResearch convenient, people adopt cambridge filter that flue gas is divided into granule phase substance matter and gaseous substance two parts, whereinUnder room temperature condition, can be called as gaseous substance by the flue gas partial of cambridge filter, can be cut by cambridge filterThe part of getting is called as granule phase substance matter. The proportion of the shared amount of flue gas emission of gaseous substance, up to 92%, mainly contains nitrogenGas, oxygen, carbon dioxide, carbon monoxide and hydrogen, comprise in addition volatile hydrocarbon, ester class, furans,Nitrile, aldehyde ketone, alcohols etc.; Granule phase substance matter account for amount of flue gas emission less than 8%, mainly by water, nicotineForm with tar. Complicated cigarette smoke composition has produced direct impact to the mouthfeel of cigarette, makes inhomogeneityThe cigarette of type produces different mouthfeels. In fact in cigarette smoking process, the composition of every mouthful of cigarette smoke alsoVariantly cause the each mouthful of difference in mouthfeel. Therefore, more next by mouth analysis of cigarette main flume in recent yearsMore come into one's own, but gas gas-phase objects few by mouth analysis in relevant main flume.
CN102192950A has invented a kind of online capturing device in real time of components in cigarette smoke gas phase chemical composition,This disclosure of the invention a kind of components in cigarette smoke gas phase chemical composition on-line analysis device, it is characterized in that at smoking machineFlue gas transmission quartz capillary is set between suction cylinder and on-line analysis mass spectrograph, can realizes single port cigaretteFlue gas gas phase composition carries out online, automatically and continuously analyzes. But this invention is in can only real-time analysis gas phaseSome chemical properties can not trap the composition in gas phase, so quantitative analysis main flume gas phase exactlyMiddle chemical composition is also analysed in depth. In addition, this invention still exists in the time analyzing gas chemistry compositionWeak point, so for example this invention judges that by mass-to-charge ratio the chemical composition in gas phase can not accurate analysis gasA same point allosome mutually. CN201145652Y discloses a kind of cigarette successive suction trapping device, but thisBright can only trapping fixed certain a bite cigarette mainstream flue gas grain phase constituent or grain and the mixture of gas phase, can notTrap same gas gas-phase objects in the every a bite flue gas of cigarette simultaneously.
Summary of the invention
The technical problem to be solved in the present invention is to provide one manually by gas phase in mouth solvent trapping main flumeThe device of thing, this apparatus structure is simple, easy to use, is applicable to straight line smoking machine, applies this device favourableIn analyzing the gas gas-phase objects in main flume by mouth, for the character of analysing in depth cigarette mainstream flue gas provides technology to prop upHold. In view of the puff number of most of cigarette is all in 9 mouthfuls, this device is applicable to analyze pump orifice by mouthThe cigarette of number in 9 mouthfuls.
For solving the problems of the technologies described above, the present invention adopts following technical proposals:
Manually, by a device for gas gas-phase objects in mouth solvent trapping main flume, comprise the volume with cambridge filterThe tracheae of cigarette clamper, smoking machine suction source, solvent trapping bottle, the above-mentioned parts of manual three-way valve and UNICOM;Wherein, solvent trapping bottle connects respectively manual three-way valve, and above-mentioned manual three-way valve is connected afterwards and smoking machine suctionSource connects, and after the parallel connection of solvent trapping bottle, is connected with cigarette clamper, realizes taking out by manual control triple valveThe control of inspiratory flow direction. When each triple valve does not rotate, the gas of suction source, solvent trapping bottle and each triple valveRoad is in the state of being interconnected.
Preferably, when work, the granule phase substance of the clamper trapping main flume of cambridge filter is housed, manual threeLogical valve is for control and suck airflow direction, in the time of suction conversion by controlling manual three-way valve combined controllerButton makes the gas gas-phase objects of every a bite flue gas by different absorption bottles, thereby realizes manually main by the trapping of mouth solventStream flue gas gas gas-phase objects.
Beneficial effect of the present invention:
Device of the present invention can be manually by the chemical composition in mouth solvent trapping main flume gas phase, by choosingSelect solution of different nature and can trap different gaseous substances such as analyzing ammonia, HCN, oxynitrides, withBe beneficial to the character of analysis of cigarette flue gas. This apparatus structure is simple, easy to use, is applicable to straight line smoking machine,Apply this device and be conducive to analyze the gas gas-phase objects in main flume by mouth, for analysing in depth cigarette mainstream flue gasCharacter provides technical support.
Brief description of the drawings
Fig. 1 is structural representation of the present invention.
