CN103586175A - Electrostatic coating method for polyether-ether-ketone powder - Google Patents
Electrostatic coating method for polyether-ether-ketone powder Download PDFInfo
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- CN103586175A CN103586175A CN201310602468.3A CN201310602468A CN103586175A CN 103586175 A CN103586175 A CN 103586175A CN 201310602468 A CN201310602468 A CN 201310602468A CN 103586175 A CN103586175 A CN 103586175A
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Abstract
The invention discloses an electrostatic coating method for polyether-ether-ketone powder. According to the electrostatic coating method for the polyether-ether-ketone powder, an electrostatic spraying device is adopted, physical and chemical coating particles take negative charges in a high-voltage direct-current electric field and flow to a workpiece surface with positive charges directionally under the action of an electrostatic field, and a layer of even and firm thin film is formed by neutralizing and deposition. The electrostatic coating method for the polyether-ether-ketone powder achieves good film coating performance, lowers the degree of pollution to the environment, saves coating materials, enables a coating process to be mechanical and continuous, reduces the rejection rate, improves labor productivity, improves working conditions, thereby obtaining considerable social and economic benefits.
Description
Technical field
The invention belongs to a kind of electrostatic coating method of surface powder application, relate to specifically a kind of electrostatic coating method for polyether-ether-ketone powder.
Background technology
Special engineering plastics polyether-ether-ketone (polyether ether ketone, be called for short PEEK resin) be successfully a kind of novel semi-crystalline state aromatic thermoplastic engineering plastics of late 1970s Britain Victrex company research and development, compare with other special engineering plastics, it has high temperature resistant, the advantage such as mechanical performance is excellent, self lubricity good, easy processing.
Crank axle and linkage in the needle bearing that engine uses, be intended to reduce two frictions between surface of revolution, thereby avoid outer surface to be subject to extreme wear.And remarkable wearability and the durability of PEEK can be born this extreme applications condition.The roller that industry textile production is used must bear high temperature and eroding chemical and abrasive condition, and the roller comparable common cylinder in service life that scribbles PEEK coating improves 4 times, and can at the temperature of 260 ℃, use continuously and fabulous chemical resistance.
At present, the spraying goods of polyether-ether-ketone are in the majority with electrostatic spraying and suspension spraying, and electrostatic spraying has lot of advantages, and transmission efficiency is high, saves coating, and spray efficiency can reach 90%; System is simple, by electrostatic generator, electrostatic gun, air compressor, baking box etc.; Easy to use, but electrostatic efficiency spray gun move, thereby be widely used in external coating field.
Yet existing Electrostatic Spray Technology exists that coating adhesion is poor, coating layer thickness is inhomogeneous, the problems such as bubble, pin hole easily appear in coating surface.
Summary of the invention
For solving the above-mentioned problems in the prior art, inventor provides a kind of electrostatic coating method for polyether-ether-ketone powder, and the method adopts electrostatic spraying device, makes the paint particles of materialization in DC high voltage electric field, be with negative electrical charge, and under the effect of electrostatic field, directed stream
To positively charged surface of the work, neutralization deposition one deck evenly, film firmly.
Technical scheme of the present invention is as follows:
For the electrostatic coating method of polyether-ether-ketone powder, adopt electrostatic spraying device, in surface of workpiece spraying PEEK powder, preparation PEEK coating;
Specifically comprise the following steps:
A. surface of workpiece pretreatment
Clean out the jagged sharp edge of surface of workpiece; Remove surperficial greasy dirt, by acid washing phosphorization, at surface of workpiece, generate the phosphate layer that one deck is insoluble in water;
B. the blasting treatment of metal works
Use 60-80 object aluminium oxide to carry out the blasting treatment of surface of the work, sand-blasting machine pressure, at 0.6-0.7MPa, obtains rough surface, blows off the floating sand on surface with air-flow, with acetone clean metal surface of the work, dries;
C. polyether-ether-ketone electrostatic powder spraying
With polyether-ether-ketone powdery paints, metal works is sprayed, should be by blasting treatment or solvent degreasing before coating, to strengthen the bonding force with polymer;
D. spray post processing
The metal works that spraying is reunited after ether ether ketone powder is placed after 3-5min, puts into heating furnace and is warming up to 200-230 ℃, and insulation 30min takes out.
Preferably, in the spraying process of step c, the distance between the metal works in powder spraying chamber should keep 200-300mm; Spray distance general control is apart from metal works 10-25cm; , in the spraying incipient stage amount of dusting, be controlled within the scope of 50g/min-300g/min.
