CN103337447B - Hollow cathode lamp device - Google Patents
Hollow cathode lamp device Download PDFInfo
- Publication number
- CN103337447B CN103337447B CN201310220745.4A CN201310220745A CN103337447B CN 103337447 B CN103337447 B CN 103337447B CN 201310220745 A CN201310220745 A CN 201310220745A CN 103337447 B CN103337447 B CN 103337447B
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- glass tubing
- cushion block
- top end
- end cover
- rear portion
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- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Abstract
The invention provides hollow cathode lamp device, it by the external spectrogrph of hollow cathode lamp internal combustion, can directly detect the content of low-melting impurities in alloy to be detected, and its precision can reach 0.00001%～0.0001%, and its accuracy of detection is high.It includes glass tubing, top end cover, cushion block, rear portion fixed block, the front end of described glass tubing is provided with described top end cover, the rear end of described glass tubing is provided with described cushion block, described cushion block is fastenedly connected the described rear portion fixed block at its rear portion, it is characterized in that: described glass tube is provided with graphite electrode, described graphite electrode connects the leading section of described glass tubing by connecting rod, the rear portion of described glass tubing is provided with tungsten bar, the front end of described tungsten bar has been welded to connect nickel sheet structure, the rear end of described tungsten bar is plugged in inside described cushion block, one end towards described tungsten bar of described graphite electrode is provided with hollow object placing cavity, alloy to be detected is placed in described hollow object placing cavity, the inside of described glass tubing is full of noble gas.
Description
Technical field
The present invention relates to the technical field of metal spectrum analysis, specially hollow cathode lamp device.
Background technology
Blade in the market, the main material of axle are all to be made up of dystectic alloy, but in manufacturing process,
The inside of material can be mixed into the low-melting-point metal impurity such as some such as stannum, lead, bismuths, causes during blade, axle run up,
These low-melting-point metal impurity first melt, and then form crack on blade, axle, cause the working life of these frame for movements
Short.
So-called plasma source in spectrum analysis, is often referred to be similar in appearance a class charging source of flame.Mesh
Before the most frequently used have three classes: i.e. induction coupled plasma torch (ICP), direct-current plasma bright eruption (DCP) and microwave is inducted
Gas ions torch (MIP).For MIP, although allowing micro-sampling, air consumption is little, and power mensuration low, easy is nonmetal, but right
Most metal detection limits are poor, Interelement interference serious, needs helium, is therefore mainly used in the detector of chromatography.ICP and
This two classes plasma source of DCP has preferable analytical performance, has the most been applied to Atomic Emission Spectrometer AES.But it is existing
This two classes plasma source of ICP and DCP detection be limited to 0.001% detection limit, for lower loading foreign metal its cannot
Detect.And in existing spectrogrph, hollow cathode lamp functions only as the effect of luminescence, and its effect is single.
Summary of the invention
For the problems referred to above, the invention provides hollow cathode lamp device, it can be by hollow cathode lamp internal junction
Close external spectrogrph, directly detect the content of low-melting impurities in alloy to be detected, and its precision can reach
0.00001%～0.0001%, its accuracy of detection is high.
Hollow cathode lamp device, its technical scheme is such that it and includes that glass tubing, top end cover, cushion block, rear portion are fixed
Block, the front end of described glass tubing is provided with described top end cover, and the rear end of described glass tubing is provided with described cushion block, and described cushion block is tight
It is solidly connected the described rear portion fixed block at its rear portion, it is characterised in that: described glass tube is provided with graphite electrode, described graphite
Electrode connects the leading section of described glass tubing by connecting rod, and the rear portion of described glass tubing is provided with tungsten bar, before described tungsten bar
End be welded to connect nickel sheet structure, the rear end of described tungsten bar is plugged in inside described cushion block, described graphite electrode towards described
One end of tungsten bar is provided with hollow object placing cavity, places alloy to be detected in described hollow object placing cavity, and the inside of described glass tubing is filled
Full noble gas.
It is further characterized by outside the outer ring surface of described glass tubing being provided with fixing bar, every described fixing bar
Two ends connect described top end cover, cushion block respectively, and are fastenedly connected by fixing screw；
It is provided with silicagel pad between the contact surface of described glass tubing and described top end cover；
Described silicagel pad, top end cover are run through in the front end of described connecting rod, and plug cover is loaded on the anterior suit of described top end cover
In hole, described plug blocks the front portion of described connecting rod.
After using the structure of the present invention, graphite electrode is as the negative electrode of hollow cathode lamp, the hollow object placing cavity of graphite electrode
Interior placement alloy to be detected, is welded with the tungsten bar of nickel sheet structure as anode, when applying high voltage between two-stage, to be detected
Low-melting-point metal in alloy is the most luminous, refractory metal luminescence afterwards, is divided by spectrogrph according to the spectrum that its metal is luminous
Analysis, it is possible to analyze the content of low-melting impurities drawing alloy to be detected, and its precision can reach 0.00001%～
0.0001%, accuracy of detection is high.
Accompanying drawing explanation
Fig. 1 is the axonometric chart structural schematic block diagram of the present invention；
Fig. 2 is the front view structural representation of the present invention.
