CN103484192A - High-weather-resistance anti-rust oil - Google Patents
High-weather-resistance anti-rust oil Download PDFInfo
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- CN103484192A CN103484192A CN201310361700.9A CN201310361700A CN103484192A CN 103484192 A CN103484192 A CN 103484192A CN 201310361700 A CN201310361700 A CN 201310361700A CN 103484192 A CN103484192 A CN 103484192A
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- oil
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- coalescence aid
- film coalescence
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- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a high-weather-resistance anti-rust oil which is prepared from the following raw materials in parts by weight: 70-75 parts of 75SN base oil, 3-5 parts of calcium dinonylnaphthalene sulfonate, 2-3 parts of lanolin magnesium soap, 1-2 parts of citric acid, 1-2 parts of N-oleoylsarcosine octadecylamine salt, 2-3 parts of sulfurized fatty acid ester, 1-2 parts of 2-aminoethylheptadecenylimidazoline, 2-3 parts of film-forming assistant and 0.1-0.3 part of beta-(3,5-ditert-butyl-4-hydroxyphenyl)propionic acid n-octadecanol ester. The anti-rust oil disclosed by the invention has the advantages of high aging resistance, high corrosion resistance, stable coated film, favorable spreadability on the workpiece surface, favorable protective action on the metal workpiece, and high weather resistance; and the coated film can not be easily damaged under natural conditions.
Description
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Technical field
The present invention relates generally to a kind of rust-preventive agent, relates in particular to a kind of high weather resisteant slushing oil.
Background technology
It is antirust that rust-preventive agent is mainly used in the metalwork surface, very eurypalynous antirust product is arranged at present, the rust-preventive agent be prepared from such as components such as general employing solvent slushing oil or Sodium Nitrite water, film forming material pitch and petroleum resin, but certain defect is also arranged, such as rate of drying is slow, paint film is unstable etc., and it is necessary therefore by reasonably combined new various raw materials, preparing more high performance rust-preventive agent.
Summary of the invention
The object of the invention just is to provide a kind of high weather resisteant slushing oil.
The present invention is achieved by the following technical solutions:
A kind of high weather resisteant slushing oil, it is comprised of the raw material of following weight parts:
75SN base oil 70-75, dinonylnaphthalene sulfonic acid calcium 3-5, lanolin magnesium soap 2-3, citric acid 1-2, KORANTIN SH stearylamine salt 1-2, sulfide aliphatic acid ester 2-3,2-aminoethyl 17 alkenyl imidazoline 1-2, film coalescence aid 2-3, the β-positive octadecanol ester of (3,5-di-tert-butyl-hydroxy phenyl) propionic acid 0.1-0.3;
Described film coalescence aid is comprised of the raw material of following weight parts:
Drying oil alkyd resin 30-40, hexamethoxymethyl melamine resin 2-3, Oleum Cinnamomi 1-2, polyvinylpyrrolidone 1-2, N-phenyl-2-naphthylamine 0.1-0.3, Union carbide A-162 0.1-0.2;
Above-mentioned drying oil alkyd resin is mixed with Oleum Cinnamomi, at 90-100 ℃ of lower insulated and stirred 6-8 minute, the reduction temperature is 55-65 ℃, adds the hexamethoxymethyl melamine resin, after fully stirring, adds Union carbide A-162,200-300 rev/min of dispersed with stirring 10-15 minute, the rising temperature is 130-135 ℃, adds each raw material of residue, insulation reaction 1-3 hour, be cooled to normal temperature, obtain described film coalescence aid.
A kind of preparation method of high weather resisteant slushing oil comprises the following steps:
Above-mentioned 75SN base oil is mixed with citric acid, at 100-120 ℃ of lower stirring reaction 10-14 minute, dinonylnaphthalene sulfonic acid calcium, lanolin magnesium soap, fully stir, and the reduction temperature is 70-80 ℃, add KORANTIN SH stearylamine salt, sulfide aliphatic acid ester, 2-aminoethyl 17 alkenyl imidazolines, film coalescence aid, insulated and stirred 2-3 hour, add each raw material of residue, at 40-50 ℃ of lower insulated and stirred 1-2 hour, filter discharging, obtain described high weather resisteant slushing oil.
Advantage of the present invention is:
Slushing oil of the present invention had both had well ageing-resistant, corrosion resistance nature, filmed stable, good at the workpiece surface spreading property, and metal works is had to good provide protection, and weather resisteant is strong, and under natural condition, filming, it is destroyed to be difficult to.
Embodiment
Embodiment 1
A kind of high weather resisteant slushing oil, it is comprised of the raw material of following weight parts (kilogram):
75SN base oil 75, dinonylnaphthalene sulfonic acid calcium 5, lanolin magnesium soap 3, citric acid 1, KORANTIN SH stearylamine salt 1, sulfide aliphatic acid ester 2,2-aminoethyl 17 alkenyl imidazolines 2, film coalescence aid 3, β-positive octadecanol ester 0.3 of (3,5-di-tert-butyl-hydroxy phenyl) propionic acid;
Described film coalescence aid is comprised of the raw material of following weight parts:
Drying oil alkyd resin 40, hexamethoxymethyl melamine resin 3, Oleum Cinnamomi 2, polyvinylpyrrolidone 2, N-phenyl-2-naphthylamine 0.3, Union carbide A-162 0.2;
Above-mentioned drying oil alkyd resin is mixed with Oleum Cinnamomi, 100 ℃ of lower insulated and stirred 8 minutes, reducing temperature is 65 ℃, adds the hexamethoxymethyl melamine resin, after fully stirring, adds Union carbide A-162,300 rev/mins of dispersed with stirring 15 minutes, the rising temperature is 135 ℃, adds each raw material of residue, insulation reaction 1 hour, be cooled to normal temperature, obtain described film coalescence aid.
