CN103393562B - 维生素洗发香波 - Google Patents
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- 239000002453 shampoo Substances 0.000 title claims abstract description 37
- 239000011782 vitamin Substances 0.000 title claims abstract description 21
- 229940088594 vitamin Drugs 0.000 title claims abstract description 21
- 229930003231 vitamin Natural products 0.000 title claims abstract description 21
- 235000013343 vitamin Nutrition 0.000 title claims abstract description 21
- 150000003722 vitamin derivatives Chemical class 0.000 title claims abstract description 21
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 27
- SNPLKNRPJHDVJA-UHFFFAOYSA-N dl-panthenol Chemical compound OCC(C)(C)C(O)C(=O)NCCCO SNPLKNRPJHDVJA-UHFFFAOYSA-N 0.000 claims abstract description 10
- 235000019489 Almond oil Nutrition 0.000 claims abstract description 9
- 239000008168 almond oil Substances 0.000 claims abstract description 9
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 230000002421 anti-septic effect Effects 0.000 claims description 17
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- DNKGZSOYWMQDTK-UHFFFAOYSA-N 3-iodoprop-1-ynyl N-butylcarbamate Chemical compound CCCCNC(=O)OC#CCI DNKGZSOYWMQDTK-UHFFFAOYSA-N 0.000 claims description 10
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims description 10
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 10
- 235000013824 polyphenols Nutrition 0.000 claims description 10
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 9
- 239000004330 calcium propionate Substances 0.000 claims description 9
- 235000010331 calcium propionate Nutrition 0.000 claims description 9
- 239000004302 potassium sorbate Substances 0.000 claims description 9
- 235000010241 potassium sorbate Nutrition 0.000 claims description 9
- 229940069338 potassium sorbate Drugs 0.000 claims description 9
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 8
- -1 amido propyl amine Chemical compound 0.000 claims description 8
- WGYKZJWCGVVSQN-UHFFFAOYSA-N mono-n-propyl amine Natural products CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 claims description 8
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 8
- 235000011152 sodium sulphate Nutrition 0.000 claims description 8
- 244000269722 Thea sinensis Species 0.000 claims description 7
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- 210000004209 hair Anatomy 0.000 abstract description 6
- 239000003755 preservative agent Substances 0.000 abstract description 6
- 230000002335 preservative effect Effects 0.000 abstract description 2
- 150000001412 amines Chemical class 0.000 abstract 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 abstract 1
- 235000011130 ammonium sulphate Nutrition 0.000 abstract 1
- 239000006260 foam Substances 0.000 abstract 1
- 229940051841 polyoxyethylene ether Drugs 0.000 abstract 1
- 229920000056 polyoxyethylene ether Polymers 0.000 abstract 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 4
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- OPVLOHUACNWTQT-UHFFFAOYSA-N azane;2-dodecoxyethyl hydrogen sulfate Chemical compound N.CCCCCCCCCCCCOCCOS(O)(=O)=O OPVLOHUACNWTQT-UHFFFAOYSA-N 0.000 description 2
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 description 2
