CN103435291A - Fire retardant foam wall body insulation board and preparation method thereof - Google Patents

Fire retardant foam wall body insulation board and preparation method thereof Download PDF

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Publication number
CN103435291A
CN103435291A CN2013102973608A CN201310297360A CN103435291A CN 103435291 A CN103435291 A CN 103435291A CN 2013102973608 A CN2013102973608 A CN 2013102973608A CN 201310297360 A CN201310297360 A CN 201310297360A CN 103435291 A CN103435291 A CN 103435291A
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China
Prior art keywords
parts
loess
powder
retardant foam
foam wall
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CN2013102973608A
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Chinese (zh)
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CN103435291B (en
Inventor
汪永辉
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Kangbao Laoga Thermal Insulation Materials Co Ltd
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Individual
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Publication of CN103435291B publication Critical patent/CN103435291B/en
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  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)

Abstract

The invention provides a fire retardant foam wall body insulation board and a preparation method thereof, and is characterized in that the fire retardant foam wall body insulation board is prepared from the following raw materials in parts by weight: 95-105 parts of polystyrene, 8-10 parts of a polyacrylic emulsion, 5-8 parts of sodium lauryl sulfate, 2-4 parts of freon, 3.5-5 parts of zinc cyanurate, 4-6 parts of a silane coupling agent KH560, 5-6 parts of dimethicone, 8-10 parts of antimony trioxide, 38-45 parts of an aluminum hydroxide powder, and 30-35 parts of modified loess. Thermal conductivity coefficient, flame retardance, heat resistance and cold resistance, thermal stability, strength and other indicators of the fire retardant foam wall body insulation board are all higher than those of an existing extruded polystyrene foam insulation board.

Description

A kind of flame-retardant foam wall insulated board and preparation method thereof
Technical field
The present invention relates to a kind of wallboard, more particularly, is a kind of flame-retardant foam wall insulated board and preparation method thereof.
Background technology
The building construction of building construction, particularly extremely frigid zones, the amount of heat in building scatters and disappears by roof and body of wall.Therefore, need to pave warming plate on roof and exterior wall, play the effect of heat insulating and save energy.Existing plastic extrusion heated board, have the shortcoming that intensity is low, resistance to compression is low, density is low, resistance to deterioration is weak, cost is high, need to have new product to emerge, and participates in the competition.
Summary of the invention
The purpose of this invention is to provide a kind of flame-retardant foam wall insulated board and preparation method thereof.
The technical solution adopted in the present invention is:
A kind of flame-retardant foam wall insulated board is characterized in that being made by the raw material of following weight part:
Polystyrene 95-105, ACRYLIC EMULSION 8-10, sodium laurylsulfate 5-8, freon-12-4, cyanuric acid zinc 3.5-5, silane coupling agent KH560 4-6, dimethyl silicone oil 5-6, antimonous oxide 8-10, aluminium hydrate powder 38-45, modified Loess 30-35;
Described modified Loess is made by the raw material of following weight part: loess 100-120, plant ash 30-40, used oil 10-12, starch 10-12, Sodium dodecylbenzene sulfonate 1-2, aluminium powder 0.2-0.3, water are appropriate;
The preparation method is: loess is calcined under 460-480 ℃ to 2-3 hour, grinding powder; Starch, Sodium dodecylbenzene sulfonate are joined in suitable quantity of water, be heated into pasty state; Add described calcining loess powder, plant ash, aluminium powder, used oil in sticking with paste, mix and blend 40-50 minute, send in 60-70 ℃ of drying room and dry, and is broken into coarse particles, and the coarse particles that sifts out 1-3mm gets final product.
The preparation method of described flame-retardant foam wall insulated board is characterized in that comprising the following steps:
(1) ACRYLIC EMULSION, sodium laurylsulfate, cyanuric acid zinc, silane coupling agent KH560, dimethyl silicone oil, antimonous oxide, aluminium hydrate powder, modified Loess are mixed, stir;
(2) then by polystyrene and step (1) mixing of materials, be heated to 190-235 ℃; Make each material melting and mixing, form polymer melt; Then add freonll-11 to be uniformly mixed; Melt is cooled to 100-125 ℃, then, sends into extruding machine, extrusion moulding.
The indexs such as thermal conductivity of the present invention, flame retardant resistance, heat-resisting and winter hardiness, thermostability, intensity are all higher than existing extruded polystyrene foam heat-insulating board.
Embodiment
A kind of flame-retardant foam wall insulated board, by the raw material of following weight part (kilogram), made:
Polystyrene 105, ACRYLIC EMULSION 10, sodium laurylsulfate 8, freon-12, cyanuric acid zinc 5, silane coupling agent KH560 6, dimethyl silicone oil 6, antimonous oxide 10, aluminium hydrate powder 45, modified Loess 35;
Described modified Loess is made by the raw material of following weight part (kilogram): loess 120, plant ash 30, used oil 10, starch 12, Sodium dodecylbenzene sulfonate 2, aluminium powder 0.3, water are appropriate;
The preparation method is: loess is calcined under 460-480 ℃ to 2-3 hour, grinding powder; Starch, Sodium dodecylbenzene sulfonate are joined in suitable quantity of water, be heated into pasty state; Add described calcining loess powder, plant ash, aluminium powder, used oil in sticking with paste, mix and blend 40-50 minute, send in 60-70 ℃ of drying room and dry, and is broken into coarse particles, and the coarse particles that sifts out 1-3mm gets final product.
The preparation method of flame-retardant foam wall insulated board comprises the following steps:
(1) ACRYLIC EMULSION, sodium laurylsulfate, cyanuric acid zinc, silane coupling agent KH560, dimethyl silicone oil, antimonous oxide, aluminium hydrate powder, modified Loess are mixed, stir;
(2) then by polystyrene and step (1) mixing of materials, be heated to 190-235 ℃; Make each material melting and mixing, form polymer melt; Then add freonll-11 to be uniformly mixed; Melt is cooled to 100-125 ℃, then, sends into extruding machine, extrusion moulding.
The present invention after testing, ultimate compression strength >=280kPa, thermal conductivity≤0.03W/mk, water-intake rate≤1% (V/V), aqueous vapor moisture permeable coefficient≤3ng/m.s.Pa.