Preferably, what described step c adopted is that electrostatic spraying apparatus sprays in powder spraying chamber, and described electrostatic spraying apparatus comprises electrostatic generator, electrostatic gun and air compressor.Make polyether-ether-ketone powder in DC high voltage electric field, be with negative electrical charge, and under the effect of electrostatic field, directed flow to positively charged surface of workpiece, neutralization deposition one deck evenly, film firmly.
The invention has the beneficial effects as follows:
Adopt said method, can obtain excellent film performance, reduce the pollution level of environment, save coating, and can make spraying coating process mechanization, serialization, minimizing percent defective, raise labour productivity, improve working conditions, thereby obtain considerable economic results in society.
Accompanying drawing explanation
The present invention has accompanying drawing 2 width.
Fig. 1 is the structural representation of electrostatic spraying apparatus;
Fig. 2 is spraying process principle schematic.
In the drawings, 1-electrostatic generator; 2-electrostatic gun; 3-air compressor.
The specific embodiment
Below by specific embodiment, the present invention is further set forth, but do not limit the present invention.
Embodiment 1
Clean out the jagged sharp edge of surface of workpiece; Remove surperficial greasy dirt, by acid washing phosphorization, at surface of workpiece, generate the phosphate layer that one deck is insoluble in water; Use 60 object aluminium oxide to carry out the blasting treatment of surface of the work, sand-blasting machine pressure, at 0.6-0.7MPa, obtains rough surface, blows off the floating sand on surface with air-flow, with acetone clean metal surface of the work, dries; Coating polyether-ether-ketone powder is front by the bonding force of blasting treatment enhancing and polymer; With polyether-ether-ketone powdery paints, metal works is sprayed; The metal works that spraying is reunited after ether ether ketone powder is placed after 3-4min, puts into heating furnace and is warming up to 200 ℃, insulation 25min, then cooling coming out of the stove.The indoor whirligig of rotary spraying during spraying, by workpiece suspension, in powder spraying chamber on rotatable device, the distance between workpiece keeps 250-300mm.Speed spraying in the spraying incipient stage with 100g/min, guarantees that workpiece can be uniformly sprayed.
Clean out the jagged sharp edge of surface of workpiece; Remove surperficial greasy dirt, by acid washing phosphorization, at surface of workpiece, generate the phosphate layer that one deck is insoluble in water; Use 80 object aluminium oxide to carry out the blasting treatment of surface of the work, sand-blasting machine pressure, at 0.6-0.7MPa, obtains rough surface, blows off the floating sand on surface with air-flow, with acetone clean metal surface of the work, dries; Coating polyether-ether-ketone powder is front by the bonding force of blasting treatment enhancing and polymer; With polyether-ether-ketone powdery paints, metal works is sprayed; The metal works that spraying is reunited after ether ether ketone powder is placed after 4-5min, puts into heating furnace and is warming up to 230 ℃, insulation 30min, then cooling coming out of the stove.The indoor whirligig of rotary spraying during spraying, by workpiece suspension, in powder spraying chamber on rotatable device, the distance between workpiece keeps 250-300mm.Speed spraying in the spraying incipient stage with 100g/min, guarantees that workpiece can be uniformly sprayed.
Embodiment properties of product are in Table 1
Table 1
? | Embodiment 1 | |
Outward appearance (bubble, pin hole, drain spray) | Nothing | Nothing |
Coating layer thickness (mm) | 0.3 | 0.6 |
Coating adhesion (MPa) | 3.2 | 4.5 |
。
Claims (3)
1. for the electrostatic coating method of polyether-ether-ketone powder, adopt electrostatic spraying device, in surface of workpiece spraying PEEK powder, preparation PEEK coating;
Specifically comprise the following steps:
A. surface of workpiece pretreatment
Clean out the jagged sharp edge of surface of workpiece; Remove surperficial greasy dirt, by acid washing phosphorization, at surface of workpiece, generate the phosphate layer that one deck is insoluble in water;
B. the blasting treatment of metal works
Use 60-80 object aluminium oxide to carry out the blasting treatment of surface of the work, sand-blasting machine pressure, at 0.6-0.7MPa, obtains rough surface, blows off the floating sand on surface with air-flow, with acetone clean metal surface of the work, dries; Coating polyether-ether-ketone powder is front by the bonding force of blasting treatment enhancing and polymer;
C. polyether-ether-ketone electrostatic powder spraying
With polyether-ether-ketone powdery paints, metal works is sprayed;
D. spray post processing
The metal works that spraying is reunited after ether ether ketone powder is placed after 3-5min, puts into heating furnace and is warming up to 200-230 ℃, and insulation 30min takes out.
2. a kind of electrostatic coating method for polyether-ether-ketone powder according to claim 1, is characterized in that: in the spraying process of step c, the distance between the metal works in powder spraying chamber should keep 200-300mm; Spray distance general control is apart from metal works 10-25cm; , in the spraying incipient stage amount of dusting, be controlled within the scope of 50g/min-300g/min.
