CN103585944A - Subminiature magnetic-stirring photocatalytic reaction kettle - Google Patents
Subminiature magnetic-stirring photocatalytic reaction kettle Download PDFInfo
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- CN103585944A CN103585944A CN201310480937.9A CN201310480937A CN103585944A CN 103585944 A CN103585944 A CN 103585944A CN 201310480937 A CN201310480937 A CN 201310480937A CN 103585944 A CN103585944 A CN 103585944A
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- magnetic
- kettle
- quartz glass
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- photocatalytic reaction
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Abstract
The invention relates to a subminiature magnetic-stirring photocatalytic reaction kettle which comprises a kettle body, a magnetic transmission stirring device and a heat transmission coiled pipe and is characterized in that the bottom of the kettle body is quartz glass; flanges and studs are arranged at two ends of the outer side of the bottom of the kettle body; metal pads are arranged on the sealed surfaces of the flanges; O-shaped rings are arranged on the two end parts of the quartz glass through grooves. The subminiature magnetic-stirring photocatalytic reaction kettle disclosed by the invention is high in light transmittance due to the quartz glass of the kettle body and can generate photocatalytic reaction; by adopting the two sealing forms of the metal pads and the O-shaped rings, the subminiature magnetic-stirring photocatalytic reaction kettle can bear high pressure and has enough sealing force, and the sealing effect is guaranteed.
Description
Technical field
The present invention relates to a kind of reactor, particularly a kind of microminiature magnetic agitation light-catalyzed reaction still.
Background technology
At present, because a kind of volume of equipment of experiment demand is 200ml, in course of reaction, liquids and gases add reactor simultaneously, in coiled pipe, by vapours, carry out preheating, starting agitating device stirs and makes it abundant mixing material, at the outside ultraviolet light source that starts of reaction kettle body, seeing through kettle carries out light-catalysed material and reacts and manufacture a finished product, in whole course of reaction, temperature can reach 200 ℃, during reacting balance, can produce a small amount of granule, after having reacted, in coiled pipe, passing into cooling water carries out cooling to material, and release kettle internal pressure by writing pressure relief opening, by boost port, carry out supercharging, the magnetic agitation light-catalyzed reaction still sampling from sample tap.
Summary of the invention
The present invention aims to provide a kind of microminiature magnetic agitation light-catalyzed reaction still for above-mentioned requirement of experiment.
Microminiature magnetic agitation light-catalyzed reaction still of the present invention, comprise kettle, magnetic transmission stirring device, heat transfer coils, characterized by further comprising in the bottom of kettle and be set to quartz glass, two ends in the bottom outside of kettle are provided with flange and studs, on the front cover of flange, metallic gasket is set, the two-end part of quartz glass is provided with O shape circle.
Preferably, microminiature magnetic agitation light-catalyzed reaction still of the present invention, wherein said magnetic transmission stirring device is comprised of motor, driving-belt, magnetic coupling and agitator, wherein the output shaft of motor is connected with the outer rotor of magnetic coupling by conveyer belt, agitator is connected with the interior magnet rotor of magnetic coupling, inside and outside turn between non-magnetic sealed cylinder separation sleeve is installed.
Preferably, microminiature magnetic agitation light-catalyzed reaction still of the present invention, wherein blind flange is provided with groove, and quartz glass is arranged in the groove on blind flange.
More preferably, microminiature magnetic agitation light-catalyzed reaction still of the present invention, wherein said heat transfer coils is designed to U-shaped.
Microminiature magnetic agitation light-catalyzed reaction still of the present invention, the light transmission that quartz glass by kettle has had is carried out light-catalyzed reaction, and adopt metallic gasket and two kinds of seal form of O type circle, effectively met and can either bear outside larger pressure-bearing, also there is enough sealing forces and guaranteed its sealing effectiveness.
Accompanying drawing explanation
Fig. 1 is the microminiature magnetic agitation light-catalyzed reaction still structure chart in embodiment 1.
1-driving-belt; 2-magnetic transmission stirring device; 3-shaft; 4-heat transfer coils; 5-kettle; 6-quartz glass.
