CN103468051B - Preparation method of rubber coating - Google Patents

Preparation method of rubber coating Download PDF

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Publication number
CN103468051B
CN103468051B CN201310422279.8A CN201310422279A CN103468051B CN 103468051 B CN103468051 B CN 103468051B CN 201310422279 A CN201310422279 A CN 201310422279A CN 103468051 B CN103468051 B CN 103468051B
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component
rubber
preparation
rubber coating
mixing
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CN103468051A (en
Inventor
朱卫峰
周圣峰
高纪超
曲坚冰
娄江波
宋翠玲
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Yantai Ishikawa Sealing Technology Co., Ltd.
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YANTAI QUANFENG SEALING TECHNOLOGY Co Ltd
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Abstract

The invention discloses a preparation method of a rubber coating. The rubber coating is characterized in that the rubber coating is prepared by independently preparing a component A and a component B and finally mixing; the component A contains rubber, fillers and accessory ingredients; the preparation process comprises the following steps: firstly, mixing raw materials in the component A uniformly with an internal mixer, discharging slices with an open mill, cutting the materials by using a material cutting machine, then melting the rubber, adding a defoaming agent and a flatting agent, grinding and filtering for multiple times. The component B comprises raw rubber, fillers and a rubber accelerant; the preparation process comprises the following steps: plasticating the raw materials in the component B with the open mill, thinning and discharging slices, cutting the materials by using the material cutting machine, melting the rubber and filtering for multiple times; then mixing rubber slurry of the component A and the component B uniformly, standing and defoaming, and thus preparing the rubber coating. The rubber coating is mixed uniformly; the quality and the color are easily controllable, so that the rubber coating is suitable for flow production and long-term storage, and the fineness of the coating and the flatting of the coating are not affected.

