CN103418759A - Method with glass as covering heat preservation agent for vacuum nickel ingot casting and special mould - Google Patents

Method with glass as covering heat preservation agent for vacuum nickel ingot casting and special mould Download PDF

Info

Publication number
CN103418759A
CN103418759A CN2013103404337A CN201310340433A CN103418759A CN 103418759 A CN103418759 A CN 103418759A CN 2013103404337 A CN2013103404337 A CN 2013103404337A CN 201310340433 A CN201310340433 A CN 201310340433A CN 103418759 A CN103418759 A CN 103418759A
Authority
CN
China
Prior art keywords
ingot casting
nickel
glass
nickel ingot
die body
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN2013103404337A
Other languages
Chinese (zh)
Other versions
CN103418759B (en
Inventor
高骏
高盼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Baoji Hai Ji Titanium & Nickel Co Ltd
Original Assignee
Baoji Hai Ji Titanium & Nickel Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Baoji Hai Ji Titanium & Nickel Co Ltd filed Critical Baoji Hai Ji Titanium & Nickel Co Ltd
Priority to CN201310340433.7A priority Critical patent/CN103418759B/en
Publication of CN103418759A publication Critical patent/CN103418759A/en
Application granted granted Critical
Publication of CN103418759B publication Critical patent/CN103418759B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Abstract

The invention provides a method with glass as covering heat preservation agent for vacuum nickel ingot casting and a special mould. A glass ring is additionally arranged on the inner wall of a mould body, during the process of nickel ingot casting, the glass ring is melted by pouring liquid and floats on the liquid level of the nickel ingot casting pouring liquid, heat preservation effect is achieved on nickel metal liquid below, heat radiation on the surface of the nickel metal liquid is lowered, setting time of the metal liquid in a heat preservation cap is prolonged, so that the position of a finished product nickel ingot casting contraction hole is lifted to the top, finished product rate of nickel ingot casting is improved, and high practicability is achieved.

