CN103451039A - Special-purpose solid cleaning agent of dish-washing machine and preparation method thereof - Google Patents
Special-purpose solid cleaning agent of dish-washing machine and preparation method thereof Download PDFInfo
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- CN103451039A CN103451039A CN2012102349361A CN201210234936A CN103451039A CN 103451039 A CN103451039 A CN 103451039A CN 2012102349361 A CN2012102349361 A CN 2012102349361A CN 201210234936 A CN201210234936 A CN 201210234936A CN 103451039 A CN103451039 A CN 103451039A
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Abstract
The invention relates to a special-purpose solid cleaning agent of a dish-washing machine and a preparation method thereof. The special-purpose solid cleaning agent consists of the following substances in percent by weight: 20%-50% of sodium hydroxide or/and potassium hydroxide, 15%-30% of sodium carbonate, 10%-20% of sodium metasilicate, 3%-6% of sodium dichloro isocyanurate or imidazolidinedione, 4%-8% of EDTA (Ethylene Diamine Tetraacetic Acid), 1%-5% of sodium citrate, 5%-10% of a dispersing agent PAA (Poly Acrylic Acid), 1%-5% of borax and the balance of water. The preparation method of the special-purpose solid cleaning agent comprises the following steps of preparing the solid substances according to a proportion of the formula; starting up a reaction kettle, and respectively adding the solid materials under stirring; adding water after all solid materials are added and uniformly stirred; starting to heat up inside the reaction kettle with the addition of water, so that the materials generate reaction; stirring reactants for cooling to 50 DEG C-60DEG C, and starting to discharge; metering and pouring moving materials to a product container when the moving materials are hot, cooling and forming to obtain a finished product. The preparation method disclosed by the invention is low in reaction temperature, good in reactant mobility, easy for finally forming, energy-saving, environment-friendly and high in efficiency.
Description
Technical field
The present invention relates to a kind of dishwasher special solid clean-out system and preparation method thereof.
Background technology
The solid detergent of use in dishwasher, all extensively adopt solid powder at present both at home and abroad, and existing problems are to feed in raw material in batches, and number of times is frequent.And solids feed opening being blocked and pipeline easily occur in use procedure, and be developed to the solid shaped detergent both at home and abroad, but its production process power consumption being high, effect is low.Its process using reaction mass heating and melting, mix rear discharging first cooling, moulding, then pack.Because binder is difficult for cooled and solidified, cause and waste time and energy, waste energy.
Summary of the invention
The purpose of this invention is to provide a kind of dishwasher special solid clean-out system and preparation method thereof; Spontaneous heat while adopting the mixing of materials reaction, make the mobile property of reaction mass be convenient to well mix, and material is even and good fluidity, be easy to last moulding, due to good fluidity, during reaction, temperature is low, can directly be put in plastic barrel and directly pack, energy-conserving and environment-protective efficiency is high.
Dishwasher special solid clean-out system of the present invention 100% is comprised of following material by weight: sodium hydroxide or potassium hydroxide 20-50%, soda ash 15-30%, Starso 10-20%, Surchlor GR 60 or two chlordantoin 3-6%, EDTA4-8%, Trisodium Citrate 1-5%, dispersion agent PAA consumption 5-10%, borax 1-5%, surplus are water.
Cleaning decontamination host in formula is basic cpd, and with sodium hydroxide, potassium hydroxide one class is main, take soda ash as auxiliary, is equipped with sterilant, water-softening chemicals, dispersion agent, sanitas.
The technological process of dishwasher special solid clean-out system of the present invention:
Above-mentioned solid matter is got the raw materials ready by formula rate, start reactor, under agitation add respectively solid materials, after solid materials all adds, wait to stir, add water, along with adding of water, in reactor, start to heat up, material reacts, and reaction stirred is cooled to 50-60 ℃ and starts blowing, by flowable materials, metering is while hot poured in product vessel, and cooling forming, be finished product.
The cardinal principle of this explained hereafter solid shaped detergent is that thermopositive reaction generation heat can occur raw material solid strongly alkaline compound chance water, utilize solution heat that thermal source is provided, the heat that produces can meet whole reaction requirement, make each raw material of product that further polymerization and crystal hydration reaction occur, rapidly by flowable materials, metering is while hot poured in product vessel, and cooling forming, be finished product.