Detailed description of the invention
For understanding better the present invention, will further illustrate side of the present invention by specific embodiment belowCase, protection scope of the present invention should comprise the full content of claim, but is not limited to this.
Embodiment 1
As shown in the figure, a kind of manually by the device of gas gas-phase objects in mouth solvent trapping main flume, comprise with swordThe cigarette clamper 1 of bridge filter disc, smoking machine suction source 2, solvent trapping bottle 31,32,33,34,35,36,37,38,39, manual three-way valve 41,42,43,44,45,46,47,48; Wherein, solventTrapping bottle 31,32,33,34,35,36,37,38 connect respectively manual three-way valve 41,42,43,44,45,46,47,48, solvent trapping bottle 39 is connected with manual three-way valve 48, above-mentioned manual three-way valveAfter series connection, is connected with smoking machine suction source 2, solvent trapping bottle 31,32,33,34,35,36,37,38,After 39 parallel connections, be connected with cigarette clamper 1, realize the control to suction airstream direction by manual control triple valveSystem.
Before experiment starts as shown in the figure, in each trapping bottle, pack 20ml10mmol/LHCL into by mouthAmmonia in trapping main flume gas gas-phase objects. When before the 1st mouthful of flue gas of this device work suction, rotate triple valve 41Make gas circuit be switched to the 1st trapping bottle 31, collect the gaseous substance of the 1st mouthful of flue gas, other threeway is in mutuallyState is connected; Gas circuit is switched to triple valve 42 directions by the 1st mouthful of complete rotation triple valve 41 of suction, turnsMoving triple valve 42 makes gas circuit be switched to the 2nd trapping bottle direction, collects the gaseous substance of the 2nd mouthful of flue gas;Complete when the 2nd mouthful of suction, rotate triple valve 42 switching gas circuits to triple valve 43 directions, rotate triple valve 43Be switched to the 3rd trapping bottle direction, collect the gaseous substance of the 3rd mouthful of flue gas, the rest may be inferred to being drawn intoThe 9th mouthful time, suction source, triple valve 41,42,43,44,45,46,47,48 and solvent trapping bottle39 in interconnecting state, and the gas gas-phase objects of the 9th mouthful of flue gas is absorbed by solvent trapping bottle 39.Application said apparatus record certain cigarette by implication the ammonia content result in mutually as table 1
Certain cigarette of table 1 is the ammonia content (ng/cig) in mutually by implication
| Mouth number | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 |
| Ammonia content | 35 | 40 | 46 | 52 | 57 | 62 | 68 | 75 | 86 |
Obviously, the above embodiment of the present invention is only for example of the present invention is clearly described, and alsoNon-is restriction to embodiments of the present invention. For those of ordinary skill in the field, above-mentionedOn the basis illustrating, can also make other changes in different forms. Here cannot be to all enforcementMode gives exhaustive. Everyly belong to apparent variation or the variation that technical scheme of the present invention is extended outThe still row in protection scope of the present invention.
Claims (1)
1. manually by a device for gas gas-phase objects in mouth solvent trapping main flume, it is characterized in that: described inDevice comprises with the cigarette clamper (1) of cambridge filter, smoking machine suction source (2), solvent trapping bottle(31), (32), (33), (34), (35), (36), (37), (38), (39), manual three-way valve (41),(42), (43), (44), (45), (46), (47, the tracheae (6) of the above-mentioned parts in (48) and UNICOM;Wherein, solvent trapping bottle (31), (32), (33), (34), (35), (36), (37), (38) pointDo not connect manual three-way valve (41), (42), (43), (44), (45), (46), (47), (48), moltenAgent trapping bottle (39) is connected with manual three-way valve (48), and above-mentioned manual three-way valve is connected afterwards and smoking machineSuction source (2) connects, solvent trapping bottle (31), (32), (33), (34), (35), (36), (37),(38), (39) be connected with cigarette clamper (1) after in parallel, realize taking out by manual control triple valveThe control of inspiratory flow direction; When each triple valve does not rotate, suction source, solvent trapping bottle (39) and each threeThe gas circuit of logical valve is in the state of being interconnected.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310660635.XA CN103616264B (en) | 2013-12-06 | 2013-12-06 | A kind of device that manually traps gas gas-phase objects in main flume by mouth solvent |
