CN103316501B - Percolation device - Google Patents
Percolation device Download PDFInfo
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- CN103316501B CN103316501B CN201310237263.XA CN201310237263A CN103316501B CN 103316501 B CN103316501 B CN 103316501B CN 201310237263 A CN201310237263 A CN 201310237263A CN 103316501 B CN103316501 B CN 103316501B
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- medicinal powder
- shelved
- diacolation
- solvent
- percolate
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- 238000005325 percolation Methods 0.000 title claims abstract description 24
- 239000000843 powder Substances 0.000 claims abstract description 38
- 239000002904 solvent Substances 0.000 claims abstract description 35
- 238000003860 storage Methods 0.000 claims abstract description 12
- 239000007921 spray Substances 0.000 claims description 5
- 239000005336 safety glass Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 10
- 238000000605 extraction Methods 0.000 description 9
- 239000004480 active ingredient Substances 0.000 description 6
- 239000004615 ingredient Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 235000020097 white wine Nutrition 0.000 description 3
- 239000003814 drug Substances 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 208000006820 Arthralgia Diseases 0.000 description 1
- 208000000112 Myalgia Diseases 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 238000000944 Soxhlet extraction Methods 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000005465 channeling Effects 0.000 description 1
- 229940126678 chinese medicines Drugs 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 235000019991 rice wine Nutrition 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 210000000952 spleen Anatomy 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 235000014101 wine Nutrition 0.000 description 1
Landscapes
- Medicines Containing Plant Substances (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention discloses a percolation device which comprises a frame, a total solvent pipeline, a collecting pipeline, a percolation device and a storage barrel, wherein the percolation device is arranged inside the frame, the collecting pipeline is connected with the storage barrel, the percolation device comprises a solvent distributor, a chemical powder mounting frame and a percolate receiving disc from top to bottom, the solvent distributor is connected with the total solvent pipeline, and an outlet of the percolate receiving disc is connected with the collecting pipeline. The percolation device is reasonable in structure, modular in multiple layers, high in production efficiency, and stable and reliable in running.
Description
Technical field
The present invention relates to a kind of Percolation device, more particularly relate to a kind of Percolation device of multilayer fabric.
Background technology
Traditional Chinese medicine extyaction process is the critical process affecting effective ingredient leaching, the extracting mode of current domestic most employing is: percolation, dynamic circulation extraction method, supercritical fluid extraction, ultrasonic wave extraction, intelligent Continuous Countercurrent Extraction method, the ultrasound-enhanced extraction method of continuous flow upstream, soxhlet extraction etc., it respectively has feature, all can carry out the extraction of active ingredient for a certain class feature or whole Chinese medicines.
Percolation is exactly one of effective ways of extract component, and it is mainly for volatilizing, the Extraction and separation of thermally sensitive effective ingredient.Traditional handicraft is that the medicinal material that appropriateness is pulverized is placed in percolator, and constantly add solvent by top, solvent infiltrate medicinal material sulfate layer flows downhill is moved in process and leached medicinal ingredient.Diacolation belongs to Dynamic Leaching method, and solvent utilization rate is high, and active ingredient leaches completely, directly can collect leachate.This method commonly uses the white wine of variable concentrations or white wine makees solvent.And medicinal powder is thinner, the extraction of active ingredient is more abundant, extraction rate and efficiency higher.
Tradition diacolation Percolation device used and method as follows:
(1) single percolation means the normal pressure diacolation method with a percolator.
(2) Repercolation method is that percolate is reused as the solvent of new medicinal powder by two or more percolator arranged in series, carries out repeatedly diacolation to improve the method for percolate concentration.
Tradition diacolation greatest drawback is that medicinal material can only be ground into meal, and stack 6 to 7 times that height must not exceed diacolation bucket diameter, when solvent is used as medicine foundation cream portion from medicinal powder overhead stream, be in content dynamic equilibrium already, concentration gradient difference cannot fully demonstrate, diacolation weak effect; Medicinal material is too thin, and stack excessive height and solvent all can be caused to flow very slowly maybe can not to flow, cannot realize diacolation, production efficiency is low, fluctuation of service.
