CN103359779B - Method for preventing calcium, magnesium and iron adhesion blockage at top of chlorination furnace during production of titanium tetrachloride - Google Patents
Method for preventing calcium, magnesium and iron adhesion blockage at top of chlorination furnace during production of titanium tetrachloride Download PDFInfo
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- CN103359779B CN103359779B CN201310263836.6A CN201310263836A CN103359779B CN 103359779 B CN103359779 B CN 103359779B CN 201310263836 A CN201310263836 A CN 201310263836A CN 103359779 B CN103359779 B CN 103359779B
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Abstract
The invention discloses a method for preventing calcium, magnesium and iron adhesion blockage at the top of a chlorination furnace during the production of titanium tetrachloride. According to the method, an outlet pipeline arranged at the top of the chlorination furnace is connected with a second gas pipeline (5); the second gas pipeline is connected with a lower end flange of a four-way pipe (1) through a flange; an upper end flange of the four-way pipe is connected with an inverted conical dust collection hood (2) through an upper end gate valve; a left end or right end flange of the four-way pipe is connected with a first gas pipeline (4) through a first gate valve; the right end or left end of the four-way pipe is closed or opened through a side end gate valve and can be connected with a standby pipeline; a pressure balancing pipe (3) is connected between the dust collection hood and the first gas pipeline; and the process of cleaning the dust collection hood or the first gas pipeline does not influence the normal discharging of chloride impurity gas by the second gas pipeline, so that the outlet pipeline arranged at the top of the chlorination furnace surely can normally discharge the chloride impurity gas during the production of titanium tetrachloride, and blockage is not generated. The method disclosed by the invention has the characteristics of simplicity and practicability.
Description
Technical field
The invention belongs to chlorination furnace technical field, refer more particularly to the anti-calcium of chlorination furnace roof, magnesium, iron in a kind of titanium tetrachloride production and adhere to the method for stopping up.
Background technology
Titanium tetrachloride production and application chlorination furnace, its gaseous reaction products is discharged from the outlet conduit of furnace roof, and in the reaction product of gaseous state, can carry secretly as calcium, magnesium, the formed chloride impurity of iron, these calcium, magnesium, iron contamination can stick on the inwall of described outlet conduit, along with the chlorination furnace prolongation of duration of service, calcium, magnesium, the semi-invariant that iron contamination adheres to will get more and more, cause described outlet conduit internal diameter diminish and make its obstruction, when serious, can cause chlorination furnace to be forced to stop produce, stopping production can affecting the production declining of titanium tetrachloride, and on also producing certain impact the work-ing life of chlorination furnace and auxiliary facility thereof, mixed economy loss is larger.
Summary of the invention
For solving easily blocked problem of chlorination furnace top outlet conduit, the invention provides the anti-calcium of chlorination furnace roof, magnesium, iron in a kind of titanium tetrachloride production and adhere to the method for stopping up, by the method can solve titanium tetrachloride produce in the easy blocked problem of chlorination furnace furnace roof outlet conduit, for production, the service efficiency of raising chlorination furnace have been established primary condition.