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 description 2
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- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 2
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- 230000003648 hair appearance Effects 0.000 description 1
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- 239000003845 household chemical Substances 0.000 description 1
- ZCTXEAQXZGPWFG-UHFFFAOYSA-N imidurea Chemical compound O=C1NC(=O)N(CO)C1NC(=O)NCNC(=O)NC1C(=O)NC(=O)N1CO ZCTXEAQXZGPWFG-UHFFFAOYSA-N 0.000 description 1
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- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
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- CHHHXKFHOYLYRE-STWYSWDKSA-M potassium sorbate Chemical compound [K+].C\C=C\C=C\C([O-])=O CHHHXKFHOYLYRE-STWYSWDKSA-M 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
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- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
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- 239000000126 substance Substances 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
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Abstract
本发明公开了一种维生素洗发香波，由下述组分按重量百分比组成：月桂基聚氧乙烯醚硫酸铵8-12%，杏仁油酰胺丙基胺氧化物2-4%，丙二醇2-6%，DL-泛醇0.4-0.6%，防腐剂0.1-0.3%，余量为水。本发明的维生素洗发香波，泡沫丰富，能够显著改善头发的强度、弹性和健康状况。
Description
技术领域
本发明涉及一种洗发香波，具体涉及一种维生素洗发香波。
背景技术
洗发香波是人们日常生活中不可缺少的必需品，使用时能从头发及头皮中去除表面的油污和皮屑，而对头发、头皮和人身健康无不良影响。洗发香波种类繁多，按剂型和功能分主要有透明洗发香波、膏状洗发香波、珠光洗发香波、调理洗发香波、去屑洗发香波、专用洗发香波等。
近年来，由于人们生活品质的提高，洗发次数的增多，对洗发香波也提出了越来越多的要求。既需要洗发香波具有较好的去污去屑效果，又需要其具有较好的气味，同时还需要保持发质的光泽，具有较长的保质期。
为了延长洗发香波的保质期，使其在开封使用后长期放置仍不变质，通常会在洗发香波中加入一定量的防腐剂，但是目前市面上的洗发香波常用的高效防腐剂有对羟基苯甲酸甲酯(即尼泊金甲酯)、对羟基苯甲酸乙酯(即尼泊金乙酯)、苯甲酸钠、异噻唑啉酮等，它们对皮肤和眼睛都有一定的刺激性，在与眼睛接触后，需要立即用大量清水冲洗；甚至会引起部分人群皮肤过敏、发生皮炎等症状，因此其在洗发香波中的用量也受到严格的控制。
另外，咪唑烷基脲和已内酰脲作为防腐剂的原理均是作为甲醛供体，通过释放甲醛达到杀灭微生物的作用，当释放甲醛超标时也会对人体皮肤造成损害，在很多国家都是严格限制其含量甚至禁止使用的。
发明内容
针对现有技术中存在的上述不足，本发明所要解决的技术问题之一提供一种维生素洗发香波。
本发明目的是通过如下技术方案实现的：
一种维生素洗发香波，由下述组分按重量百分比组成：月桂基聚氧乙烯醚硫酸铵8-12％，杏仁油酰胺丙基胺氧化物2-4％，丙二醇2-6％，DL-泛醇0.4-0.6％，防腐剂0.1-0.2％，余量为水。
优选地，
所述防腐剂由下述组分按重量份组成：茶多酚10-15份，山梨酸钾10-15份，丙酸钙10-15份，丁基氨基甲酸碘代丙炔酯5-10份。
本发明中，
月桂基聚氧乙烯醚硫酸铵，英文名:Ammonium lauryl ether sulfate，CAS号：32612-48-9。
杏仁油酰胺丙基胺氧化物，CAS号：124046-20-4。
丙二醇，CAS号：26264-14-2。
DL-泛醇，CAS登录号：16485-10-2。
茶多酚，Tea Polyphenols，CAS号:84650-60-2。
山梨酸钾，CAS：24634-61-5。
丙酸钙，CAS号：4075-81-4。
丁基氨基甲酸碘代丙炔酯，CAS号：55406-53-6。
本发明的维生素洗发香波，泡沫丰富，能够显著改善头发的强度、弹性和健康状况。本发明的维生素洗发香波，选用茶多酚、山梨酸钾、丙酸钙和丁基氨基甲酸碘代丙炔酯的配伍制成的防腐剂，具有很好的协同增效的抑杀效果和安全性能。
具体实施方式
下面实施例是对本发明的进一步说明，而不是限制本发明的范围。在本发明中，如无特别说明，各原料均以有效物含量为100％计。
实施例1
一种维生素洗发香波，由下述组分按重量百分比组成：月桂基聚氧乙烯醚硫酸铵10％，杏仁油酰胺丙基胺氧化物3％，丙二醇4％，DL-泛醇0.5％，防腐剂0.2％，余量为水。
上述防腐剂，由下述组分按重量份组成：茶多酚10份、山梨酸钾10份、丙酸钙10份、丁基氨基甲酸碘代丙炔酯10份。将茶多酚、山梨酸钾、丙酸钙和丁基氨基甲酸碘代丙炔酯搅拌混合均匀，即可制成混合防腐剂。
取适量的水，加热至80-90℃，在搅拌过程中，按所述比例加入月桂基聚氧乙烯醚硫酸铵和杏仁油酰胺丙基胺氧化物，搅拌均匀后，降低温度至50-60℃，加入丙二醇、DL-泛醇和混合防腐剂，搅拌1.5小时后，冷却至室温，得到维生素洗发香波。
实施例2
一种维生素洗发香波，由下述组分按重量百分比组成：月桂基聚氧乙烯醚硫酸铵10％，杏仁油酰胺丙基胺氧化物3％，丙二醇4％，DL-泛醇0.5％，防腐剂0.2％，余量为水。
上述防腐剂，由下述组分按重量份组成：山梨酸钾20份、丙酸钙10份、丁基氨基甲酸碘代丙炔酯10份。
按实施例1的方法进行制备，得到维生素洗发香波。
实施例3
一种维生素洗发香波，由下述组分按重量百分比组成：月桂基聚氧乙烯醚硫酸铵10％，杏仁油酰胺丙基胺氧化物3％，丙二醇4％，DL-泛醇0.5％，防腐剂0.2％，余量为水。
上述防腐剂，由下述组分按重量份组成：茶多酚10份、丙酸钙20份、丁基氨基甲酸碘代丙炔酯10份。
按实施例1的方法进行制备，得到维生素洗发香波。
实施例4