Description

A kind of preparation method of rubber coating
Technical field
The present invention relates to technical field of rubber material, specifically a kind of preparation method of rubber coating.
Background technology
At present, preparing the normally used method of rubber coating is undertaken mixing without overstocked, mill by filler and rubber, directly powder, auxiliary agent, rubber are dropped into colloidal sol still solubilizing agent and dissolves, although mode is simple, but owing to lacking the process of rubber and the mixing of auxiliary material banburying high speed shear and plasticizing of beginning to pratise, rubber mixes uneven with auxiliary material, the easy layering of coating, summer, configuration easily produced gelatin phenomenon, and the more difficult control of the color of coating, strict to configuration temperature requirement, be not suitable for streamline operration and standing storage; In addition, without the rubber coating of sand milling, filtration, there is certain impurity, thus affect the fineness of coating and the smooth of coating.
Summary of the invention
The object of the invention is the deficiency overcoming above-mentioned prior art, and a kind of preparation method of rubber coating is provided, mainly solve uneven, the easy layering of existing rubber coating mixing, easily produce gelatin phenomenon, the more difficult control of color, be not suitable for streamline operration and standing storage and affect the problem such as the fineness of coating and the smooth of coating.
Technical scheme of the present invention is: a kind of preparation method of rubber coating, and its special character is, described rubber coating is prepared separately by component A, B component, finally mixes; Described component A is mainly containing rubber, filler, auxiliary agent, and its preparation technology is first that the raw material in component A is even by Banbury mixer, by mill slice, utilizes material cutting machine to cut out material, then colloidal sol, after adding defoamer and flow agent, carries out grinding, Multi-channel filtering; Described B component is mainly containing rubber, filler and vulcanization accelerator, and the raw material in B component is plasticated by mill, put through slice by its preparation technology, utilizes material cutting machine to cut out material, colloidal sol, Multi-channel filtering; Then A, B component rubber cement are mixed, static froth breaking, the rubber coating of system.
Further, the rubber of described component A is one or both and two or more combinations in paracril, viton, acrylic elastomer, hydrogenated nitrile-butadiene rubber, silicon rubber.
Further, the filler of described component A is carbon black, white carbon black, diatomite, one or more mixing in potter's clay.
Further, the auxiliary agent of described component A is stearic acid, softening agent, anti-aging agent, one or more mixing in paraffin.
Further, the one in paracril, viton, acrylic elastomer, hydrogenated nitrile-butadiene rubber, silicon rubber selected by the rubber of described B component, or selects identical with the kind of component A.
Further, the filler of described B component is carbon black, white carbon black, diatomite, one or more mixing in potter's clay, or selects identical with component A.
Further, the vulcanization accelerator of described B component is one or more mixing in CZ, M, DM, DCP, TMTD.
Further, described component A be ground to sand milling, ball milling or triple-roller mill.
Further, described Multi-channel filtering is deep bed filter, pipe filter and Jenag strainer or vibratory screening apparatus.
Compared with the prior art the preparation method of a kind of rubber coating of the present invention has outstanding substantive distinguishing features and marked improvement, 1, select rubber first mixing with filler etc. become rubber unvulcanizate be dissolved into the way of coating again and existing rubber first dissolves the way adding the powders such as filler afterwards, due to the mode that mixing method have passed through banburying, opens refining, also has the repeatedly mechanical dispersion of dispersed with stirring in dissolving, make the compatible more abundant of material and rubber, rubber coating is mixed, quality and color easy to control, be applicable to streamline operration; 2, be the way adopting the mixing of AB glue, make the staging life of AB two kinds of rubber unvulcanizates all very long, avoid the situation that material that the reason due to staging life causes is cross-linked inefficacy and be applicable to standing storage; 3, because the coating after dissolving also will make the fineness of coating be controlled further through multistage physical filtering, the fineness of coating and the smooth of coating is not affected.
Embodiment
In order to Comprehension and Implementation better, describe the present invention in detail below in conjunction with embodiment; Illustrated embodiment, only for explaining the present invention, is not for limiting the present invention.
Embodiment 1, rubber coating is divided into A, B component is prepared separately:
Component A compounding rubber, selects suitable rubber as required, and rubber can be one or both and two or more combinations in paracril, viton, acrylic elastomer, hydrogenated nitrile-butadiene rubber, silicon rubber; Select suitable filler and auxiliary agent according to rubber and kind, filler is one or more mixing in carbon black, white carbon black, diatomite, potter's clay, and auxiliary agent is stearic acid, softening agent, anti-aging agent simultaneously, one or more mixing in paraffin; By rubber stripping and slicing, then rubber pig, filler, auxiliary agent are dropped into mixer mixing 40 minutes, the 4-5 of mill thin-pass afterwards time slice, slice thickness 5-7MM;
B component compounding rubber, rubber is put into open type rubber mixing machine to plasticate, add filler, vulcanization accelerator after bag roller, rubber is the one in paracril, viton, acrylic elastomer, hydrogenated nitrile-butadiene rubber, silicon rubber, or selects identical with the kind of component A; Filler is carbon black, white carbon black, diatomite, one or more mixing in potter's clay, or selects identical with component A, reaches and facilitates mixing object; Vulcanization accelerator is one or more mixing in CZ, M, DM, DCP, TMTD, mill slice after thin-pass, slice thickness 5-7MM;
A, B component film are cut into respectively the fritter of 2-3cm; Squeezed into by solvent in stirred pot 1 and stirred pot 2, stirred pot passes into water coolant; In stirred pot 1, drop into component A film, in stirred pot 2, drop into B component film, start to stir and dispersion; In component A, defoamer and flow agent is added after being uniformly dispersed; Again component A rubber cement is carried out sand milling 3 times, lapping mode is sand milling, ball milling or triple-roller mill; Component A after sand milling is carried out the filtration of Multi-channel filtering system; Scattered B component is carried out the filtration of Multi-channel filtering system; Multi-channel filtering is deep bed filter, pipe filter and Jenag strainer, vibratory screening apparatus; Then by the component A rubber cement that filtered and B component rubber cement blending dispersion, static froth breaking is stand-by.