For achieving the above object, the present invention adopts following technical scheme:
In a kind of titanium tetrachloride production, the anti-calcium of chlorination furnace roof, magnesium, iron adhere to the method for stopping up, in the method, relate to four-way pipe, inverted cone-shaped dust collection cover, pressure equalizing pipe, the first gas pipeline and the second gas pipeline, chlorination furnace roof disposes outlet conduit, described outlet conduit is discharged and is contained calcium, magnesium, the formed chloride impurity gas of iron, and feature of the present invention is as follows:
First described outlet conduit is connected with the second gas pipeline, the second gas pipeline is by the lower end flange connect of flange and four-way pipe, the upper flanges of four-way pipe connects with inverted cone-shaped dust collection cover by upper end gate valve, the left end of four-way pipe or right-hand member flange connect with the first gas pipeline by the first gate valve, the right-hand member of four-way pipe or left end are implemented close or open and can connect backup line by side gate valve, between inverted cone-shaped dust collection cover and the first gas pipeline, be connected with pressure equalizing pipe, between dust collection cover and described backup line, be also connected with pressure equalizing pipe;
During work, described upper end gate valve and described the first gate valve all in opening working order described side gate valve in closing working order, described chloride impurity gas enters in four-way pipe by the second gas pipeline, because making the pressure in inverted cone-shaped dust collection cover and the first gas pipeline, the configuration of pressure equalizing pipe equates, a large amount of described chloride impurity gases directly enter in vertically disposed inverted cone-shaped dust collection cover along with the effect of its rising inertia, a small amount of described chloride impurity gas can enter in horizontally disposed the first gas pipeline and directly be discharged, enter the calcium in described chloride impurity gas in inverted cone-shaped dust collection cover, magnesium, iron is adhered on the inwall of inverted cone-shaped dust collection cover under the effect of gravity, through gathering dust, the described chloride impurity gas of processing can enter in the first gas pipeline along pressure equalizing pipe, enter the calcium in described chloride impurity gas in the first gas pipeline, magnesium, iron also can partly be adhered on the inwall of the first gas pipeline under the effect of gravity,
When the described calcium, magnesium, the iron that are adhered on inverted cone-shaped dust collection cover inwall are more, close described upper end gate valve and pull down inverted cone-shaped dust collection cover, after inverted cone-shaped dust collection cover is cleared up, connect with described upper end gate valve again and make described upper end gate valve can recover the effect of gathering dust of inverted cone-shaped dust collection cover in described unlatching working order;
When the described calcium, magnesium, the iron that are adhered on the inwall of the first gas pipeline are more, first on described side gate valve, connect clean described backup line, and then close described the first gate valve and pull down the first gas pipeline, through to connecting with described the first gate valve again and make described the first gate valve can recover the smoke evacuation effect of the first gas pipeline in described unlatching working order after the first gas pipeline cleaning, close again afterwards described side gate valve and pull down described backup line and to its cleaning;
The process of cleaning inverted cone-shaped dust collection cover or cleaning the first gas pipeline does not affect the described chloride impurity gas of the normal discharge of the second gas pipeline, and then guaranteed during titanium tetrachloride is produced that outlet conduit is normal described in chlorination furnace roof and discharged described chloride impurity gas, owing to producing without adhering to latch up phenomenon in the inverted cone-shaped dust collection cover of being cleared up in time, the first gas pipeline and described backup line, thus titanium tetrachloride produce in chlorination furnace roof also can not adhered to by described calcium, magnesium, iron and produce latch up phenomenon.
The caliber of caliber < first gas pipeline of pressure equalizing pipe.
The caliber of caliber≤the second gas pipeline of the first gas pipeline, the caliber of caliber≤the first gas pipeline of described backup line.
The external size of described upper end gate valve or equate with the external size of described the first gate valve, or unequal.
The external size of described the first gate valve or equate with the external size of described side gate valve, or unequal.
By adopting technical scheme as mentioned above, the present invention produces following beneficial effect:
1, method of the present invention can effectively solve titanium tetrachloride produce in the easy blocked problem of chlorination furnace furnace roof outlet conduit, for production, the service efficiency of raising chlorination furnace have been established primary condition.
2,the invention solves on the inwall that described calcium, magnesium, iron often sticks to described outlet conduit and cause chlorination furnace to stop the problem of producing, simple, practical feature that method has, for good technical qualification have been created in the normal production of titanium tetrachloride, also reduced the stopping production number of times causing due to plugging, improved titanium tetrachloride turnout, according to measuring and calculating: production can increase by 1,008 ten thousand yuan of profits more continuously.
3, the present invention configures on outlet conduit smoke evacuation and preventing clogging up device, have make simple, connect convenient feature, the Fast Installation of being more convenient for and dismounting.
Accompanying drawing explanation
Fig. 1 is the structural representation sketch of anti-blockage method of the present invention.
In Fig. 1: 1-four-way pipe; 2-inverted cone-shaped dust collection cover; 3-pressure equalizing pipe; 4-the first gas pipeline; 5-the second gas pipeline.
Embodiment
The present invention is the method for the anti-calcium of chlorination furnace roof during a kind of titanium tetrachloride is produced, magnesium, iron adhesion obstruction, the method can effectively solve titanium tetrachloride produce in the easy blocked problem of chlorination furnace furnace roof outlet conduit, for production, the service efficiency of raising chlorination furnace have been established primary condition.