3. a kind of electrostatic coating method for polyether-ether-ketone powder according to claim 1, is characterized in that:
What described step c adopted is that electrostatic spraying apparatus sprays in powder spraying chamber, described electrostatic spraying apparatus comprises electrostatic generator (1), electrostatic gun (2) and air compressor (3), make polyether-ether-ketone powder in DC high voltage electric field, be with negative electrical charge, and under the effect of electrostatic field, directed flow to positively charged surface of workpiece, neutralization deposition one deck evenly, film firmly.
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104482026A (en) * | 2014-12-12 | 2015-04-01 | 中国船舶重工集团公司第七二五研究所 | Preservative treatment method of tail vane connecting rod threads |
CN107350138A (en) * | 2017-07-25 | 2017-11-17 | 苏州市鑫渭阀门有限公司 | The preparation method of metal valve surface spraying preservation antioxidation type coating |
CN110123435A (en) * | 2019-04-08 | 2019-08-16 | 上海双申医疗器械股份有限公司 | A kind of rush osteogenesis type polyether-ether-ketone cranium jawbone internal fixation plate and preparation method thereof |
CN111036845A (en) * | 2020-01-06 | 2020-04-21 | 江苏中超航宇精铸科技有限公司 | Liquid-free formwork manufacturing method and system for investment precision casting |
CN114377869A (en) * | 2021-12-31 | 2022-04-22 | 江苏盛安信息科技有限公司 | Ionized film-coating spraying equipment for inner cavity environment of twisted soft robot |
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US20040253387A1 (en) * | 2003-06-06 | 2004-12-16 | Jose Cavero | Non-stick powder coating |
CN102500537A (en) * | 2011-11-18 | 2012-06-20 | 吉林大学 | Preparation method for anticorrosion wear-resistant anti-scaling plunger of oil well pump |
CN102504678A (en) * | 2011-11-18 | 2012-06-20 | 吉林大学 | Protection coating for petroleum equipment and construction method thereof |
CN102698941A (en) * | 2012-06-08 | 2012-10-03 | 中国电子科技集团公司第二十二研究所 | Coating process for electrostatic spraying of polyether-ether-ketone powder on surfaces of drill collar threads |
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2013
- 2013-11-25 CN CN201310602468.3A patent/CN103586175A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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US20040253387A1 (en) * | 2003-06-06 | 2004-12-16 | Jose Cavero | Non-stick powder coating |
CN102500537A (en) * | 2011-11-18 | 2012-06-20 | 吉林大学 | Preparation method for anticorrosion wear-resistant anti-scaling plunger of oil well pump |
CN102504678A (en) * | 2011-11-18 | 2012-06-20 | 吉林大学 | Protection coating for petroleum equipment and construction method thereof |
CN102698941A (en) * | 2012-06-08 | 2012-10-03 | 中国电子科技集团公司第二十二研究所 | Coating process for electrostatic spraying of polyether-ether-ketone powder on surfaces of drill collar threads |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104482026A (en) * | 2014-12-12 | 2015-04-01 | 中国船舶重工集团公司第七二五研究所 | Preservative treatment method of tail vane connecting rod threads |
CN104482026B (en) * | 2014-12-12 | 2016-06-29 | 中国船舶重工集团公司第七二五研究所 | A kind of method for anticorrosion treatment of tail vane connecting rod screw thread |
CN107350138A (en) * | 2017-07-25 | 2017-11-17 | 苏州市鑫渭阀门有限公司 | The preparation method of metal valve surface spraying preservation antioxidation type coating |
CN110123435A (en) * | 2019-04-08 | 2019-08-16 | 上海双申医疗器械股份有限公司 | A kind of rush osteogenesis type polyether-ether-ketone cranium jawbone internal fixation plate and preparation method thereof |
CN111036845A (en) * | 2020-01-06 | 2020-04-21 | 江苏中超航宇精铸科技有限公司 | Liquid-free formwork manufacturing method and system for investment precision casting |
CN111036845B (en) * | 2020-01-06 | 2023-09-29 | 江苏中超航宇精铸科技有限公司 | Method and system for manufacturing liquid-free shuttering for investment precision casting |
CN114377869A (en) * | 2021-12-31 | 2022-04-22 | 江苏盛安信息科技有限公司 | Ionized film-coating spraying equipment for inner cavity environment of twisted soft robot |
CN114377869B (en) * | 2021-12-31 | 2022-12-20 | 江苏盛安信息科技有限公司 | Ionized film-coating spraying equipment for inner cavity environment of twisted soft robot |
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Application publication date: 20140219 |