Detailed description of the invention
Seeing Fig. 1, Fig. 2, it includes glass tubing 1, top end cover 2, cushion block 3, rear portion fixed block 4, and the front end of glass tubing 1 is provided with
Top end cover 2, the rear end of glass tubing 1 is provided with cushion block 3, and cushion block 3 is fastenedly connected the rear portion fixed block 4 at its rear portion, and glass tubing 1 is internal
Being provided with graphite electrode 5, graphite electrode 5 connects the leading section of glass tubing 1 by connecting rod 6, and the rear portion of glass tubing 1 is provided with tungsten
Rod 7, the front end of tungsten bar 7 has been welded to connect nickel sheet structure 8, and it is internal that the rear end of tungsten bar 7 is plugged in cushion block 3, graphite electrode 5 towards
One end of tungsten bar 7 is provided with hollow object placing cavity 9, places alloy 14 to be detected in hollow object placing cavity 9, and the inside of glass tubing 1 is full of
Noble gas.Be provided with fixing bar 10 outside the outer ring surface of glass tubing 1, the two ends of every fixing bar 10 connect respectively top end cover 2,
Cushion block 3, and be fastenedly connected by fixing screw 11；Silicagel pad 12 it is provided with between the contact surface of glass tubing 1 and top end cover 2；Connect
The front end through-silicon rubber cushion 12 of bar 6, top end cover 2, plug 13 lid is loaded in the anterior suit hole of top end cover 2, and plug 13 blocks
The front portion of connecting rod 6.
Claims (4)
1. hollow cathode lamp device, it includes glass tubing, top end cover, cushion block and rear portion fixed block, and the front end of described glass tubing sets
Being equipped with described top end cover, the rear end of described glass tubing is provided with described cushion block, described cushion block be fastenedly connected its rear portion described after
Portion's fixed block, it is characterised in that: described glass tube is provided with graphite electrode, and described graphite electrode connects institute by connecting rod
Stating the leading section of glass tubing, the rear portion of described glass tubing is provided with tungsten bar, and the front end of described tungsten bar has been welded to connect nickel sheet structure,
The rear end of described tungsten bar is plugged in inside described cushion block, and one end towards described tungsten bar of described graphite electrode is provided with hollow putting
Thing chamber, places alloy to be detected in described hollow object placing cavity, the inside of described glass tubing is full of noble gas.
Hollow cathode lamp device the most according to claim 1, it is characterised in that: arrange outside the outer ring surface of described glass tubing
Fixing bar, the two ends of every described fixing bar is had to connect described top end cover, cushion block respectively, and be fastenedly connected by fixing screw.
Hollow cathode lamp device the most according to claim 2, it is characterised in that: connecing of described glass tubing and described top end cover
Silicagel pad it is provided with between contacting surface.
Hollow cathode lamp device the most according to claim 3, it is characterised in that: described silicon is run through in the front end of described connecting rod
Rubber cushion, top end cover, plug cover is loaded in the anterior suit hole of described top end cover, before described plug blocks described connecting rod
Portion.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310220745.4A CN103337447B (en) | 2013-06-05 | 2013-06-05 | Hollow cathode lamp device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310220745.4A CN103337447B (en) | 2013-06-05 | 2013-06-05 | Hollow cathode lamp device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103337447A CN103337447A (en) | 2013-10-02 |
| CN103337447B true CN103337447B (en) | 2016-12-28 |
Family
ID=49245586
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310220745.4A Active CN103337447B (en) | 2013-06-05 | 2013-06-05 | Hollow cathode lamp device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103337447B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106855505B (en) * | 2016-12-29 | 2023-07-21 | 山东非金属材料研究所 | Hollow cathode lamp testing device and testing method |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3851213A (en) * | 1971-10-28 | 1974-11-26 | Philips Corp | Arrangement for generating modulated atomic resonance |
| CN2105765U (en) * | 1991-12-09 | 1992-05-27 | 北京有色金属研究总院 | High quality hollow cathode lamp |
| CN2411468Y (en) * | 1999-12-29 | 2000-12-20 | 吴安林 | Multi-cathode element hollow cathode lamp |
| CN2749050Y (en) * | 2004-10-19 | 2005-12-28 | 北京同立在线系统集成有限公司 | Hollow cathode lamp |
| CN102184834A (en) * | 2011-04-21 | 2011-09-14 | 齐齐哈尔医学院 | Hollow cathode lamp and atomic absorption spectrometer manufactured by hollow cathode lamp |
| CN203367230U (en) * | 2013-06-05 | 2013-12-25 | 无锡市金义博仪器科技有限公司 | Hollow cathode lamp device, |
-
2013
- 2013-06-05 CN CN201310220745.4A patent/CN103337447B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3851213A (en) * | 1971-10-28 | 1974-11-26 | Philips Corp | Arrangement for generating modulated atomic resonance |
| CN2105765U (en) * | 1991-12-09 | 1992-05-27 | 北京有色金属研究总院 | High quality hollow cathode lamp |
| CN2411468Y (en) * | 1999-12-29 | 2000-12-20 | 吴安林 | Multi-cathode element hollow cathode lamp |
| CN2749050Y (en) * | 2004-10-19 | 2005-12-28 | 北京同立在线系统集成有限公司 | Hollow cathode lamp |
| CN102184834A (en) * | 2011-04-21 | 2011-09-14 | 齐齐哈尔医学院 | Hollow cathode lamp and atomic absorption spectrometer manufactured by hollow cathode lamp |
| CN203367230U (en) * | 2013-06-05 | 2013-12-25 | 无锡市金义博仪器科技有限公司 | Hollow cathode lamp device, |
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| Publication number | Publication date |
|---|---|
| CN103337447A (en) | 2013-10-02 |
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