It is to be noted: chlorination furnace roof disposes outlet conduit, described outlet conduit is discharged and is contained calcium, magnesium, the formed chloride impurity gas of iron.
The present invention disposes smoke evacuation and preventing clogging up device on described outlet conduit, this device comprises four-way pipe 1, inverted cone-shaped dust collection cover 2, pressure equalizing pipe 3, the first gas pipeline 4, the second gas pipeline 5, backup line and relevant gate valve, although these configurations are common, but act on chlorination furnace and can prevent described calcium, magnesium, iron from being adhered to and produce the latch up phenomenon unfavorable problem that causes discharging fume, its effect is unforeseen.
By the following examples, can explain in more detail the present invention, the present invention is not limited to the following examples, discloses object of the present invention and is intended to protect all changes and improvements in the scope of the invention.
In conjunction with Fig. 1, first described outlet conduit is connected with the second gas pipeline 5, the second gas pipeline 5 is by the lower end flange connect of flange and four-way pipe 1, the upper flanges of four-way pipe 1 connects with inverted cone-shaped dust collection cover 2 by upper end gate valve, the left end of four-way pipe 1 or right-hand member flange connect with the first gas pipeline 4 by the first gate valve, between inverted cone-shaped dust collection cover 2 and the first gas pipeline 4, are connected with pressure equalizing pipe 3.
Although Fig. 1 does not directly provide described upper end gate valve, described the first gate valve, described side gate valve and described backup line, but do not affect the existence of these configurations, the right-hand member of four-way pipe 1 or left end are implemented close or open and can connect backup line by side gate valve, between inverted cone-shaped dust collection cover 2 and described backup line, are also connected with pressure equalizing pipe 3.
The caliber of caliber < first gas pipeline 4 of pressure equalizing pipe 3.
The caliber of caliber≤the second gas pipeline 5 of the first gas pipeline 4, the caliber of caliber≤the first gas pipeline 4 of described backup line.
The external size of described upper end gate valve or equate with the external size of described the first gate valve, or unequal.
The external size of described the first gate valve or equate with the external size of described side gate valve, or unequal.
The present invention advises that the external size of described upper end gate valve, described the first gate valve, described side gate valve equates, because the described upper end gate valve of same model, described the first gate valve, described side gate valve have better interchangeability, above-mentioned gate valve or rotary valve or plate valve are advised in the Fast Installation of being more convenient for and dismounting simultaneously.
When above-mentioned smoke evacuation and preventing clogging up device work, described upper end gate valve and described the first gate valve all in opening working order described side gate valve in closing working order, described chloride impurity gas enters in four-way pipe 1 by the second gas pipeline 5, because making the pressure in inverted cone-shaped dust collection cover 2 and the first gas pipeline 4, the configuration of pressure equalizing pipe 3 equates, a large amount of described chloride impurity gases directly enter in vertically disposed inverted cone-shaped dust collection cover 2 along with the effect of its rising inertia, a small amount of described chloride impurity gas can enter in horizontally disposed the first gas pipeline 4 and directly be discharged, enter the calcium in the interior described chloride impurity gas of inverted cone-shaped dust collection cover 2, magnesium, iron is adhered on the inwall of dust collection cover 2 under the effect of gravity, through gathering dust, the described chloride impurity gas of processing can enter in the first gas pipeline 4 along pressure equalizing pipe 3, enter the calcium in the interior described chloride impurity gas of the first gas pipeline 4, magnesium, iron also can partly be adhered on the inwall of the first gas pipeline 4 under the effect of gravity.
Because the spatial content in inverted cone-shaped dust collection cover 2 is larger, when the described calcium, magnesium, the iron that are adhered on inverted cone-shaped dust collection cover 2 inwalls are more, close described upper end gate valve and pull down dust collection cover, after inverted cone-shaped dust collection cover 2 is cleared up, connect with described upper end gate valve again and make described upper end gate valve can recover the effect of gathering dust of inverted cone-shaped dust collection cover 2 in described unlatching working order.