Description

Vacuum pouring nickel ingot casting is made method and the particular manufacturing craft of covering and heat insulating agent with glass
Technical field
The invention belongs to casting technology field, be specifically related to a kind of vacuum pouring nickel ingot casting and make method and the particular manufacturing craft of covering and heat insulating agent with glass.
Background technology
Nickel belongs to rare metal, very easily oxidized when high temperature, and under atmosphere, melting also is unfavorable for the discharge of the inner contained gas of raw material, therefore, when making the nickel ingot casting, need in vacuum induction melting furnace, carry out.Owing to casting under vacuum state, the heat at metal liquid top scatters and disappears very fast because of the heat radiation reason, can't carry out concurrent heating with riser compound etc. under vacuum state, ubiquity hot top top is cooled and solidified at first, the shrinkage cavity position formed is usually between hot top and ingot mould, the yield rate of ingot casting is lower, therefore, is necessary to seek more efficiently vacuum method.
Summary of the invention
The technical problem that the present invention solves: provide a kind of vacuum pouring nickel ingot casting to make method and the particular manufacturing craft of covering and heat insulating agent with glass, by on the die body inwall, setting up glass ring, in nickel ingot casting casting process, glass ring is melted by potting syrup and swims on nickel ingot casting potting syrup liquid level, nickel metal liquid below it is played to insulation, reduced the heat radiation on nickel metal liquid surface, extended the setting time of hot top inner metal liquid body, make the position of finished product nickel ingot casting shrinkage cavity to top lift, improved the yield rate of nickel ingot casting.
The technical solution used in the present invention: the method for glass covering and heat insulating agent for vacuum pouring nickel ingot casting comprises the steps:
1) 99.96% sheet nickel is put into to the crucible of vacuum induction melting furnace;
2) particular manufacturing craft that inwall is provided with to glass ring is put on the mold base of vacuum induction melting furnace;
3) close vacuum induction melting furnace, and be evacuated to and be not more than 10Pa;
4) connect intermediate frequency power supply, start melting, continue to be heated to 1520 ℃ and refining after sheet nickel dissolves 30 minutes;
5) by refining in crucible, good nickel metal liquid is poured in particular manufacturing craft, and along with the rising of nickel metal liquid liquid level, glass ring is melted and covers all the time the nickel solution top;
6) broken empty blow-on after 10 minutes, take out mould and continue cooling under atmosphere;
7) be cooled to below 300 ℃ take out the nickel ingot casting;
8) dispose the glass at nickel ingot casting top, obtain the nickel ingot casting that shrinkage cavity is positioned at hot top;
9) amputate rising head, the outer surface of car light nickel ingot casting, obtain the nickel ingot casting that yield rate is higher.
Above-mentioned particular manufacturing craft has die body and is placed in the hot top of die body upper surface, on described die body internal face, is fixed with glass ring.
Further, described glass ring is fixed in die body internal face top.
Further, described hot top internal diameter is less than the die body internal diameter.
The present invention compared with prior art by setting up glass ring on the die body inwall, in nickel ingot casting casting process, glass ring is melted by potting syrup and swims on nickel ingot casting potting syrup liquid level, nickel ingot casting potting syrup under it is played to the effect of insulation, thereby extended the setting time of upper metal liquid, at first metal liquid in die body is solidified, improve the internal soundness of nickel ingot casting, improved the yield rate of nickel ingot casting.
The accompanying drawing explanation
Fig. 1 is Special mould structure schematic diagram of the present invention.
The specific embodiment
Below in conjunction with Fig. 1, a kind of embodiment of the present invention is described.
Vacuum pouring nickel ingot casting is made the method for covering and heat insulating agent with glass, comprise the steps:
1) 99.96% sheet nickel is put into to the crucible of vacuum induction melting furnace;
2) particular manufacturing craft that inwall is provided with to glass ring is put on the mold base of vacuum induction melting furnace; Above-mentioned particular manufacturing craft has die body 1 and is placed in the hot top 2 of die body 1 upper surface, and described die body 1 internal face top is fixed with glass ring 3, and described hot top internal diameter is less than the die body internal diameter;
3) close vacuum induction melting furnace, and be evacuated to and be not more than 10Pa;
4) connect intermediate frequency power supply, start melting, continue to be heated to 1520 ℃ and refining after sheet nickel dissolves 30 minutes;
5) by refining in crucible, good nickel metal liquid is poured in particular manufacturing craft, and along with the rising of nickel metal liquid liquid level, glass ring is melted and covers all the time the nickel solution top;
6) broken empty blow-on after 10 minutes, take out mould and continue cooling under atmosphere;
7) be cooled to below 300 ℃ take out the nickel ingot casting;
8) dispose the glass at nickel ingot casting top, obtain the nickel ingot casting that shrinkage cavity is positioned at hot top;
9) amputate rising head, the outer surface of car light nickel ingot casting, obtain the nickel ingot casting that yield rate is higher.
The present invention by setting up glass ring on the die body inwall, in nickel ingot casting casting process, glass ring is melted by potting syrup and swims on nickel ingot casting potting syrup liquid level, nickel ingot casting potting syrup under it is played to the effect of insulation, reduced the heat radiation on nickel metal liquid surface, extended the setting time of hot top inner metal liquid body, make the position of finished product nickel ingot casting shrinkage cavity to top lift, improved the yield rate of nickel ingot casting.
Above-described embodiment, be preferred embodiment of the present invention, not is used for limiting the scope of the present invention, and the equivalence of being done with the described content of the claims in the present invention therefore all changes, within all should being included in the claims in the present invention scope.

Claims (4)