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| CN201310660635.XA CN103616264B (en) | 2013-12-06 | 2013-12-06 | A kind of device that manually traps gas gas-phase objects in main flume by mouth solvent |
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| CN103616264A CN103616264A (en) | 2014-03-05 |
| CN103616264B true CN103616264B (en) | 2016-05-25 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104020019A (en) * | 2014-06-05 | 2014-09-03 | 上海大学 | Portable automatic collecting device of volatile organic compounds in atmosphere |
| CN104931303A (en) * | 2015-03-27 | 2015-09-23 | 北京京能电力股份有限公司石景山热电厂 | Sampling device and sampling method for detecting ammonia escaping concentration of smoke denitration |
| CN110988188B (en) * | 2019-12-23 | 2022-12-23 | 江苏中烟工业有限责任公司 | Method for detecting ammonia content in particulate matters of main stream smoke of cigarettes |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4019366A (en) * | 1975-11-04 | 1977-04-26 | Philip Morris Incorporated | Variable parameter smoking machine |
| JPS60227146A (en) * | 1984-04-26 | 1985-11-12 | Mitsubishi Heavy Ind Ltd | Testing device for smoke diffusion model |
| CN1888848A (en) * | 2006-08-01 | 2007-01-03 | 中国烟草总公司郑州烟草研究院 | Smoke suction device capable of realizing single-port main flow smoke continuous collecting |
| CN201145652Y (en) * | 2007-12-11 | 2008-11-05 | 中国烟草总公司郑州烟草研究院 | Cigarette successive suction trapping device |
| CN101324491A (en) * | 2008-08-04 | 2008-12-17 | 中国烟草总公司郑州烟草研究院 | Smoking apparatus capable of implementing continuous one-time sampling of main fume gas phase object |
| CN102192950A (en) * | 2011-03-11 | 2011-09-21 | 安徽中烟工业公司 | Device for analyzing gas phase chemical components of cigarette smoke on line |
| CN102928544A (en) * | 2012-11-03 | 2013-02-13 | 中国烟草总公司郑州烟草研究院 | Method for analyzing ammonia in cigarette mainstream smoke through gas chromatography-mass spectrometry |
| WO2013060829A2 (en) * | 2011-10-28 | 2013-05-02 | Philip Morris Products S.A. | On-line system and method for nicotine analysis of a smoking article |
| CN103196736A (en) * | 2013-04-16 | 2013-07-10 | 江苏中烟工业有限责任公司 | Puff-by-puff measuring method for carbon monoxide in main stream smoke of cigarette and special device thereof |
| CN103383384A (en) * | 2013-07-04 | 2013-11-06 | 湖南中烟工业有限责任公司 | Atmosphere controllable smoking device |
| CN203587403U (en) * | 2013-12-06 | 2014-05-07 | 江苏中烟工业有限责任公司 | Device for trapping gas-phase substances in main stream smoke in manual port-by-port solvent mode |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0227715D0 (en) * | 2002-11-28 | 2003-01-08 | British American Tobacco Co | Smoking behaviour analyser |
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Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4019366A (en) * | 1975-11-04 | 1977-04-26 | Philip Morris Incorporated | Variable parameter smoking machine |
| JPS60227146A (en) * | 1984-04-26 | 1985-11-12 | Mitsubishi Heavy Ind Ltd | Testing device for smoke diffusion model |
| CN1888848A (en) * | 2006-08-01 | 2007-01-03 | 中国烟草总公司郑州烟草研究院 | Smoke suction device capable of realizing single-port main flow smoke continuous collecting |
| CN201145652Y (en) * | 2007-12-11 | 2008-11-05 | 中国烟草总公司郑州烟草研究院 | Cigarette successive suction trapping device |
| CN101324491A (en) * | 2008-08-04 | 2008-12-17 | 中国烟草总公司郑州烟草研究院 | Smoking apparatus capable of implementing continuous one-time sampling of main fume gas phase object |
| CN102192950A (en) * | 2011-03-11 | 2011-09-21 | 安徽中烟工业公司 | Device for analyzing gas phase chemical components of cigarette smoke on line |
| WO2013060829A2 (en) * | 2011-10-28 | 2013-05-02 | Philip Morris Products S.A. | On-line system and method for nicotine analysis of a smoking article |
| CN102928544A (en) * | 2012-11-03 | 2013-02-13 | 中国烟草总公司郑州烟草研究院 | Method for analyzing ammonia in cigarette mainstream smoke through gas chromatography-mass spectrometry |
| CN103196736A (en) * | 2013-04-16 | 2013-07-10 | 江苏中烟工业有限责任公司 | Puff-by-puff measuring method for carbon monoxide in main stream smoke of cigarette and special device thereof |
| CN103383384A (en) * | 2013-07-04 | 2013-11-06 | 湖南中烟工业有限责任公司 | Atmosphere controllable smoking device |
| CN203587403U (en) * | 2013-12-06 | 2014-05-07 | 江苏中烟工业有限责任公司 | Device for trapping gas-phase substances in main stream smoke in manual port-by-port solvent mode |
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