When the described calcium, magnesium, the iron that are adhered on the inwall of the first gas pipeline 4 are more, first on described side gate valve, connect clean described backup line, and then close described the first gate valve and pull down the first gas pipeline 4, through to connecting with described the first gate valve again and make described the first gate valve can recover the smoke evacuation effect of the first gas pipeline 4 in described unlatching working order after the first gas pipeline 4 cleaning, close again afterwards described side gate valve and pull down described backup line and to its cleaning.
Cleaning inverted cone-shaped dust collection cover 2 or the process of cleaning the first gas pipeline 4 do not affect the described chloride impurity gas of the second gas pipeline 5 normal discharge, and then guaranteed during titanium tetrachloride is produced that outlet conduit is normal described in chlorination furnace roof and discharged described chloride impurity gas, owing to producing without adhering to latch up phenomenon in inverted cone-shaped dust collection cover 2, the first gas pipeline 4 and the described backup line cleared up in time, thus titanium tetrachloride produce in chlorination furnace roof also can not adhered to by described calcium, magnesium, iron and produce latch up phenomenon.
By above-mentioned, can obviously find out: the invention solves on the inwall that described calcium, magnesium, iron often sticks to described outlet conduit and cause chlorination furnace to stop the problem of producing, simple, practical feature that method has, for good technical qualification have been created in the normal production of titanium tetrachloride, also reduced the stopping production number of times causing due to plugging, improved titanium tetrachloride turnout, according to measuring and calculating: production can increase by 1,008 ten thousand yuan of profits more continuously.
Claims (5)
1. in a titanium tetrachloride production, the anti-calcium of chlorination furnace roof, magnesium, iron adhere to the method for stopping up, in the method, relate to four-way pipe (1), inverted cone-shaped dust collection cover (2), pressure equalizing pipe (3), the first gas pipeline (4) and the second gas pipeline (5), chlorination furnace roof disposes outlet conduit, described outlet conduit is discharged and is contained calcium, magnesium, the formed chloride impurity gas of iron, its feature in this way:
First described outlet conduit is connected with the second gas pipeline (5), the second gas pipeline (5) is by the lower end flange connect of flange and four-way pipe (1), the upper flanges of four-way pipe (1) connects with inverted cone-shaped dust collection cover (2) by upper end gate valve, the left end of four-way pipe (1) or right-hand member flange connect with the first gas pipeline (4) by the first gate valve, the right-hand member of four-way pipe (1) or left end are implemented close or open and can connect backup line by side gate valve, between inverted cone-shaped dust collection cover (2) and the first gas pipeline (4), be connected with pressure equalizing pipe (3), between inverted cone-shaped dust collection cover (2) and described backup line, be also connected with pressure equalizing pipe (3),
During work, described upper end gate valve and described the first gate valve all in opening working order described side gate valve in closing working order, described chloride impurity gas enters in four-way pipe (1) by the second gas pipeline (5), because making the pressure in inverted cone-shaped dust collection cover (2) and the first gas pipeline (4), the configuration of pressure equalizing pipe (3) equates, a large amount of described chloride impurity gases directly enter in vertically disposed inverted cone-shaped dust collection cover (2) along with the effect of its rising inertia, a small amount of described chloride impurity gas can enter in horizontally disposed the first gas pipeline (4) and directly be discharged, enter the calcium in described chloride impurity gas in inverted cone-shaped dust collection cover (2), magnesium, iron is adhered on the inwall of inverted cone-shaped dust collection cover (2) under the effect of gravity, through gathering dust, the described chloride impurity gas of processing can enter in the first gas pipeline (4) along pressure equalizing pipe (3), enter the calcium in described chloride impurity gas in the first gas pipeline (4), magnesium, iron also can partly be adhered on the inwall of the first gas pipeline (4) under the effect of gravity,
When the described calcium, magnesium, the iron that are adhered on inverted cone-shaped dust collection cover (2) inwall are more, close described upper end gate valve and pull down inverted cone-shaped dust collection cover (2), after inverted cone-shaped dust collection cover (2) is cleared up, connect with described upper end gate valve again and make described upper end gate valve can recover the effect of gathering dust of inverted cone-shaped dust collection cover (2) in described unlatching working order;
When the described calcium, magnesium, the iron that are adhered on the inwall of the first gas pipeline (4) are more, first on described side gate valve, connect clean described backup line, and then close described the first gate valve and pull down the first gas pipeline (4), through connecting with described the first gate valve again and make described the first gate valve can recover the smoke evacuation effect of the first gas pipeline (4) in described unlatching working order after the first gas pipeline (4) cleaning, close again afterwards described side gate valve and pull down described backup line and to its cleaning;
The process of cleaning inverted cone-shaped dust collection cover (2) or cleaning the first gas pipeline (4) does not affect the second gas pipeline (5) and normally discharges described chloride impurity gas, and then guaranteed during titanium tetrachloride is produced that outlet conduit is normal described in chlorination furnace roof and discharged described chloride impurity gas, owing to producing without adhering to latch up phenomenon in the inverted cone-shaped dust collection cover (2) of being cleared up in time, the first gas pipeline (4) and described backup line, thus titanium tetrachloride produce in chlorination furnace roof also can not adhered to by described calcium, magnesium, iron and produce latch up phenomenon.