Summary of the invention
The object of this invention is to provide a kind of rational in infrastructure, multi-layered modular, production efficiency are high, the Percolation device of stable and reliable operation.
The present invention is achieved by the following technical programs:
A kind of Percolation device, comprise framework, total solvent pipeline, collection conduit, percolating device, storage barrel, total solvent pipeline, collection conduit, storage barrel are all arranged on the outside of framework, percolating device is arranged on lower portion, one end of percolating device is connected with total solvent pipeline, the other end is connected with collection conduit, and collection conduit is connected with storage barrel; Lower portion is provided with several diacolation chambeies; Percolating device is arranged in diacolation chamber, and shelved by solution dispenser, medicinal powder from top to bottom, percolate take-up reel forms, solution dispenser is connected with total solvent pipeline, and the outlet of percolate take-up reel is connected with collection conduit.
Object of the present invention can also be realized further by following technical measures.
Aforesaid a kind of Percolation device, medicinal powder is shelved as " drawer class " structure member, and its inside is provided with several cells, and the bottom that medicinal powder is shelved is provided with bolting silk.
Aforesaid a kind of Percolation device, solution dispenser is also provided with a valve in the junction with total solvent pipeline.
Aforesaid a kind of Percolation device, the cell that solution dispenser one_to_one corresponding is shelved in medicinal powder is equipped with mouth spray.
Aforesaid a kind of Percolation device, medicinal powder is shelved, percolate take-up reel is made up of transparent safety glass.
Aforesaid a kind of Percolation device, several diacolation chambeies of framework all can arrange percolating device.
The present invention is compared with traditional Percolation device, heap high separation to 200 object fine powder medicinal powder become some sections to load in the cell shelved of medicinal powder by being crushed to 100 orders, the medicinal powder of identical weight and height is placed in each cell, because solution dispenser is provided with mouth spray, solvent is evenly distributed in each cell by Valve controlling by it, compared with traditional percolating device, reduce or avoid the generation of solvent channeling, greatly improve the efficiency of diacolation and the content of active ingredient; Solution dispenser equal control solvent flows in each cell, makes the active ingredient of solvent and medicinal powder remain the concentration difference of high gradient, and the active ingredient of medicinal powder fast to solvent penetration, can improve diacolation efficiency; Due to medicinal powder shelve, percolate take-up reel makes by transparent safety glass, solution dispenser solvent allocation situation in observable diacolation process, observe the motion state of solvent in medicinal powder, each layer solution dispenser solvent flux can be adjusted at any time, ensure that whole equipment normally runs; Diacolation terminates, and medicinal powder is shelved extraction, pours out medicinal powder slag, simple to operation; And the operation quantity of percolating device can be adjusted according to plan, change the immutable defect of traditional Percolation device, realize modularization, integrated production; the present invention is taken up an area little; configuration is quick, and fixed investment is few, is applicable to the fast integration of reconstruction, enlarging, newly-built large-scale production.
Accompanying drawing explanation
Fig. 1 is Percolation device figure of the present invention;
Fig. 2 is that front view shelved by medicinal powder of the present invention;
Fig. 3 is solution dispenser upward view of the present invention.
Detailed description of the invention
As shown in Figure 1, the present invention includes framework 1, total solvent pipeline 2, collection conduit 3, percolating device 4, storage barrel 5; The inside of framework 1 is provided with 4 diacolation chambeies 11, and each diacolation chamber 11 all can arrange a percolating device 4; Percolating device 4 shelves 42 by solution dispenser 41, medicinal powder from top to bottom, percolate take-up reel 43 forms, solution dispenser 41 is connected with total solvent pipeline 2 by valve 411, the outlet of percolate take-up reel 43 is connected with collection conduit 3, as shown in Figure 2, medicinal powder is shelved 42 inside and is provided with 30 cells 421, and the bottom that medicinal powder shelves 42 is provided with bolting silk 422; As shown in Figure 3, solution dispenser 41 is provided with 30 mouth sprays 412, and cell 421 one_to_one corresponding of 42 shelved by mouth spray 412 and medicinal powder; Collection conduit 3 is connected with storage barrel 5.
This embodiment of diacolation adopting invigorating the spleen to strengthen waist wine effective ingredient is below described further.
