CN103386208A - Novel tower distillation system - Google Patents

Novel tower distillation system Download PDF

Info

Publication number
CN103386208A
CN103386208A CN2012101448124A CN201210144812A CN103386208A CN 103386208 A CN103386208 A CN 103386208A CN 2012101448124 A CN2012101448124 A CN 2012101448124A CN 201210144812 A CN201210144812 A CN 201210144812A CN 103386208 A CN103386208 A CN 103386208A
Authority
CN
China
Prior art keywords
tower
destilling tower
distillation
novel
condenser
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2012101448124A
Other languages
Chinese (zh)
Inventor
肖世才
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sichuan Huili Industrial Co Ltd
Original Assignee
Sichuan Huili Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sichuan Huili Industrial Co Ltd filed Critical Sichuan Huili Industrial Co Ltd
Priority to CN2012101448124A priority Critical patent/CN103386208A/en
Publication of CN103386208A publication Critical patent/CN103386208A/en
Pending legal-status Critical Current

Links

Images

Abstract

The invention discloses a novel tower distillation system. The novel tower distillation system comprises a distillation tower, a heating tube is arranged in the distillation tower, a condenser is arranged in the distillation tower, a collection bottle is arranged outside the distillation tower, and the collection bottle is connected with the internal of the distillation tower. The distillation system has the advantages of simple structure, simple principle, few needed apparatuses, rapid distillation, stable quality of the obtained distilled product, satisfying of the needs of subsequent production processes, and production cost reduction.

