CN103332654A - High-purity iodine production device - Google Patents
High-purity iodine production device Download PDFInfo
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- CN103332654A CN103332654A CN2013102961530A CN201310296153A CN103332654A CN 103332654 A CN103332654 A CN 103332654A CN 2013102961530 A CN2013102961530 A CN 2013102961530A CN 201310296153 A CN201310296153 A CN 201310296153A CN 103332654 A CN103332654 A CN 103332654A
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- sublimating
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Abstract
The invention discloses a high-purity iodine production device which comprises a reaction part, a desublimation part and a washing part, wherein the reaction part consists of a ceramic reactor (2), a refrigeration drier (11), a compressor (4) and an air pretreater (10); a jacket heating device is arranged outside the ceramic reactor (2); the desublimation part consists of a desublimation device (1); a product storage tank (6) is arranged at the bottom of the desublimation device (1); the washing part consists of a washing tank (3), a cleaning solution preparation tank (5) and a cleaning solution storage tank (7); the washing tank (3) is connected with an outlet of the desublimation device (1) by a pipeline; and a gas outlet of the washing tank (3) is connected with a fan (9). The device can produce high-purity iodine with the purity greater than or equal to 99.9%, and brings a great economic benefit.
Description
Technical field
The present invention relates to separate, specifically relate to the purification of iodine.
Background technology
Iodine has critical role as one of important Inorganic Chemicals in national economy, at present, the smart iodine that purity is high worldwide all belongs to narrow resources.Application number 201220037235.4 in the prior art " thick iodine retrieving arrangement " is though structure is comparatively simple, can reclaim thick iodine, but adopt the purity of the iodine product that this device obtains high not enough, of the present invention focus on specially provides a kind of device at the purification of iodine, can reduce the impurity in the iodine product, improve the purity of iodine.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art, a kind of high-purity iodine purifying plant is provided, can reduce the impurity in the iodine product, improve the purity of iodine.
Technical scheme of the present invention: a kind of high-purity iodine production equipment, it comprises reactive moieties, sublimates partly and the washing part; Wherein reactive moieties is made of ceramic reactor, freezing type drier, air compressor and air pretreater, and the outside of described ceramic reactor is provided with the jacketed type heating unit; The described part of sublimating is made of the device of sublimating, and the bottom of the described device of sublimating is provided with the product storage tank; Described washing part is made of washing tank, washings Preparation tank and washings storage tank; Described washing tank is by the outlet of pipe connection to the device of sublimating, and the pneumatic outlet of described washing tank is connected with blower fan.
Above-mentioned freezing type drier is the series connection of 2-5 platform.
Above-mentioned air pretreater is in the room of a relatively dry, guarantees air purity and humidity.
Above-mentioned electric heater unit is provided with temperature display meter.
The above-mentioned pipeline that is connected to the device of sublimating from ceramic reactor outlet is provided with heating unit.
The both sides of the above-mentioned device of sublimating are provided with centrifugal blower.
Device of the present invention carries out pre-treatment to air, reduces humidity and the impurity of air.Freezing type drier by one group of series connection further carries out drying to pressurized air again, obtains the pressurized air of humidity≤10%, improves the quality of products thereby reduce the moisture that enters reactor.Adopt device of the present invention can produce 〉=high-purity iodine of 99.9%, can be applicable to electronic industry, war industry and medicine industry etc.Be 600,000 yuan/ton of the market value of 420,000 yuan/ton and high-purity iodine according to the market value of thick iodine, both price differences are: 180,000 yuan/ton.If by 100 tons of calculating of annual product, can create 1,800 ten thousand yuan of economic worths in 1 year.
Description of drawings
Fig. 1 is structural representation of the present invention;
Among the figure: the 1-device of sublimating; The 2-ceramic reactor; The 3-washing tank; The 4-compressor; 5-washings Preparation tank; 6-product storage tank; 7-washings storage tank; The 8-centrifugal blower; The 9-blower fan; 10-air pretreater; The 11-freezing type drier.
Embodiment
Embodiment
A kind of high-purity iodine production equipment, it comprises reactive moieties, sublimates partly and the washing part; Wherein reactive moieties is made of ceramic reactor 2, freezing type drier 11, compressor 4 and air pretreater 10, and the outside of described ceramic reactor 2 is provided with the jacketed type heating unit; The described part of sublimating is made of the device 1 of sublimating, and described bottom of sublimating device 1 is provided with product storage tank 6; Described washing part is made of washing tank 3, washings Preparation tank 5 and washings storage tank 7; Described washing tank 3 is by the outlet of pipe connection to the device 1 of sublimating, and the pneumatic outlet of described washing tank 3 is connected with blower fan 9.
Above-mentioned freezing type drier 11 is the series connection of 2-5 platform.