As shown in Figure 2, the present embodiment adopts three percolating devices 4, and the cell 421 that each medicinal powder shelves 42 is from top to bottom of a size of 150mm × 150mm, 170mm × 170mm, 200mm × 200mm;
1. the bottom of each medicinal powder being shelved 42 covers with 200 object bolting silks 422, arthralgia and myalgia yeast for brewing rice wine powder 6 is loaded three medicinal powder and shelves 42, the medicinal powder height of cell 421 is respectively 50mm, 60mm, 70mm from top to bottom, medicinal powder is shelved 42 and pushes in diacolation chamber 11.
2. prepare 47 degree of white wine as solvent, open valve 411, keep the surface of solvent higher than medicinal powder 6 of each cell 421, and keep the inflow of solvent and flow out balance, solvent liquid level is substantially constant, flow is respectively 30ml, 50ml, 60ml per minute, and the percolate in percolate take-up reel 43 flows into storage barrel 5 through collection conduit 3.
3. diacolation terminates, and each medicinal powder is shelved 42 pull-outs, pours out the dregs of a decoction, and cleaning medicinal powder shelves 42, the airtight storage of percolate.
In addition to the implementation, the present invention can also have other embodiments, and all employings are equal to the technical scheme of replacement or equivalent transformation formation, all drop in the protection domain of application claims.
Claims (1)
1. a Percolation device, it is characterized in that: comprise framework, total solvent pipeline, collection conduit, percolating device, storage barrel, described total solvent pipeline, collection conduit, storage barrel are all arranged on the outside of framework, described percolating device is arranged on the inside of framework, one end of percolating device is connected with total solvent pipeline, the other end is connected with collection conduit, and described collection conduit is connected with storage barrel; The inside of described framework is provided with several diacolation chambeies; Described percolating device is arranged in diacolation chamber, and shelved by solution dispenser, medicinal powder from top to bottom, percolate take-up reel forms, described solution dispenser is connected with total solvent pipeline, and the outlet of described percolate take-up reel is connected with collection conduit; Described medicinal powder is shelved as " drawer class " structure member, and its inside is provided with several cells, and the bottom that medicinal powder is shelved is provided with bolting silk; Described solution dispenser is also provided with a valve in the junction with total solvent pipeline; The cell that described solution dispenser one_to_one corresponding is shelved in medicinal powder is equipped with mouth spray; Described medicinal powder is shelved, percolate take-up reel is made up of transparent safety glass; Several diacolation chambeies of described framework all can arrange percolating device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310237263.XA CN103316501B (en) | 2013-06-17 | 2013-06-17 | Percolation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310237263.XA CN103316501B (en) | 2013-06-17 | 2013-06-17 | Percolation device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103316501A CN103316501A (en) | 2013-09-25 |
| CN103316501B true CN103316501B (en) | 2015-05-20 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310237263.XA Active CN103316501B (en) | 2013-06-17 | 2013-06-17 | Percolation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103316501B (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202822849U (en) * | 2012-07-20 | 2013-03-27 | 项小孟 | Semi-automatic constant-temperature percolate extraction integrated system |
| CN203329408U (en) * | 2013-06-17 | 2013-12-11 | 江苏七O七天然制药有限公司 | Percolation facility |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1236836C (en) * | 2003-12-08 | 2006-01-18 | 曹培生 | A process for extraction and apparatus thereof |
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2013
- 2013-06-17 CN CN201310237263.XA patent/CN103316501B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202822849U (en) * | 2012-07-20 | 2013-03-27 | 项小孟 | Semi-automatic constant-temperature percolate extraction integrated system |
| CN203329408U (en) * | 2013-06-17 | 2013-12-11 | 江苏七O七天然制药有限公司 | Percolation facility |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103316501A (en) | 2013-09-25 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
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Address after: No. 707, Changjiang Road, Zhenjiang, Jiangsu, 212002 Patentee after: JIANGSU 707 NATURAL PHARMACEUTICAL Co.,Ltd. Country or region after: China Address before: No. 707, Changjiang Road, Zhenjiang, Jiangsu, 212002 Patentee before: JIANGSU 707 NATURAL PHARMACEUTICAL Co.,Ltd. Country or region before: China |