According to claim 1 titanium tetrachloride produce in the anti-calcium of chlorination furnace roof, magnesium, iron adhere to the method for stopping up, it is characterized in that: the caliber of caliber < first gas pipeline (4) of pressure equalizing pipe (3).
According to claim 1 titanium tetrachloride produce in the anti-calcium of chlorination furnace roof, magnesium, iron adhere to the method for stopping up, it is characterized in that: the caliber of caliber≤the second gas pipeline (5) of the first gas pipeline (4), the caliber of caliber≤the first gas pipeline (4) of described backup line.
According to claim 1 titanium tetrachloride produce in the anti-calcium of chlorination furnace roof, magnesium, iron adhere to the method for stopping up, it is characterized in that: the external size of described upper end gate valve or equate with the external size of described the first gate valve, or unequal.
According to claim 1 titanium tetrachloride produce in the anti-calcium of chlorination furnace roof, magnesium, iron adhere to the method for stopping up, it is characterized in that: the external size of described the first gate valve or equate with the external size of described side gate valve, or unequal.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310263836.6A CN103359779B (en) | 2013-06-28 | 2013-06-28 | Method for preventing calcium, magnesium and iron adhesion blockage at top of chlorination furnace during production of titanium tetrachloride |
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| CN201310263836.6A CN103359779B (en) | 2013-06-28 | 2013-06-28 | Method for preventing calcium, magnesium and iron adhesion blockage at top of chlorination furnace during production of titanium tetrachloride |
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| CN103359779A CN103359779A (en) | 2013-10-23 |
| CN103359779B true CN103359779B (en) | 2014-11-19 |
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| CN106587144B (en) * | 2016-12-22 | 2018-02-16 | 遵义钛业股份有限公司 | One kind is without sieve plate fluidizing chlorination system |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202297170U (en) * | 2011-09-01 | 2012-07-04 | 洛阳双瑞万基钛业有限公司 | Device for recycling waste residues in production of titanium tetrachloride |
| CN202346779U (en) * | 2011-11-07 | 2012-07-25 | 天津渤天化工有限责任公司 | Dust collector of chlorination furnace |
| CN102732656A (en) * | 2012-07-17 | 2012-10-17 | 新兴铸管股份有限公司 | Method for cleaning blockage of bell-less furnace top pressure equalizing relief pipeline of blast furnace |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH061613A (en) * | 1992-06-24 | 1994-01-11 | Ishihara Sangyo Kaisha Ltd | Production of titanium tetrachloride |
| JP3883829B2 (en) * | 2001-08-31 | 2007-02-21 | 住友チタニウム株式会社 | Blocking prevention device in chlorination furnace |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202297170U (en) * | 2011-09-01 | 2012-07-04 | 洛阳双瑞万基钛业有限公司 | Device for recycling waste residues in production of titanium tetrachloride |
| CN202346779U (en) * | 2011-11-07 | 2012-07-25 | 天津渤天化工有限责任公司 | Dust collector of chlorination furnace |
| CN102732656A (en) * | 2012-07-17 | 2012-10-17 | 新兴铸管股份有限公司 | Method for cleaning blockage of bell-less furnace top pressure equalizing relief pipeline of blast furnace |
Non-Patent Citations (2)
| Title |
|---|
| JP特開2003-73121A 2003.03.12 * |
| JP特開平6-1613A 1994.01.11 * |
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