CN103387216B - With TiOSO 4the method that titanium source and carbon source prepare TiCN powder is respectively with starch - Google Patents
With TiOSO 4the method that titanium source and carbon source prepare TiCN powder is respectively with starch Download PDFInfo
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- CN103387216B CN103387216B CN201310320085.7A CN201310320085A CN103387216B CN 103387216 B CN103387216 B CN 103387216B CN 201310320085 A CN201310320085 A CN 201310320085A CN 103387216 B CN103387216 B CN 103387216B
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- 239000000843 powder Substances 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims abstract description 25
- 229920002472 Starch Polymers 0.000 title claims abstract description 10
- 239000008107 starch Substances 0.000 title claims abstract description 10
- 235000019698 starch Nutrition 0.000 title claims abstract description 10
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title abstract description 14
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract description 12
- 239000010936 titanium Substances 0.000 title abstract description 12
- 229910052719 titanium Inorganic materials 0.000 title abstract description 12
- 229910052799 carbon Inorganic materials 0.000 title abstract description 9
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 238000002360 preparation method Methods 0.000 claims abstract description 10
- 238000005516 engineering process Methods 0.000 claims abstract description 8
- 239000000203 mixture Substances 0.000 claims abstract description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000012298 atmosphere Substances 0.000 claims abstract description 5
- 239000008367 deionised water Substances 0.000 claims abstract description 4
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 4
- 239000004615 ingredient Substances 0.000 claims abstract description 4
- 239000011259 mixed solution Substances 0.000 claims abstract description 4
- 239000012299 nitrogen atmosphere Substances 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 3
- 230000015572 biosynthetic process Effects 0.000 abstract description 3
- 239000013064 chemical raw material Substances 0.000 abstract description 3
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 3
- 238000003786 synthesis reaction Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 229910010413 TiO 2 Inorganic materials 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 150000003609 titanium compounds Chemical class 0.000 description 1
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- Carbon And Carbon Compounds (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
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Application Number | Priority Date | Filing Date | Title |
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CN201310320085.7A CN103387216B (en) | 2013-07-28 | 2013-07-28 | With TiOSO 4the method that titanium source and carbon source prepare TiCN powder is respectively with starch |
Applications Claiming Priority (1)
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CN201310320085.7A CN103387216B (en) | 2013-07-28 | 2013-07-28 | With TiOSO 4the method that titanium source and carbon source prepare TiCN powder is respectively with starch |
Publications (2)
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CN103387216A CN103387216A (en) | 2013-11-13 |
CN103387216B true CN103387216B (en) | 2016-03-02 |
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CN201310320085.7A Active CN103387216B (en) | 2013-07-28 | 2013-07-28 | With TiOSO 4the method that titanium source and carbon source prepare TiCN powder is respectively with starch |
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Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115872443A (en) * | 2021-09-29 | 2023-03-31 | 溧阳天目先导电池材料科技有限公司 | Preparation method of nano titanium oxide and nano titanium oxide prepared by same |
CN115872369A (en) * | 2021-09-29 | 2023-03-31 | 溧阳天目先导电池材料科技有限公司 | Preparation method of nano titanium nitride and prepared nano titanium nitride |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101462722A (en) * | 2009-01-09 | 2009-06-24 | 北京科技大学 | Method for preparing titanium carbide ceramic powder |
CN101863663A (en) * | 2010-07-15 | 2010-10-20 | 武汉工程大学 | Combustion method for preparing submicron grade titanium carbide polycrystal powder |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103130506B (en) * | 2013-03-15 | 2014-07-09 | 长沙伟徽高科技新材料股份有限公司 | Method for preparing superfine titanium carbonitride |
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2013
- 2013-07-28 CN CN201310320085.7A patent/CN103387216B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101462722A (en) * | 2009-01-09 | 2009-06-24 | 北京科技大学 | Method for preparing titanium carbide ceramic powder |
CN101863663A (en) * | 2010-07-15 | 2010-10-20 | 武汉工程大学 | Combustion method for preparing submicron grade titanium carbide polycrystal powder |
Non-Patent Citations (4)
Title |
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Carbothermal Reduction Synthesis of Superfined TiC Powders From TiOSO4;Jie Li;《Advanced Materials Research》;20111218;第415-417卷;510-513 * |
NaBr-KCl和不同炭源对合成Ti(C,N)粉末的影响;陈希来等;《耐火材料》;20070630;第41卷(第6期);413-416 * |
以酚醛树脂为碳源碳热还原制备TiC的研究;李鹏飞等;《硅酸盐通报》;20121031;第31卷(第5期);1312-1316 * |
高钛渣提取碳氮化钛的研究;李慈颖等;《钢铁钒钛》;20060930;第7页右栏第2段以及第2.2节 * |
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Effective date of registration: 20240425 Address after: 541199 Baoshan High end Equipment Intelligent Manufacturing Industrial Park (Phase I), Lingui District, Guilin City, Guangxi Zhuang Autonomous Region Plant 1 and 2 Patentee after: GUILIN GUIYE HEAVY INDUSTRIES CO.,LTD. Country or region after: China Address before: 541004 the Guangxi Zhuang Autonomous Region Guilin Construction Road No. 12 Patentee before: GUILIN University OF TECHNOLOGY Country or region before: China |
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Effective date of registration: 20240603 Address after: 541199 Baoshan Industrial Park plot in Liangjiang Town, Lingui District, Guilin City, Guangxi Zhuang Autonomous Region (limited to industrial business activities only); 2 Yaohui, No. 2 Xicheng North Road, Lingui Town, Lingui District, No. 01, 4th to 6th floors, Building 2, Beautiful Home Patentee after: Guilin Guiye High Temperature and High Pressure Machinery Co.,Ltd. Country or region after: China Address before: 541199 Baoshan High end Equipment Intelligent Manufacturing Industrial Park (Phase I), Lingui District, Guilin City, Guangxi Zhuang Autonomous Region Plant 1 and 2 Patentee before: GUILIN GUIYE HEAVY INDUSTRIES CO.,LTD. Country or region before: China |