Description

A kind of novel tower-type Distallation systm
Technical field
The present invention relates to a kind of Distallation systm, especially relate to a kind of novel tower-type Distallation systm, belong to the fields such as pharmacy, chemical industry.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, and it utilizes each component boiling point difference in mixing material or liquid-solid system, makes the low boiling component evaporation, then condensation is the associating of evaporation and two kinds of unit operations of condensation to separate the unit process of whole component.With other separation means, wait and compare as extraction, its advantage is need not use system components other solvent in addition, thereby guarantees can not introduce new impurity.The mass transport process that refers to utilize the difference of each component volatilization in liquid mixture and component is separated.The steam that liquid boiling is produced imports condenser pipe, makes it cooling a kind of evaporation of liquid, the process of condensation of condensing into.Distillation is a kind of important operating technology of separating mixture, especially the separation for liquid mixture has important Practical significance to utilize the difference of each component volatilization degree in liquid mixture, liquid mixture partly vaporized and make the vapor portion condensation thereupon, thereby realizing the separation of its contained component.It is a kind of unit operations that mass transfer separates that belongs to.Be widely used in the fields such as oil refining, chemical industry, light industry.
Its principle is to separate the bi-component mixed liquor as example.It is partly vaporized the feed liquid heating, volatile components obtains enrichment in steam, and difficult volatile component also obtains enrichment in raffinate, and this has realized the separation of two components to a certain extent.The volatilization ability of two components differs larger, and above-mentioned enrichment degree is also larger.In industrial rectifying device, the liquid phase of part vaporization is directly contacted with the gas phase of partial condensation, to carry out the vapour-liquid interphase mass transfer, result is that the difficult volatile component in gas phase partly changes liquid phase over to, volatile components in liquid phase partly changes gas phase over to, has also namely realized simultaneously the part vaporization of liquid phase and the partial condensation of vapour phase.
The molecule of liquid has the tendency of from surface, overflowing due to molecular motion.This tendency increases along with the rising of temperature.If liquid is placed in airtight vacuum systems, fluid molecule overflows with keeping and forms steam on liquid level top, and the speed that makes finally molecule be overflowed by liquid is equated by the speed of getting back to liquid in steam with molecule, the pressure that the steam maintenance is certain.Steam on liquid level reaches capacity at this moment, is called saturated vapor, and the pressure that it is executed liquid level is called saturated vapour pressure.The saturated vapour pressure that experiment showed, liquid is only relevant with temperature, and namely liquid has certain vapour pressure at a certain temperature.Pressure when this refers to liquid and its balance of steam, irrelevant with the absolute magnitude of liquid in system and steam.At chemical process, need to distill material, traditional distillation equipment is because its efficiency is low, causes distilling the material mass that obtains unstable, affects follow-up production process.
Summary of the invention
The object of the invention is to overcome the shortcoming and defect of above-mentioned prior art, a kind of novel tower-type Distallation systm is provided, this Distallation systm simple in structure, principle is easy, need the equipment that uses few, can reach rapidly the purpose of distillation, the steady quality of the product that distills out, can meet the needs of subsequent production process, reduce production cost.
Purpose of the present invention is achieved through the following technical solutions: a kind of novel tower-type Distallation systm, comprise destilling tower, be provided with heating tube in described destilling tower, be provided with condenser in described destilling tower, destilling tower is outside equipped with receiving flask, described receiving flask and destilling tower internal communication.
The place of described receiving flask and destilling tower internal communication is provided with collector and every the foam device, the described below that is arranged on collector every the foam device.
Be provided with the water level pipe that communicates with destilling tower inside on the outer wall of described destilling tower.
Described condenser is arranged on the top of destilling tower inside.
Be provided with cooling water inlet and coolant outlet on the outer wall of described destilling tower, described cooling water inlet and coolant outlet all communicate with condenser.
Be provided with the filling opening that communicates with its inside on described destilling tower.
In sum, the invention has the beneficial effects as follows: this Distallation systm simple in structure, principle is easy, need the equipment that uses few, can reach rapidly the purpose of distillation, the steady quality of the product that distills out, can meet the needs of subsequent production process, reduce production cost.
Description of drawings
Fig. 1 is structural representation of the present invention.
Mark and corresponding parts title in accompanying drawing: 1-heating tube; 2-destilling tower; 3-receiving flask; 4-condenser; 5-cooling water inlet; 6-coolant outlet; 7-collector; 8-every the foam device; 9-filling opening; 10-water level pipe.
The specific embodiment
Below in conjunction with embodiment and accompanying drawing, the present invention is described in further detail, but embodiments of the present invention are not limited only to this.
Embodiment:
As shown in Figure 1, a kind of novel tower-type Distallation systm, comprise destilling tower 2, is provided with heating tube 1 in described destilling tower 2, is provided with condenser 4 in described destilling tower 2, and destilling tower 2 is outside equipped with receiving flask 3, described receiving flask 3 and destilling tower 2 internal communication.Collect by receiving flask 3 liquid that condenser 4 condensations are got off.
The place of described receiving flask 3 and destilling tower 2 internal communication is provided with collector 7 and every foam device 8, the described below that is arranged on collector 7 every foam device 8.Solution is after heating tube 1 heating, inner material produces evaporation, after condenser 4 condensations on top, becoming liquid is collected by collector 7, then flow in receiving flask 3 by pipeline, the foam that intercepts in heating process every foam device 8 enters into destilling tower 2 the first half, in order to avoid the effect of impact evaporation.
Be provided with the water level pipe 10 that communicates with destilling tower inside on the outer wall of described destilling tower 2.Observe at any time the position of solution in destilling tower 2 by water level pipe 10, keep the height of the height of solution higher than heating tube 1, to avoid security incident.
Described condenser 4 is arranged on the top of destilling tower 2 inside.Can distill better.
Be provided with cooling water inlet 5 and coolant outlet 6 on the outer wall of described destilling tower 2, described cooling water inlet 5 and coolant outlet 6 all communicate with condenser 4.By cooling water inlet 5 and coolant outlet 6, continue to pass into cooling water in condenser 4, keep the working effect of condenser 4.
Be provided with the filling opening 9 that communicates with its inside on described destilling tower 2.Add solution by filling opening 9 in destilling tower 2, guarantee the continuity of distillation.Filling opening 9 should be arranged on the middle and upper part of destilling tower 2 simultaneously, adds more easily solution.
Take aforesaid way, just can realize preferably the present invention.

Claims (6)

1. novel tower-type Distallation systm, it is characterized in that: comprise destilling tower (2), be provided with heating tube (1) in described destilling tower (2), be provided with condenser (4) in described destilling tower (2), destilling tower (2) is outside equipped with receiving flask (3), described receiving flask (3) and destilling tower (2) internal communication.
2. a kind of novel tower-type Distallation systm as claimed in claim 1, it is characterized in that: the place of described receiving flask (3) and destilling tower (2) internal communication is provided with collector (7) and every foam device (8), the described below that is arranged on collector (7) every foam device (8).
3. a kind of novel tower-type Distallation systm as claimed in claim 2, is characterized in that: be provided with the water level pipe (10) that communicates with destilling tower (2) inside on the outer wall of described destilling tower (2).
4. a kind of novel tower-type Distallation systm as claimed in claim 3 is characterized in that: described condenser (4) is arranged on the inner top of destilling tower (2).
5. a kind of novel tower-type Distallation systm as claimed in claim 4, it is characterized in that: be provided with cooling water inlet (5) and coolant outlet (6) on the outer wall of described destilling tower (2), described cooling water inlet (5) and coolant outlet (6) all communicate with condenser (4).
6. a kind of novel tower-type Distallation systm as described in any one in claim 1 to 5, is characterized in that: be provided with the filling opening (9) that communicates with its inside on described destilling tower (2).
CN2012101448124A 2012-05-11 2012-05-11 Novel tower distillation system Pending CN103386208A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012101448124A CN103386208A (en) 2012-05-11 2012-05-11 Novel tower distillation system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012101448124A CN103386208A (en) 2012-05-11 2012-05-11 Novel tower distillation system