The specific embodiment
The present invention relates to a kind of microminiature magnetic agitation light-catalyzed reaction still, comprise magnetic transmission stirring device, shaft, transmission coil pipe and kettle, wherein the bottom of kettle is set to quartz glass, two ends in the bottom outside of kettle are provided with flange and studs, on the front cover of flange, metallic gasket is set, two-end part at quartz glass is provided with O shape circle, simultaneously, blind flange is provided with groove, when quartz glass is arranged on and prevents from back-outing bolt in the groove on blind flange, quartz glass drops, wherein magnetic transmission stirring device is by motor, driving-belt, magnetic coupling and agitator form, wherein the output shaft of motor is connected with the outer rotor of magnetic coupling by conveyer belt, agitator is connected with the interior magnet rotor of magnetic coupling, inside and outside turn between non-magnetic sealed cylinder separation sleeve is installed, realized the static seal of the sealing surface of joint face, reach a junction honeybee volume little, whole leak free object, transmission coil pipe is designed to not only good effect of heat exchange but also reduced manufacture difficulty of U-shaped, while inlet, boost port, sample tap, side pressure mouth, temperature-measuring port, pressure relief opening, the import and export of coil pipe are changed with magnetic transmission stirring device and are all arranged on kettle room temperature top, in the situation that not affecting use, a mouthful welding bend pipe is taken in its top, get out of the way space and connect again instrument, or part of interface is arranged on to the side outer of flange.
Claims (4)
1. a magnetic agitation light-catalyzed reaction still, comprise kettle, magnetic transmission stirring device, heat transfer coils, characterized by further comprising in the bottom of kettle and be set to quartz glass, two ends in the bottom outside of kettle are provided with flange and studs, on the front cover of flange, metallic gasket is set, groove is provided with O shape circle at the two-end part of quartz glass.
2. magnetic agitation light-catalyzed reaction still according to claim 1, it is characterized in that wherein said magnetic transmission stirring device is comprised of motor, driving-belt, magnetic coupling and agitator, wherein the output shaft of motor is connected with the outer rotor of magnetic coupling by conveyer belt, agitator is connected with the interior magnet rotor of magnetic coupling, inside and outside turn between non-magnetic sealed cylinder separation sleeve is installed.
3. magnetic agitation light-catalyzed reaction still according to claim 1 and 2, is characterized in that blind flange is wherein provided with groove, and quartz glass is arranged in the groove on blind flange.
4. magnetic agitation light-catalyzed reaction still according to claim 1 and 2, is characterized in that heat transfer coils is designed to U-shaped.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310480937.9A CN103585944A (en) | 2013-10-15 | 2013-10-15 | Subminiature magnetic-stirring photocatalytic reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310480937.9A CN103585944A (en) | 2013-10-15 | 2013-10-15 | Subminiature magnetic-stirring photocatalytic reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103585944A true CN103585944A (en) | 2014-02-19 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310480937.9A Pending CN103585944A (en) | 2013-10-15 | 2013-10-15 | Subminiature magnetic-stirring photocatalytic reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103585944A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104785186A (en) * | 2015-04-16 | 2015-07-22 | 内蒙古师范大学 | Photocatalytic reaction device for magnetic stirring |
| CN110314628A (en) * | 2019-06-14 | 2019-10-11 | 西安交通大学 | A kind of side illuminated reactor decomposing aquatic products hydrogen for studying photo-thermal coupling and catalyzing |
-
2013
- 2013-10-15 CN CN201310480937.9A patent/CN103585944A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104785186A (en) * | 2015-04-16 | 2015-07-22 | 内蒙古师范大学 | Photocatalytic reaction device for magnetic stirring |
| CN104785186B (en) * | 2015-04-16 | 2016-06-01 | 内蒙古师范大学 | A kind of magnetic agitation photocatalytic reaction device |
| CN110314628A (en) * | 2019-06-14 | 2019-10-11 | 西安交通大学 | A kind of side illuminated reactor decomposing aquatic products hydrogen for studying photo-thermal coupling and catalyzing |
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| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20140219 |
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| WD01 | Invention patent application deemed withdrawn after publication |