Key problem in technology of the present invention is to utilize the chemical reaction solution heat that heat is provided, and strictly controls the accurate proportioning of raw material, and with the adaptive response polymerization degree, reaching due shaping hardness must condition with the production that meets the dishwasher use with solubleness in water.
Processing unit:
This processing requirement, can make solid materials evenly mix, and requires stirring in reactor that enough power should be arranged, and it is that the anchor formula combines with the propeller formula that agitator structure adopts duplex.And stirring rake can be scraped wall, in case the sticky wall of material.
Processing condition:
Reactor stirring velocity: 60-80 rev/min.
Temperature is controlled:
Heat up: it is by automatic heating that reaction heats up.
Discharging: question response still temperature drop gets final product discharging to 50-60 ℃, and discharging keeps 50-60 ℃.
The dishwasher special solid clean-out system that present method is produced:
1. washing fluid concentration: rinse with 3 premium on currency, in water, should be no less than 0.2% containing solid.
2 product hardness: with finger, press by method, test should bear generally presses.
Spontaneous heat when dishwasher special solid clean-out system of the present invention adopts the mixing of materials reaction, make the mobile property of reaction mass be convenient to well mix, and material is even and good fluidity, be easy to last moulding, due to good fluidity, during reaction, temperature is low, can directly be put in plastic barrel and directly pack, and energy-conserving and environment-protective efficiency is high.
Embodiment
Embodiment 1
Dishwasher special solid clean-out system of the present invention 100% forms in respect of following material by weight: sodium hydroxide 20%, soda ash 15%, Starso 20%, Surchlor GR 60 6%, EDTA8%, Trisodium Citrate 5%, dispersion agent PAA consumption 10%, borax 5%, surplus are water.
Above-mentioned solid matter is got the raw materials ready by formula rate, start reactor, under agitation add respectively solid materials, after solid materials all adds, wait to stir, add water, along with adding of water, in reactor, start to heat up, material reacts, and reaction stirred is cooled to 55 ℃ and starts blowing, by flowable materials, measure while hot 3 kilograms one and pour in product vessel, cooling forming, be finished product.Reactor stirring velocity: 80 rev/mins.With 3 premium on currency, rinsing, is 0.2% containing solid in water.
Embodiment 2
Dishwasher special solid clean-out system of the present invention 100% forms in respect of following material by weight: potassium hydroxide 25%, soda ash 20%, Starso 20%, two chlordantoins 3%, EDTA4%, Trisodium Citrate 1%, dispersion agent PAA consumption 8%, borax 1%, surplus are water.
Above-mentioned solid matter is got the raw materials ready by formula rate, start reactor, under agitation add respectively solid materials, after solid materials all adds, wait to stir, add water, along with adding of water, in reactor, start to heat up, material reacts, and reaction stirred is cooled to 50 ℃ and starts blowing, by flowable materials, measure while hot 2 kilograms one and pour in product vessel, cooling forming, be finished product.Reactor stirring velocity: 60 rev/mins.
Embodiment 3
Dishwasher special solid clean-out system of the present invention 100% forms in respect of following material by weight: sodium hydroxide 30%, soda ash 20%, Starso 15%, Surchlor GR 60 4%, EDTA5%, Trisodium Citrate 3%, dispersion agent PAA consumption 6%, borax 2%, surplus are water.
Above-mentioned solid matter is got the raw materials ready by formula rate, start reactor, under agitation add respectively solid materials, after solid materials all adds, wait to stir, add water, along with adding of water, in reactor, start to heat up, material reacts, and reaction stirred is cooled to 60 ℃ and starts blowing, by flowable materials, metering is while hot poured in product vessel, and cooling forming, be finished product.Reactor stirring velocity: 70 rev/mins.
Claims (2)
1. a dishwasher special solid clean-out system, it is characterized in that: 100% is comprised of following material by weight: sodium hydroxide is or/and potassium hydroxide 20-50%, soda ash 15-30%, Starso 10-20%, Surchlor GR 60 or two chlordantoin 3-6%, EDTA4-8%, Trisodium Citrate 1-5%, dispersion agent PAA consumption 5-10%, borax 1-5%, surplus are water.