A kind of preparation method of high weather resisteant slushing oil comprises the following steps:
Above-mentioned 75SN base oil is mixed with citric acid, 120 ℃ of lower stirring reactions 14 minutes, dinonylnaphthalene sulfonic acid calcium, lanolin magnesium soap, fully stir, and reducing temperature is 80 ℃, add KORANTIN SH stearylamine salt, sulfide aliphatic acid ester, 2-aminoethyl 17 alkenyl imidazolines, film coalescence aid, insulated and stirred 2 hours, add each raw material of residue, 50 ℃ of lower insulated and stirred 2 hours, filter discharging, obtain described high weather resisteant slushing oil.
Performance test:
Humid heat test: 20 days, result: 45 steel were qualified, T3 copper is qualified;
Corrosion test: 7 days, result: 45 steel were qualified, T3 copper is qualified;
Salt-fog test: 7 days, 45 steel were qualified, T3 copper is qualified.
Claims (2)
1. one kind high weather resisteant slushing oil is characterized in that what it was comprised of the raw material of following weight parts:
75SN base oil 70-75, dinonylnaphthalene sulfonic acid calcium 3-5, lanolin magnesium soap 2-3, citric acid 1-2, KORANTIN SH stearylamine salt 1-2, sulfide aliphatic acid ester 2-3,2-aminoethyl 17 alkenyl imidazoline 1-2, film coalescence aid 2-3, the β-positive octadecanol ester of (3,5-di-tert-butyl-hydroxy phenyl) propionic acid 0.1-0.3;
Described film coalescence aid is comprised of the raw material of following weight parts:
Drying oil alkyd resin 30-40, hexamethoxymethyl melamine resin 2-3, Oleum Cinnamomi 1-2, polyvinylpyrrolidone 1-2, N-phenyl-2-naphthylamine 0.1-0.3, Union carbide A-162 0.1-0.2;
Above-mentioned drying oil alkyd resin is mixed with Oleum Cinnamomi, at 90-100 ℃ of lower insulated and stirred 6-8 minute, the reduction temperature is 55-65 ℃, adds the hexamethoxymethyl melamine resin, after fully stirring, adds Union carbide A-162,200-300 rev/min of dispersed with stirring 10-15 minute, the rising temperature is 130-135 ℃, adds each raw material of residue, insulation reaction 1-3 hour, be cooled to normal temperature, obtain described film coalescence aid.
2. the preparation method of a high weather resisteant slushing oil as claimed in claim 1 is characterized in that comprising the following steps:
Above-mentioned 75SN base oil is mixed with citric acid, at 100-120 ℃ of lower stirring reaction 10-14 minute, dinonylnaphthalene sulfonic acid calcium, lanolin magnesium soap, fully stir, and the reduction temperature is 70-80 ℃, add KORANTIN SH stearylamine salt, sulfide aliphatic acid ester, 2-aminoethyl 17 alkenyl imidazolines, film coalescence aid, insulated and stirred 2-3 hour, add each raw material of residue, at 40-50 ℃ of lower insulated and stirred 1-2 hour, filter discharging, obtain described high weather resisteant slushing oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310361700.9A CN103484192A (en) | 2013-08-19 | 2013-08-19 | High-weather-resistance anti-rust oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310361700.9A CN103484192A (en) | 2013-08-19 | 2013-08-19 | High-weather-resistance anti-rust oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103484192A true CN103484192A (en) | 2014-01-01 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310361700.9A Pending CN103484192A (en) | 2013-08-19 | 2013-08-19 | High-weather-resistance anti-rust oil |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017197718A1 (en) * | 2016-05-20 | 2017-11-23 | 邢燕 | Antirust agent for firearm |
| CN109897718A (en) * | 2017-12-11 | 2019-06-18 | 中国石油天然气股份有限公司 | Barium-free soft film anti-rust oil |
| CN114381322A (en) * | 2021-12-24 | 2022-04-22 | 苏州市浒墅关化工添加剂有限公司 | Film-forming stable anti-rust oil prepared from base oil and preparation method thereof |
-
2013
- 2013-08-19 CN CN201310361700.9A patent/CN103484192A/en active Pending
Non-Patent Citations (3)
| Title |
|---|
| 周静妤: "《防锈技术》", 31 December 1988, 化学工业出版社 * |
| 李金桂: "《防腐蚀表面工程技术》", 31 December 2002, 化学工业出版社 * |
| 李金桂等: "《腐蚀和腐蚀控制手册》", 31 July 1988, 国防工业出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017197718A1 (en) * | 2016-05-20 | 2017-11-23 | 邢燕 | Antirust agent for firearm |
| CN109897718A (en) * | 2017-12-11 | 2019-06-18 | 中国石油天然气股份有限公司 | Barium-free soft film anti-rust oil |
| CN109897718B (en) * | 2017-12-11 | 2021-11-30 | 中国石油天然气股份有限公司 | Barium-free soft film rust-proof oil |
| CN114381322A (en) * | 2021-12-24 | 2022-04-22 | 苏州市浒墅关化工添加剂有限公司 | Film-forming stable anti-rust oil prepared from base oil and preparation method thereof |
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Application publication date: 20140101 |