1. vacuum pouring nickel ingot casting is made the method for covering and heat insulating agent with glass, it is characterized in that comprising the steps:
1) 99.96% sheet nickel is put into to the crucible of vacuum induction melting furnace;
2) particular manufacturing craft that inwall is provided with to glass ring is put on the mold base of vacuum induction melting furnace;
3) close vacuum induction melting furnace, and be evacuated to and be not more than 10Pa;
4) connect intermediate frequency power supply, start melting, continue to be heated to 1520 ℃ and refining after sheet nickel dissolves 30 minutes;
5) by refining in crucible, good nickel metal liquid is poured in particular manufacturing craft, and along with the rising of nickel metal liquid liquid level, glass ring is melted and covers all the time the nickel solution top;
6) broken empty blow-on after 10 minutes, take out mould and continue cooling under atmosphere;
7) be cooled to below 300 ℃ take out the nickel ingot casting;
8) dispose the glass at nickel ingot casting top, obtain the nickel ingot casting that shrinkage cavity is positioned at hot top;
9) amputate rising head, the outer surface of car light nickel ingot casting, obtain the nickel ingot casting that yield rate is higher.
2. make the particular manufacturing craft of the method for covering and heat insulating agent with glass for vacuum pouring nickel ingot casting as claimed in claim 1, there is die body (1) and be placed in the hot top (2) of die body (1) upper surface, it is characterized in that: on described die body (1) internal face, be fixed with glass ring (3).
3. particular manufacturing craft according to claim 2, it is characterized in that: described glass ring (3) is fixed in die body (1) internal face top.
4. according to the described particular manufacturing craft of claim 2 or 3, it is characterized in that: described hot top (2) internal diameter is less than die body (1) internal diameter.
CN201310340433.7A 2013-08-06 2013-08-06 Method with glass as covering heat preservation agent for vacuum nickel ingot casting and special mould Active CN103418759B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310340433.7A CN103418759B (en) 2013-08-06 2013-08-06 Method with glass as covering heat preservation agent for vacuum nickel ingot casting and special mould

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310340433.7A CN103418759B (en) 2013-08-06 2013-08-06 Method with glass as covering heat preservation agent for vacuum nickel ingot casting and special mould

Publications (2)

Publication Number Publication Date
CN103418759A true CN103418759A (en) 2013-12-04
CN103418759B CN103418759B (en) 2015-05-20

Family

ID=49644426

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310340433.7A Active CN103418759B (en) 2013-08-06 2013-08-06 Method with glass as covering heat preservation agent for vacuum nickel ingot casting and special mould

Country Status (1)

Country Link
CN (1) CN103418759B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114888529A (en) * 2022-05-10 2022-08-12 安徽恒均粉末冶金科技股份有限公司 Preparation process of nickel strap for new energy power battery tab
CN115351245A (en) * 2022-07-27 2022-11-18 江苏远航精密合金科技股份有限公司 Method for improving yield of high-purity nickel ingot casting material for electronic industry

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2390500A (en) * 1942-07-30 1945-12-11 Ferro Eng Co Low volume sinkhead
US3262165A (en) * 1962-12-17 1966-07-26 Sandvikens Jernverks Ab Heat-insulating compositions and their use
JPS59163054A (en) * 1983-03-05 1984-09-14 Sumitomo Metal Ind Ltd Ingot making method of killed steel
JPS60158953A (en) * 1984-01-30 1985-08-20 Aichi Steel Works Ltd Riser holding plate for steel ingot
JPS632535A (en) * 1986-06-23 1988-01-07 Hitachi Ltd Production of steel ingot for forging
JPH09182939A (en) * 1995-12-28 1997-07-15 Nikko Kinzoku Kk Method for casting metallic ingot and casting device thereof
JP2005138173A (en) * 2003-11-10 2005-06-02 Sanyo Special Steel Co Ltd Ingot-making method reinforcing thermal-insulation in feeder head, and thermal-insulating box for this ingot-making
CN101101077A (en) * 2007-08-03 2008-01-09 攀钢集团攀枝花钢铁研究院 Rustless steel double-metal composite pipe and making method thereof
CN101596583A (en) * 2009-07-10 2009-12-09 攀枝花新钢钒股份有限公司 The compound centrifugal manufacturing method of axial sleeve of bushing
CN101678441A (en) * 2007-05-02 2010-03-24 Rti国际金属公司 Use the continuous casting of the reactive metal of glass coating
JP2012148293A (en) * 2011-01-18 2012-08-09 Hitachi Metals Ltd Method of casting ingot
CN102839299A (en) * 2012-08-17 2012-12-26 宝鸡海吉钛镍有限公司 Preparation method for pure nickel hollow blank for extruding pipe billet