Claims (2)

1. a flame-retardant foam wall insulated board is characterized in that being made by the raw material of following weight part:
Polystyrene 95-105, ACRYLIC EMULSION 8-10, sodium laurylsulfate 5-8, freon-12-4, cyanuric acid zinc 3.5-5, silane coupling agent KH560 4-6, dimethyl silicone oil 5-6, antimonous oxide 8-10, aluminium hydrate powder 38-45, modified Loess 30-35;
Described modified Loess is made by the raw material of following weight part: loess 100-120, plant ash 30-40, used oil 10-12, starch 10-12, Sodium dodecylbenzene sulfonate 1-2, aluminium powder 0.2-0.3, water are appropriate;
The preparation method is: loess is calcined under 460-480 ℃ to 2-3 hour, grinding powder; Starch, Sodium dodecylbenzene sulfonate are joined in suitable quantity of water, be heated into pasty state; Add described calcining loess powder, plant ash, aluminium powder, used oil in sticking with paste, mix and blend 40-50 minute, send in 60-70 ℃ of drying room and dry, and is broken into coarse particles, and the coarse particles that sifts out 1-3mm gets final product.
2. the preparation method of flame-retardant foam wall insulated board according to claim 1 is characterized in that comprising the following steps:
(1) ACRYLIC EMULSION, sodium laurylsulfate, cyanuric acid zinc, silane coupling agent KH560, dimethyl silicone oil, antimonous oxide, aluminium hydrate powder, modified Loess are mixed, stir;
(2) then by polystyrene and step (1) mixing of materials, be heated to 190-235 ℃; Make each material melting and mixing, form polymer melt; Then add freonll-11 to be uniformly mixed; Melt is cooled to 100-125 ℃, then, sends into extruding machine, extrusion moulding.
CN201310297360.8A 2013-07-16 2013-07-16 A kind of Fire retardant foam wall body insulation board and preparation method thereof Expired - Fee Related CN103435291B (en)

