CN103332698A - Process for synthesizing high-quality sodium silicate with low energy consumption - Google Patents

Process for synthesizing high-quality sodium silicate with low energy consumption Download PDF

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Publication number
CN103332698A
CN103332698A CN2013102223264A CN201310222326A CN103332698A CN 103332698 A CN103332698 A CN 103332698A CN 2013102223264 A CN2013102223264 A CN 2013102223264A CN 201310222326 A CN201310222326 A CN 201310222326A CN 103332698 A CN103332698 A CN 103332698A
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China
Prior art keywords
water
sodium silicate
gas
water glass
regenerator
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Pending
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CN2013102223264A
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Chinese (zh)
Inventor
赵东旭
汪树龙
董珂
连佩兵
沈颂良
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ANHUI LONGQUAN SILICON MATERIAL Co Ltd
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ANHUI LONGQUAN SILICON MATERIAL Co Ltd
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Priority to CN2013102223264A priority Critical patent/CN103332698A/en
Publication of CN103332698A publication Critical patent/CN103332698A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/129Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

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Abstract

The invention discloses a process for synthesizing high-quality sodium silicate with low energy consumption, aims to solve the problems of high energy consumption and poor product quality of an existing process for producing sodium silicate, and relates to the technical field of processes for producing sodium silicate. The process for synthesizing high-quality sodium silicate with low energy consumption comprises the following steps of: connecting a soft water necessary device of a gas producer with a blast blower, wherein water gas produced by the gas producer sequentially passes through a cyclone dust collector, an exchanger and a heat storage chamber, and the heat storage chamber is provided with an interlayer which is connected with a waste heat pipe of the gas producer; performing heat preservation on the heat storage chamber by using the waste heat of the gas producer; directly introducing the water gas in the heat storage chamber into a smelting kiln for burning; introducing molten sodium silicate produced by the smelting kiln into a clarifying and precipitating tank for purification and precipitation; and then putting the molten sodium silicate into a discharging machine through a chute so as to be in contact with circulating water, and packaging after cooling. According to the process, the gas supply is more stable, the water gas is preheated before entering the smelting kiln for burning, the coal consumption can be saved, and the sodium silicate is purified and precipitated, so that the product quality is improved.

Description

The technology of the synthetic high-quality water glass of less energy-consumption
Technical field:
The present invention relates to the water glass technical field of producing, relate in particular to the technology of the synthetic high-quality water glass of a kind of less energy-consumption.
Background technology:
Water glass is commonly called as water glass, and main component is silicon.
The purposes of water glass is very extensive, almost spreads all over each department of national economy.Being used to make various silicates products such as silica gel, white carbon black, zeolite molecular sieve, metasilicate pentahydrate sodium, silicon sol, layer silicon and instant powdery sodium silicate, sodium-potassium silicate at chemical system, is the basic raw material of silicon compound.In developed country, be kind surplus the deep processing series product of raw material have developed into 50 with the water glass, some has been applied to the high, precision and frontier sciemtifec and technical sphere; Being indispensable raw material in the washing composition such as washing powder, soap in light industry, also is water softener, settling agent; In textile industry, be used for helping dye, bleaching and sizing; In mechanical industry, be widely used in casting, emery wheel manufacturing and anticolodal etc.; In building trade for the manufacture of rapid hardening cement, acid-proof cement dubbin, soil-solidified-agent, refractory materials etc.; Agriculturally can make the silicon element fertilizer material; Floating, dying and slurry, mine ore dressing, waterproof, leak stopping, fire retarding wood protection, food antiseptic and preparing adhesive etc. as tackiness agent, anticolodal, water-softening agent, detergent builder, refractory materials and the ceramic raw material of the filler of the silica-alumina catalyst of petroleum catalytic cracking, soap, fluting board, textiles in addition.
In the industrial production, be that quartz sand and soda ash are mixed back being heated to about 1400 ℃ by a certain percentage in Reaktionsofen, generate the molten water glass.There is the defective of energy consumption height, product quality difference in the production technique of existing water glass.
Summary of the invention:
Technical problem to be solved by this invention is to overcome the defective of prior art, and the technology of the synthetic high-quality water glass of a kind of reinforced less energy-consumption easily is provided.
Technical problem to be solved by this invention realizes by the following technical solutions.
The technology of the synthetic high-quality water glass of a kind of less energy-consumption, comprise that part and melting part take place coal gas, it is characterized in that: described coal gas generating unit branch comprises the indispensable device of the soft water that connects producer gas generator and gas blower, the water-gas that described producer gas generator produces passes through tornado dust collector successively, interchanger and regenerator, described regenerator is provided with interlayer, the waste heat pipe coupling of interlayer and producer gas generator, waste heat by producer gas generator is incubated regenerator, water-gas in the described regenerator directly feeds melting kiln internal combustion, the molten water glass that described melting kiln is produced feeds in the clarification settling tank and purifies precipitation process, the molten water glass enters discharging machine through chute then, and packs behind the recirculated water contact cooling.
Enter circulating water pool after the recirculated water collection for the cooling water glass, cooling back recycle.
The technology of the synthetic high-quality water glass of less energy-consumption provided by the invention stores the water-gas that produces earlier through regenerator, feeding melting kiln internal combustion, and air feed is more stable; The waste heat that producer gas generator produces is incubated regenerator, before water-gas in the regenerator enters the burning of melting kiln, utilize waste heat to carry out preheating earlier, the heat that the water-gas burning is produced farthest is utilized effectively, thereby reach purpose of energy saving, against existing technologies, producing water glass per ton can save more than the coal consumption 100kg; The molten water glass of producing in the melting kiln purifies precipitation process through the clarification settling tank, has improved product quality, can make soluble solids in the product 〉=99%, surpasses international standard.
Description of drawings:
Fig. 1 is technological process of production figure of the present invention.
Embodiment:
For technique means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, below in conjunction with concrete diagram, further set forth the present invention.
As shown in Figure 1, the technology of the synthetic high-quality water glass of a kind of less energy-consumption, comprise the indispensable device of the soft water that connects producer gas generator and gas blower, the water-gas that producer gas generator produces passes through tornado dust collector successively, interchanger and regenerator, regenerator is provided with interlayer, the waste heat pipe coupling of interlayer and producer gas generator, waste heat by producer gas generator is incubated regenerator, water-gas in the regenerator directly feeds melting kiln internal combustion, the molten water glass that the melting kiln is produced feeds in the clarification settling tank and purifies precipitation process, the molten water glass enters discharging machine through chute then, with pack behind the recirculated water contact cooling, enter circulating water pool after the recirculated water collection for the cooling water glass, cooling back recycle.
More than show and described ultimate principle of the present invention, principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; that describes in above-described embodiment and the specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.

