CN103381636A - Production process for cleaning-free butyl rubber plug - Google Patents
Production process for cleaning-free butyl rubber plug Download PDFInfo
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- CN103381636A CN103381636A CN201210136805XA CN201210136805A CN103381636A CN 103381636 A CN103381636 A CN 103381636A CN 201210136805X A CN201210136805X A CN 201210136805XA CN 201210136805 A CN201210136805 A CN 201210136805A CN 103381636 A CN103381636 A CN 103381636A
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- butyl rubber
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Abstract
The invention relates to a production process for a cleaning-free butyl rubber plug. The production process comprises the following steps: a, preparation of a raw material, i.e., a semi-finished product after 100% self-inspection; b, pre-cleaning; c, removal of rubber edges, rubber threads and rubber scraps; and d, refined cleaning: a step of cleaning by using a butyl rubber cleaning machine. The concrete process of the step d comprises: 1, spraying and rough cleaning; 2, primary cleaning; 3, secondary cleaning; 4, tertiary cleaning; 5, refined cleaning; 6, siliconization; 7, flushing; 8, steam sterilization and vacuum drying; 9, hot air sterilization and vacuum drying; 10, cooling; 11, inspection; and 12, packaging of qualified products with sterilizable bags. The production process provided by the invention is capable of realizing mass production of the cleaning-free butyl rubber plug.
Description
Technical field
The present invention relates to a kind of production technology of disposable butyl rubber plug.
Background technology
Common butyl rubber plug all will clean before using, technical development along with the butyl rubber plug industry, the non-i.e. product of use of washing is brought into use in increasing pharmaceutical factory, this product can reduce pharmaceutical factory some links in use, thereby greatly enhance productivity, in the case, (formula subject to sterilization) disposable butyl rubber plug arises at the historic moment.Disposable butyl rubber plug is easy to use because of it, the pharmaceutical factory use of can directly sterilizing, become the bright spot of present butyl rubber plug industry development, but because its inherent quality is had relatively high expectations, domestic can't putting into production in enormous quantities, need plug manufacturer to strengthen research and development capabilities, control from endogenous and external factor, make the disposable butyl rubber plug that suitable explained hereafter goes out to meet the pharmaceutical factory demand.
Summary of the invention
The objective of the invention is to overcome the defective that prior art exists, a kind of production technology that can produce disposable butyl rubber plug in enormous quantities is provided.
The technical solution adopted for the present invention to solve the technical problems is: a kind of production technology of disposable butyl rubber plug has following processing step:
A, preparation raw material: the semi-finished product after 100% self check;
B, prerinse;
C, except remove photoresist limit, collodion silk and buffings;
D, fine purifiation: use the butyl rubber cleaning machine to clean, detailed process: 1, spray is slightly washed; 2, once clean; 3, secondary cleaning; 4, clean for three times; 5, fine purifiation; 6, silication; 7, rinse; 8, steam sterilizing vacuum drying; 9, hot air sterilization vacuum drying; 10, cooling; 11, check; 12, but certified products are packed with sterilizing bag.
Further, in the process 1 of described steps d, spray time of slightly washing is 1000s, water temperature 〉=80 ℃; The time of once cleaning in process 2 is 1000s, water temperature 〉=80 ℃; In process 3, the time of secondary cleaning is 1000s, water temperature 〉=80 ℃; The time that in process 4, three times are cleaned is 500s, water temperature 〉=80 ℃; In process 5, the time of fine purifiation is 1500s, water temperature 〉=80 ℃; In process 6, the time of silication is 1000s, water temperature 〉=70 ℃; The time of rinsing in process 7 is 500s.Vacuum drying time 〉=the 30min of steam sterilizing in process 8, temperature is 121 ℃; Vacuum drying time 〉=the 30min of hot air sterilization in process 9, temperature is 121 ℃.
Further, the water temperature in the process 1～6 of described steps d is 90 ℃.
Beneficial effect of the present invention: adopt the butyl rubber plug of this explained hereafter to need not again to clean, but and Mass production, product is easy to use, and the pharmaceutical factory use of can directly sterilizing has improved production efficiency greatly.
The specific embodiment
A kind of production technology of disposable butyl rubber plug has following processing step:
A, preparation raw material: the semi-finished product after 100% self check;
B, prerinse;
C, except remove photoresist limit, collodion silk and buffings;
D, fine purifiation: use the butyl rubber cleaning machine to clean, it removes remaining glue limit, buffings and the colloid institute static electrification in plug surface own and the fiber dust that adsorbs, reduces the surface tension of plug, and detailed process: 1, spray is slightly washed, time is 1000s, water temperature 〉=80 ℃; 2, once clean, the time is 1000s, water temperature 〉=80 ℃; 3, secondary cleaning, the time is 1000s, water temperature 〉=80 ℃; 4, clean for three times, the time is 500s,, water temperature 〉=80 ℃; 5, fine purifiation, the time is 1500s, water temperature 〉=80 ℃; 6, silication, the time is 1000s, water temperature 〉=70 ℃; 7, rinse, the time is 500s; 8, steam sterilizing vacuum drying, time 〉=30min, temperature is 121 ℃; 9, hot air sterilization vacuum drying, time 〉=30min, temperature is 121 ℃; 10, cooling; 11, check; 12, but certified products are packed with sterilizing bag.The preferred embodiment of this technique: the water temperature in the process 1～6 of steps d is 90 ℃; Adopt the wet method edge-removing process in step c, avoid more burr, collodion silk and buffings to produce.