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CN201310297360.8A CN103435291B (en) 2013-07-16 2013-07-16 A kind of Fire retardant foam wall body insulation board and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201310297360.8A CN103435291B (en) 2013-07-16 2013-07-16 A kind of Fire retardant foam wall body insulation board and preparation method thereof

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CN103435291A true CN103435291A (en) 2013-12-11
CN103435291B CN103435291B (en) 2016-02-03

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103509270A (en) * 2013-09-06 2014-01-15 安庆市吉美装饰材料有限责任公司 Flame-retardant foam wall thermal-insulation plate and preparation method thereof
CN103964741A (en) * 2014-05-04 2014-08-06 朱希桥 Energy-saving and environment-friendly plate and preparation method thereof
CN104355591A (en) * 2014-10-13 2015-02-18 合肥庭索环保材料有限公司 Environment-friendly thermal-insulation wallboard and manufacturing method thereof

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1483705A (en) * 2002-09-18 2004-03-24 斌 吴 Polybenzene foamed concrete thermal-insulating material and preparation process thereof
CN1702247A (en) * 2005-06-15 2005-11-30 孟永华 Environment-friendly energy-saving flame retardant extrusion moulding type polystyrene thermal insulation plate and preparation process thereof
US20070149628A1 (en) * 2005-08-22 2007-06-28 Yaollah Delaviz Deformable, rigid polystyrene foam boards
CN101319540A (en) * 2008-07-04 2008-12-10 陶国延 Polystyrene insulating brick and its production method and use method
CN101586368A (en) * 2009-06-23 2009-11-25 安徽森普新型材料发展有限公司 Extruded plastic thermal insulation thermal insulation board
CN101913900A (en) * 2010-08-26 2010-12-15 成都西亚科技发展有限公司 Foam concrete and preparation method
CN102584324A (en) * 2012-01-22 2012-07-18 深圳市沃尔核材股份有限公司 Cement flame-retardant foaming thermal insulation plate and production method thereof
CN102993351A (en) * 2011-12-15 2013-03-27 上海容志材料科技有限公司 Styrene and halogenated styrene copolymer and preparation method and application thereof

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1483705A (en) * 2002-09-18 2004-03-24 斌 吴 Polybenzene foamed concrete thermal-insulating material and preparation process thereof
CN1702247A (en) * 2005-06-15 2005-11-30 孟永华 Environment-friendly energy-saving flame retardant extrusion moulding type polystyrene thermal insulation plate and preparation process thereof
US20070149628A1 (en) * 2005-08-22 2007-06-28 Yaollah Delaviz Deformable, rigid polystyrene foam boards
CN101319540A (en) * 2008-07-04 2008-12-10 陶国延 Polystyrene insulating brick and its production method and use method
CN101586368A (en) * 2009-06-23 2009-11-25 安徽森普新型材料发展有限公司 Extruded plastic thermal insulation thermal insulation board
CN101913900A (en) * 2010-08-26 2010-12-15 成都西亚科技发展有限公司 Foam concrete and preparation method
CN102993351A (en) * 2011-12-15 2013-03-27 上海容志材料科技有限公司 Styrene and halogenated styrene copolymer and preparation method and application thereof
CN102584324A (en) * 2012-01-22 2012-07-18 深圳市沃尔核材股份有限公司 Cement flame-retardant foaming thermal insulation plate and production method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103509270A (en) * 2013-09-06 2014-01-15 安庆市吉美装饰材料有限责任公司 Flame-retardant foam wall thermal-insulation plate and preparation method thereof
CN103964741A (en) * 2014-05-04 2014-08-06 朱希桥 Energy-saving and environment-friendly plate and preparation method thereof
CN104355591A (en) * 2014-10-13 2015-02-18 合肥庭索环保材料有限公司 Environment-friendly thermal-insulation wallboard and manufacturing method thereof

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Effective date of registration: 20190528

Address after: 076650 Stone Park, Kangbao County, Zhangjiakou City, Hebei Province

Patentee after: Kangbao Laoga Thermal Insulation Materials Co., Ltd.

Address before: 241100 Wutun Road 518, New Wuhu Economic and Technological Development Zone, Wuhu City, Anhui Province

Patentee before: Wang Yonghui

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20160203

Termination date: 20210716