Claims (9)

1. a preparation method for rubber coating, is characterized in that, described rubber coating is prepared separately by component A, B component, finally mixes; Described component A is mainly containing rubber, filler, auxiliary agent, and its preparation technology is first that the raw material in component A is even by Banbury mixer, by mill slice, utilizes material cutting machine to cut out material, then colloidal sol, after adding defoamer and flow agent, carries out grinding, Multi-channel filtering; Described B component is mainly containing rubber, filler and vulcanization accelerator, and the raw material in B component is plasticated by mill, put through slice by its preparation technology, utilizes material cutting machine to cut out material, colloidal sol, Multi-channel filtering; Then A, B component rubber cement are mixed, static froth breaking, the rubber coating of system.
2. the preparation method of a kind of rubber coating according to claim 1, is characterized in that, the rubber of described component A is one or both and two or more combinations in paracril, viton, acrylic elastomer, hydrogenated nitrile-butadiene rubber, silicon rubber.
3. the preparation method of a kind of rubber coating according to claim 1, is characterized in that, the filler of described component A is carbon black, white carbon black, diatomite, one or more mixing in potter's clay.
4. the preparation method of a kind of rubber coating according to claim 1, is characterized in that, the auxiliary agent of described component A is stearic acid, softening agent, anti-aging agent, one or more mixing in paraffin.
5. the preparation method of a kind of rubber coating according to claim 1, it is characterized in that, the one in paracril, viton, acrylic elastomer, hydrogenated nitrile-butadiene rubber, silicon rubber selected by the rubber of described B component, or selects identical with the kind of component A.
6. the preparation method of a kind of rubber coating according to claim 1, is characterized in that, the filler of described B component is carbon black, white carbon black, diatomite, one or more mixing in potter's clay, or selects identical with component A.
7. the preparation method of a kind of rubber coating according to claim 1, is characterized in that, the vulcanization accelerator of described B component is one or more mixing in CZ, M, DM, DCP, TMTD.
8. the preparation method of a kind of rubber coating according to claim 1, is characterized in that, described component A be ground to sand milling, ball milling or triple-roller mill.
9. the preparation method of a kind of rubber coating according to claim 1, is characterized in that, described Multi-channel filtering is deep bed filter, pipe filter and Jenag strainer or vibratory screening apparatus.
CN201310422279.8A 2013-09-17 2013-09-17 Preparation method of rubber coating Active CN103468051B (en)

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CN106396608B (en) * 2016-08-30 2019-03-22 福建省泉州市契合工贸有限公司 Ceramics and preparation method thereof with abrasive rubber surface layer

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102585612A (en) * 2011-12-30 2012-07-18 南昌大学 Foamed rubber coating and application thereof to preparation of foamed rubber composite material

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DE10038488A1 (en) * 2000-08-08 2002-02-21 Bayer Ag Rubber mixtures containing isocyanatosilane and microgel
DE102007029644A1 (en) * 2007-06-26 2009-01-08 Henkel Ag & Co. Kgaa One-component, hot-curing reactive composition

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102585612A (en) * 2011-12-30 2012-07-18 南昌大学 Foamed rubber coating and application thereof to preparation of foamed rubber composite material

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Owner name: SHICHUAN SEAL GASKET CO., LTD., YANTAI CITY

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Effective date: 20150831

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Address after: 264000 Shandong Province, Yantai city Zhifu District moon Road No. 5

Patentee after: YANTAI ISHIKAWA GASKET CO., LTD.

Address before: 264002 Shandong Province, Yantai city Zhifu District moon Road No. 80

Patentee before: Yantai Quanfeng Sealing Technology Co., Ltd.

C56 Change in the name or address of the patentee
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Address after: 264000 Shandong Province, Yantai city Zhifu District moon Road No. 5

Patentee after: Yantai Ishikawa Sealing Technology Co., Ltd.

Address before: 264000 Shandong Province, Yantai city Zhifu District moon Road No. 5

Patentee before: YANTAI ISHIKAWA GASKET CO., LTD.