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2390500A (en) * 1942-07-30 1945-12-11 Ferro Eng Co Low volume sinkhead
US3262165A (en) * 1962-12-17 1966-07-26 Sandvikens Jernverks Ab Heat-insulating compositions and their use
JPS59163054A (en) * 1983-03-05 1984-09-14 Sumitomo Metal Ind Ltd Ingot making method of killed steel
JPS60158953A (en) * 1984-01-30 1985-08-20 Aichi Steel Works Ltd Riser holding plate for steel ingot
JPS632535A (en) * 1986-06-23 1988-01-07 Hitachi Ltd Production of steel ingot for forging
JPH09182939A (en) * 1995-12-28 1997-07-15 Nikko Kinzoku Kk Method for casting metallic ingot and casting device thereof
JP2005138173A (en) * 2003-11-10 2005-06-02 Sanyo Special Steel Co Ltd Ingot-making method reinforcing thermal-insulation in feeder head, and thermal-insulating box for this ingot-making
CN101678441A (en) * 2007-05-02 2010-03-24 Rti国际金属公司 Use the continuous casting of the reactive metal of glass coating
CN101101077A (en) * 2007-08-03 2008-01-09 攀钢集团攀枝花钢铁研究院 Rustless steel double-metal composite pipe and making method thereof
CN101596583A (en) * 2009-07-10 2009-12-09 攀枝花新钢钒股份有限公司 The compound centrifugal manufacturing method of axial sleeve of bushing
JP2012148293A (en) * 2011-01-18 2012-08-09 Hitachi Metals Ltd Method of casting ingot
CN102839299A (en) * 2012-08-17 2012-12-26 宝鸡海吉钛镍有限公司 Preparation method for pure nickel hollow blank for extruding pipe billet

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114888529A (en) * 2022-05-10 2022-08-12 安徽恒均粉末冶金科技股份有限公司 Preparation process of nickel strap for new energy power battery tab
CN115351245A (en) * 2022-07-27 2022-11-18 江苏远航精密合金科技股份有限公司 Method for improving yield of high-purity nickel ingot casting material for electronic industry

Also Published As

Publication number Publication date
CN103418759B (en) 2015-05-20

Similar Documents

Publication Publication Date Title
US9393613B2 (en) Method for manufacturing hollow ingot for retaining ring of large generator by electroslag remelting
CN104402204B (en) A kind of silica crucible mould
CN103418759B (en) Method with glass as covering heat preservation agent for vacuum nickel ingot casting and special mould
CN111922322A (en) Directional solidification device and casting method
CN103691916A (en) Casting method for protecting thin-wall casting from local isolated hot spot shrinkage
CN109909479B (en) Short-process preparation method of bimetal composite wire
CN105642874A (en) Pouring technology for bearing alloy
CN109986056B (en) Low-pressure aluminum casting process method for cast aluminum rotor
CN102886496A (en) Casting feeding method and device
CN102179497B (en) Process for performing casting under negative pressure condition
CN102441932B (en) Method for eliminating inner core expansion force of fused zirconium-corundum perforated special-shaped brick die
CN204565093U (en) Insulated pouring case
CN102784895B (en) Casting device and manufacture method for columnar ingot
RU2007136689A (en) METHOD FOR PRODUCING GLASS AND DEVICE FOR FORMING GLASS
CN103691892A (en) Manufacturing method of high-temperature high-pressure drain valve
CN204035524U (en) A kind of device preparing high purity copper and copper alloy casting ingot
CN104174817B (en) A kind of ocean platform climb casting and the Technology for Heating Processing of machine Connection Block
CN207344795U (en) Fused cast refractories incubator
CN220113573U (en) Electric smelting brick mould convenient for stripping
CN203437601U (en) Die special for vacuum pouring of nickel ingot casting
CN220112284U (en) Alloy casting mold with ceramic lining
CN217492625U (en) Electromagnetic heating and water cooling dual-function casting mold
CN103949617A (en) Device and method for preparing high-purity copper and copper alloy ingot
CN217395240U (en) Improved casting AZS hook brick sand mould
CN105855519A (en) High-temperature alloy mould and casting and demoulding method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C53 Correction of patent of invention or patent application
CB02 Change of applicant information

Address after: 721013, Shaanxi City, Baoji province Weibin District Titanium City Road South (Hot Springs Village)

Applicant after: Baoji Hai Ji Titanium & Nickel Co., Ltd.

Address before: 721013, Shaanxi City, Xianyang province Weibin District Titanium City Road South (Hot Springs Village)

Applicant before: Baoji Hai Ji Titanium & Nickel Co., Ltd.

C14 Grant of patent or utility model
GR01 Patent grant