Produce the quality requirement of disposable butyl rubber plug: the formula of producing disposable butyl rubber plug should consider that the endogenous particulate matter is few, to clean with the water that meets the water for injection quality requirement, the product that washes out should strict control of heat source, particulate and bacterial load, but to pack with sterilized packing bag, be convenient to the pharmaceutical factory and directly carry out moise-heat sterilization.
Should be appreciated that specific embodiment described above only is used for explaining the present invention, be not intended to limit the present invention.The apparent variation of being extended out by spirit of the present invention or change still are among protection scope of the present invention.
Claims (3)
1. the production technology of a disposable butyl rubber plug is characterized in that having following processing step:
A, preparation raw material: the semi-finished product after 100% self check;
B, prerinse;
C, except remove photoresist limit, collodion silk and buffings;
D, fine purifiation: use the butyl rubber cleaning machine to clean, detailed process: 1, spray is slightly washed; 2, once clean; 3, secondary cleaning; 4, clean for three times; 5, fine purifiation; 6, silication; 7, rinse; 8, steam sterilizing vacuum drying; 9, hot air sterilization vacuum drying; 10, cooling; 11, check; 12, but certified products are packed with sterilizing bag.
2. the production technology of disposable butyl rubber plug according to claim 1 is characterized in that: the time that in the process 1 of described steps d, spray is slightly washed is 1000s, water temperature 〉=80 ℃; The time of once cleaning in process 2 is 1000s, water temperature 〉=80 ℃; In process 3, the time of secondary cleaning is 1000s, water temperature 〉=80 ℃; The time that in process 4, three times are cleaned is 500s, water temperature 〉=80 ℃; In process 5, the time of fine purifiation is 1500s, water temperature 〉=80 ℃; In process 6, the time of silication is 1000s, water temperature 〉=70 ℃; The time of rinsing in process 7 is 500s.Vacuum drying time 〉=the 30min of steam sterilizing in process 8, temperature is 121 ℃; Vacuum drying time 〉=the 30min of hot air sterilization in process 9, temperature is 121 ℃.
3. the production technology of disposable butyl rubber plug according to claim 2, it is characterized in that: the water temperature in the process 1～6 of described steps d is 90 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210136805.XA CN103381636B (en) | 2012-05-04 | 2012-05-04 | The production technology of cleaning-free butyl rubber plug |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210136805.XA CN103381636B (en) | 2012-05-04 | 2012-05-04 | The production technology of cleaning-free butyl rubber plug |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103381636A true CN103381636A (en) | 2013-11-06 |
| CN103381636B CN103381636B (en) | 2016-01-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210136805.XA Active CN103381636B (en) | 2012-05-04 | 2012-05-04 | The production technology of cleaning-free butyl rubber plug |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110694996A (en) * | 2019-10-16 | 2020-01-17 | 湖北华强科技有限责任公司 | Cleaning process of butyl rubber plug with high cleanliness |
| CN114748652A (en) * | 2022-05-20 | 2022-07-15 | 河南海康生物科技有限公司 | Production process of cleaning product |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4074654A (en) * | 1976-01-06 | 1978-02-21 | Takeda Chemical Industries, Ltd. | Automatic closure cleansing and coating machine |
| JP2003062037A (en) * | 2001-08-23 | 2003-03-04 | Daikyo Seiko Ltd | Manufacturing method of rubber stopper for medicine/ medical goods |
| CN1586739A (en) * | 2004-09-30 | 2005-03-02 | 江阴兰陵瓶塞有限公司 | Medical rubber stopper cleaner |
-
2012
- 2012-05-04 CN CN201210136805.XA patent/CN103381636B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4074654A (en) * | 1976-01-06 | 1978-02-21 | Takeda Chemical Industries, Ltd. | Automatic closure cleansing and coating machine |
| JP2003062037A (en) * | 2001-08-23 | 2003-03-04 | Daikyo Seiko Ltd | Manufacturing method of rubber stopper for medicine/ medical goods |
| CN1586739A (en) * | 2004-09-30 | 2005-03-02 | 江阴兰陵瓶塞有限公司 | Medical rubber stopper cleaner |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110694996A (en) * | 2019-10-16 | 2020-01-17 | 湖北华强科技有限责任公司 | Cleaning process of butyl rubber plug with high cleanliness |
| CN110694996B (en) * | 2019-10-16 | 2022-02-01 | 湖北华强科技股份有限公司 | Cleaning process of butyl rubber plug with high cleanliness |
| CN114748652A (en) * | 2022-05-20 | 2022-07-15 | 河南海康生物科技有限公司 | Production process of cleaning product |
| CN114748652B (en) * | 2022-05-20 | 2024-04-26 | 河南海康生物科技有限公司 | Production process of cleaning product |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103381636B (en) | 2016-01-06 |
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