Publications (1)

Publication Number Publication Date
CN103386208A true CN103386208A (en) 2013-11-13

Family

ID=49530738

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2012101448124A Pending CN103386208A (en) 2012-05-11 2012-05-11 Novel tower distillation system

Country Status (1)

Country Link
CN (1) CN103386208A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3937109A1 (en) * 1989-11-07 1991-05-08 Bela Medvey Distn. of liq. contg. surfactants heated by microwaves - to counter bubble and froth formation
CN101108281A (en) * 2006-07-17 2008-01-23 蒋建君 Distillation equipment of conical baffled evaporator
CN201356988Y (en) * 2009-01-20 2009-12-09 沂南县天成生物制品有限公司 Energy-saving type alcohol recovery tower
CN201959583U (en) * 2011-03-12 2011-09-07 倪建英 Alcohol recovery tower
CN202569605U (en) * 2012-05-11 2012-12-05 四川汇利实业有限公司 Novel tower-type distillation system

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3937109A1 (en) * 1989-11-07 1991-05-08 Bela Medvey Distn. of liq. contg. surfactants heated by microwaves - to counter bubble and froth formation
CN101108281A (en) * 2006-07-17 2008-01-23 蒋建君 Distillation equipment of conical baffled evaporator
CN201356988Y (en) * 2009-01-20 2009-12-09 沂南县天成生物制品有限公司 Energy-saving type alcohol recovery tower
CN201959583U (en) * 2011-03-12 2011-09-07 倪建英 Alcohol recovery tower
CN202569605U (en) * 2012-05-11 2012-12-05 四川汇利实业有限公司 Novel tower-type distillation system

Similar Documents

Publication Publication Date Title
JP5793157B2 (en) Solution processing equipment
CN103408514A (en) Technique and device for recovering tetrahydrofuran by pervaporation method
CN105152860B (en) A kind of method of the refined mixed alcohol of rectifying pervaporation coupling technique
CN103508847A (en) Method and device for recycling high-purity butyl alcohol by dehydrating butyl alcohol
CN101700916B (en) Process and system for treating industrial normal propyl alcohol waste liquor
CN104610018B (en) Method for separating ethanol fermentation liquid
CN109745723A (en) A kind of double tower continuous feeding distillation system and control method
CN202569605U (en) Novel tower-type distillation system
CN103613480B (en) Device and method for recycling low-concentration organic solvent
CN205391768U (en) Three -dimensional atmospheric and vacuum distillation solvent purification distillation plant
CN104447267B (en) A kind of Separation of Benzene ethyl ketone, method of alpha-phenyl ethyl alcohol from 1-Phenylethanone. and alpha-phenyl ethyl alcohol mixture
CN107998677B (en) Environment-friendly cleaning device and process method for solvent recovery
CN106512463A (en) Gas and liquid separation device of rectifying tower
CN203128466U (en) Device for removing micromolecules in polysiloxane
CN103386208A (en) Novel tower distillation system
CN104341268B (en) A kind of alcohol fuel continuous dehydration method
CN104693005A (en) New process for separating methanol-propyl formate azeotrope through extractive distillation
CN113354605B (en) Separation device and process for maleic anhydride hydrogenation product
CN102698569B (en) Negative pressure-type recovery device for methanol and process for negative pressure-type recovery device
CN209645878U (en) Aqueous organic liquid waste and organic solvent separation and recovery system
CN105617703A (en) Heat pump distillation system in chemical industry
CN208911494U (en) The two tower multifunctional solvent recyclable devices for Alcohol Production
CN103897803B (en) Biofuel purifying technique and system
CN206334377U (en) A kind of gas-liquid separation device of rectifying column
CN207108876U (en) A kind of separation butyraldehyde, ethanol, the device of aqueous mixtures

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C12 Rejection of a patent application after its publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20131113