2. the preparation method of a dishwasher special solid clean-out system, it is characterized in that: solid matter claimed in claim 1 is got the raw materials ready by formula rate, start reactor, under agitation add respectively solid materials, after solid materials all adds, wait to stir, add water, along with adding of water, in reactor, start to heat up, the heat that produces meets reaction requirement, material reacts, reaction stirred is cooled to 50-60 ℃ and starts blowing, by flowable materials, metering is while hot poured in product vessel, cooling forming, be finished product, reactor stirring velocity: 60-80 rev/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201210234936.1A CN103451039B (en) | 2012-07-06 | 2012-07-06 | Special-purpose solid cleaning agent of dish-washing machine and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210234936.1A CN103451039B (en) | 2012-07-06 | 2012-07-06 | Special-purpose solid cleaning agent of dish-washing machine and preparation method thereof |
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| CN103451039A true CN103451039A (en) | 2013-12-18 |
| CN103451039B CN103451039B (en) | 2015-03-25 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107189887A (en) * | 2017-04-18 | 2017-09-22 | 浙江德清民爱生物科技有限公司 | A kind of dish washing detergent and preparation method |
| JP2017186549A (en) * | 2016-03-31 | 2017-10-12 | 株式会社Adeka | Fused solid type detergent composition |
| CN109504569A (en) * | 2018-12-10 | 2019-03-22 | 沈阳化工大学 | A kind of dish washing detergents |
| CN109652234A (en) * | 2017-10-12 | 2019-04-19 | 广州市东莱晟生物科技有限公司 | A kind of dish-washing machine detergent and preparation method thereof containing alkali protease |
| CN110819474A (en) * | 2019-08-05 | 2020-02-21 | 广州索汰清洁技术有限公司 | Cleaning agent, cleaning device and cleaning method for commercial kitchen oil stain kitchenware |
| CN112080349A (en) * | 2020-10-20 | 2020-12-15 | 广东水卫仕生物科技有限公司 | Special solid detergent for dish-washing machine and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1215749A (en) * | 1997-10-29 | 1999-05-05 | 罗俊生 | Formulation and process for preparing homogeneous base number non-toxic washing powder |
| CN1318635A (en) * | 2000-04-14 | 2001-10-24 | 苏映曦 | Multifunctional refrigerator cleaning and protecting agent |
-
2012
- 2012-07-06 CN CN201210234936.1A patent/CN103451039B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1215749A (en) * | 1997-10-29 | 1999-05-05 | 罗俊生 | Formulation and process for preparing homogeneous base number non-toxic washing powder |
| CN1318635A (en) * | 2000-04-14 | 2001-10-24 | 苏映曦 | Multifunctional refrigerator cleaning and protecting agent |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2017186549A (en) * | 2016-03-31 | 2017-10-12 | 株式会社Adeka | Fused solid type detergent composition |
| CN107189887A (en) * | 2017-04-18 | 2017-09-22 | 浙江德清民爱生物科技有限公司 | A kind of dish washing detergent and preparation method |
| CN109652234A (en) * | 2017-10-12 | 2019-04-19 | 广州市东莱晟生物科技有限公司 | A kind of dish-washing machine detergent and preparation method thereof containing alkali protease |
| CN109504569A (en) * | 2018-12-10 | 2019-03-22 | 沈阳化工大学 | A kind of dish washing detergents |
| CN110819474A (en) * | 2019-08-05 | 2020-02-21 | 广州索汰清洁技术有限公司 | Cleaning agent, cleaning device and cleaning method for commercial kitchen oil stain kitchenware |
| CN112080349A (en) * | 2020-10-20 | 2020-12-15 | 广东水卫仕生物科技有限公司 | Special solid detergent for dish-washing machine and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103451039B (en) | 2015-03-25 |
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Effective date of registration: 20160304 Address after: 100026 B13F, 23 East Lane, Bai Jia Zhuang, Beijing, Chaoyang District Patentee after: Beijing Wan en chemical products Co., Ltd. Address before: 101113, Beijing, Tongzhou District Zhang Wan Town Industrial Zone Patentee before: Beijing Wanen Science and Technology Co., Ltd. |
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Effective date of registration: 20160801 Address after: 100021, room 1, building 58, No. 2005 East Third Ring Road, Beijing, Chaoyang District Patentee after: Sino grace Technology Co., LIMITED Address before: 100026 B13F, 23 East Lane, Bai Jia Zhuang, Beijing, Chaoyang District Patentee before: Beijing Wan en chemical products Co., Ltd. |