Above-mentioned air pretreater 10 is in the room of a relatively dry, guarantees air purity and humidity.
Above-mentioned electric heater unit is provided with temperature display meter.
The above-mentioned pipeline that is connected to the device 1 of sublimating from ceramic reactor outlet is provided with heating unit.
Above-mentioned both sides of sublimating device 1 are provided with centrifugal blower 8.
Claims (6)
1. a high-purity iodine production equipment is characterized in that it comprises reactive moieties, sublimates partly and the washing part; Wherein reactive moieties is made of ceramic reactor (2), freezing type drier (11), compressor (4) and air pretreater (10), and the outside of described ceramic reactor (2) is provided with the jacketed type heating unit; The described part of sublimating is made of the device of sublimating (1), and the bottom of the described device of sublimating (1) is provided with product storage tank (6); Described washing part is made of washing tank (3), washings Preparation tank (5) and washings storage tank (7); Described washing tank (3) is by the outlet of pipe connection to the device of sublimating (1), and the pneumatic outlet of described washing tank (3) is connected with blower fan (9).
2. high-purity iodine production equipment according to claim 1 is characterized in that described freezing type drier (11) is the series connection of 2-5 platform.
3. high-purity iodine production equipment according to claim 1 is characterized in that described air pretreater (10) is in the room of a relatively dry, guarantees air purity and humidity.
4. high-purity iodine production equipment according to claim 1 is characterized in that described electric heater unit is provided with temperature display meter.
5. high-purity iodine production equipment according to claim 1 is characterized in that the pipeline that is connected to the device of sublimating (1) from the ceramic reactor outlet is provided with heating unit.
6. high-purity iodine production equipment according to claim 1 is characterized in that the both sides of the described device of sublimating (1) are provided with centrifugal blower (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102961530A CN103332654A (en) | 2013-07-16 | 2013-07-16 | High-purity iodine production device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013102961530A CN103332654A (en) | 2013-07-16 | 2013-07-16 | High-purity iodine production device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103332654A true CN103332654A (en) | 2013-10-02 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013102961530A Pending CN103332654A (en) | 2013-07-16 | 2013-07-16 | High-purity iodine production device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103332654A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5919503A (en) * | 1982-07-23 | 1984-02-01 | Mitsubishi Heavy Ind Ltd | Apparatus for recovering volatile substance |
| CN1084255A (en) * | 1992-09-15 | 1994-03-23 | 杭州嘉美净化设备有限公司 | Purified compressed air supply unit |
| CN101274748A (en) * | 2008-05-21 | 2008-10-01 | 瓮福（集团）有限责任公司 | Method for refining industrial coarse iodine |
| CN101759152A (en) * | 2009-11-17 | 2010-06-30 | 瓮福（集团）有限责任公司 | Method for removing impurities in process of extracting iodine by using iodine-contained phosphate ore as raw materials |
| CN202465270U (en) * | 2012-02-06 | 2012-10-03 | 江苏焕鑫高新材料科技有限公司 | Coarse iodine recovery device |
| CN103011083A (en) * | 2012-12-04 | 2013-04-03 | 瓮福（集团）有限责任公司 | Gas-phase iodine crystallization method |
| CN203392855U (en) * | 2013-07-16 | 2014-01-15 | 瓮福（集团）有限责任公司 | High-purity iodine production device |
-
2013
- 2013-07-16 CN CN2013102961530A patent/CN103332654A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5919503A (en) * | 1982-07-23 | 1984-02-01 | Mitsubishi Heavy Ind Ltd | Apparatus for recovering volatile substance |
| CN1084255A (en) * | 1992-09-15 | 1994-03-23 | 杭州嘉美净化设备有限公司 | Purified compressed air supply unit |
| CN101274748A (en) * | 2008-05-21 | 2008-10-01 | 瓮福（集团）有限责任公司 | Method for refining industrial coarse iodine |
| CN101759152A (en) * | 2009-11-17 | 2010-06-30 | 瓮福（集团）有限责任公司 | Method for removing impurities in process of extracting iodine by using iodine-contained phosphate ore as raw materials |
| CN202465270U (en) * | 2012-02-06 | 2012-10-03 | 江苏焕鑫高新材料科技有限公司 | Coarse iodine recovery device |
| CN103011083A (en) * | 2012-12-04 | 2013-04-03 | 瓮福（集团）有限责任公司 | Gas-phase iodine crystallization method |
| CN203392855U (en) * | 2013-07-16 | 2014-01-15 | 瓮福（集团）有限责任公司 | High-purity iodine production device |
Non-Patent Citations (1)
| Title |
|---|
| 舒文等: ""一种碘蒸汽的回收工艺与装置"", 《医药工程设计》 * |
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Application publication date: 20131002 |