一种维生素洗发香波，由下述组分按重量百分比组成：月桂基聚氧乙烯醚硫酸铵10％，杏仁油酰胺丙基胺氧化物3％，丙二醇4％，DL-泛醇0.5％，防腐剂0.2％，余量为水。
上述防腐剂，由下述组分按重量份组成：茶多酚20份、山梨酸钾10份、丁基氨基甲酸碘代丙炔酯10份。
按实施例1的方法进行制备，得到维生素洗发香波。
测试例
将实施例1-4的维生素洗发香波放入保温箱(40℃，95％湿度)，放置28天进行微生物挑战试验，选择胡梅，陈逸君的《复配化妆品防腐剂的增效作用》(《日用化学品科学》第29卷第12期,2006年12月)第4页表6的测试菌株，参照该文献2.3.2.3的评价标准，微生物挑战试验0天时，混合细菌和混合霉菌的初始菌株浓度均为5×105cfu/g(ml)。
表1：微生物挑战试验结果(cfu/g(ml))
由表1结果可见，实施例1的维生素洗发香波在试验28天后，使得混合细菌的菌株浓度都降至10cfu/g(ml)以下，证明其对细菌具有较强的抑杀作用。防腐效果明显优于实施例2-4。
因此选用了茶多酚、山梨酸钾、丙酸钙和丁基氨基甲酸碘代丙炔酯的配伍制成的防腐剂，具有很好的协同增效的抑杀效果，本发明选用此防腐剂制成的维生素洗发香波同时具有较好的防腐性和安全性能。
Claims (1)
1.一种维生素洗发香波，其特征在于，由下述组分按重量百分比组成：月桂基聚氧乙烯醚硫酸铵8-12％，杏仁油酰胺丙基胺氧化物2-4％，丙二醇2-6％，DL-泛醇0.4-0.6％，防腐剂0.1-0.2％，余量为水；
所述防腐剂由下述组分按重量份组成：茶多酚10-15份，山梨酸钾10-15份，丙酸钙10-15份，丁基氨基甲酸碘代丙炔酯5-10份。
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Non-Patent Citations (2)
| Title |
|---|
| 中华人民共和国卫生部.《表 4化妆品组分中限用防腐剂》.《化妆品卫生规范》.2007,第72页. * |
| 廖文胜.《加热保护香波》.《洗涤剂原料及配方精选》.化学工业出版社,2006,429-430. * |
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| ASS | Succession or assignment of patent right |
Owner name: ANHUI LIM KUM KEE FOODSTUFF CO., LTD. Free format text: FORMER OWNER: SHANGHAI YANZI CHEMICAL TECHNOLOGY CO., LTD. Effective date: 20141229 |
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| C41 | Transfer of patent application or patent right or utility model | ||
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Inventor after: Lin Mingchuan Inventor before: Chen Longdi |
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Free format text: CORRECT: INVENTOR; FROM: CHEN LONGDI TO: LIN MINGCHUAN Free format text: CORRECT: ADDRESS; FROM: 201111 MINHANG, SHANGHAI TO: 241000 WUHU, ANHUI PROVINCE |
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Effective date of registration: 20141229 Address after: The green food of Wuhu Economic Development Zone in Anhui province Wuhu City Sanshan District 241000 Applicant after: LIM KUM KEE FOODSTUFF Co.,Ltd. ANHUI Address before: 201111 Shanghai city Minhang District Yuanjiang Road No. 5500 building first room E2128 Applicant before: SHANGHAI YANZI CHEMICAL TECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20190925 Address after: 510000 No. 505, Fifth Floor, C District, Cross-Strait (Huilong) Information Industry Science and Technology Park, No. 8, Helong Street, Baiyun District, Guangzhou City, Guangdong Province Patentee after: Guangzhou Yuanshangcao Biotechnology Co.,Ltd. Address before: The green food of Wuhu Economic Development Zone in Anhui province Wuhu City Sanshan District 241000 Patentee before: LIM KUM KEE FOODSTUFF Co.,Ltd. ANHUI |
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| CP01 | Change in the name or title of a patent holder | ||
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Address after: No.505, 5th floor, Zone C, cross strait (Huilong) information industry science and Technology Park, No.8 Helong Road, Helong street, Baiyun District, Guangzhou, Guangdong 510000 Patentee after: Guangdong Yikangyuan Pharmaceutical Biotechnology Co.,Ltd. Address before: No.505, 5th floor, Zone C, cross strait (Huilong) information industry science and Technology Park, No.8 Helong Road, Helong street, Baiyun District, Guangzhou, Guangdong 510000 Patentee before: Guangzhou Yuanshangcao Biotechnology Co.,Ltd. |