Claims (2)

1. the technology of the synthetic high-quality water glass of a less energy-consumption, comprise that part and melting part take place coal gas, it is characterized in that: described coal gas generating unit branch comprises the indispensable device of the soft water that connects producer gas generator and gas blower, the water-gas that described producer gas generator produces passes through tornado dust collector successively, interchanger and regenerator, described regenerator is provided with interlayer, the waste heat pipe coupling of interlayer and producer gas generator, waste heat by producer gas generator is incubated regenerator, water-gas in the described regenerator directly feeds melting kiln internal combustion, the molten water glass that described melting kiln is produced feeds in the clarification settling tank and purifies precipitation process, the molten water glass enters discharging machine through chute then, and packs behind the recirculated water contact cooling.
2. the technology of the synthetic high-quality water glass of less energy-consumption according to claim 1 is characterized in that: enter circulating water pool, cooling back recycle after collecting for the recirculated water of cooling water glass.
CN2013102223264A 2013-06-05 2013-06-05 Process for synthesizing high-quality sodium silicate with low energy consumption Pending CN103332698A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013102223264A CN103332698A (en) 2013-06-05 2013-06-05 Process for synthesizing high-quality sodium silicate with low energy consumption

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2013102223264A CN103332698A (en) 2013-06-05 2013-06-05 Process for synthesizing high-quality sodium silicate with low energy consumption

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CN103332698A true CN103332698A (en) 2013-10-02

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107090250A (en) * 2017-05-24 2017-08-25 安徽龙泉硅材料有限公司 A kind of method for preparing industrial metasilicate adhesive
CN107215878A (en) * 2017-05-24 2017-09-29 安徽龙泉硅材料有限公司 The production technology of high-quality industrial metasilicate
CN115215349A (en) * 2022-06-06 2022-10-21 安徽龙泉硅材料有限公司 Preparation of sodium silicate and digital bubble purification system thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101508442A (en) * 2009-03-31 2009-08-19 洛阳豫燃煤气设备有限公司 Pre-heating heat-exchanging direct dissolution type sodium silicate production process and apparatus
CN101508441A (en) * 2008-10-17 2009-08-19 株洲兴隆化工实业有限公司 Direct dissolution process for molten sodium silicate
CN102730707A (en) * 2011-04-02 2012-10-17 青岛东岳泡花碱有限公司 System for recycling heat energy from sodium silicate production technology

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101508441A (en) * 2008-10-17 2009-08-19 株洲兴隆化工实业有限公司 Direct dissolution process for molten sodium silicate
CN101508442A (en) * 2009-03-31 2009-08-19 洛阳豫燃煤气设备有限公司 Pre-heating heat-exchanging direct dissolution type sodium silicate production process and apparatus
CN102730707A (en) * 2011-04-02 2012-10-17 青岛东岳泡花碱有限公司 System for recycling heat energy from sodium silicate production technology

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107090250A (en) * 2017-05-24 2017-08-25 安徽龙泉硅材料有限公司 A kind of method for preparing industrial metasilicate adhesive
CN107215878A (en) * 2017-05-24 2017-09-29 安徽龙泉硅材料有限公司 The production technology of high-quality industrial metasilicate
CN115215349A (en) * 2022-06-06 2022-10-21 安徽龙泉硅材料有限公司 Preparation of sodium silicate and digital bubble purification system thereof

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Application publication date: 20131002