CN103301028B - Lauroyl lysine silky hair conditioner - Google Patents
Lauroyl lysine silky hair conditioner Download PDFInfo
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- CN103301028B CN103301028B CN201310270983.6A CN201310270983A CN103301028B CN 103301028 B CN103301028 B CN 103301028B CN 201310270983 A CN201310270983 A CN 201310270983A CN 103301028 B CN103301028 B CN 103301028B
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- CN
- China
- Prior art keywords
- lauroyl lysine
- hair conditioner
- silky
- hair
- silky hair
- Prior art date
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- GYDYJUYZBRGMCC-INIZCTEOSA-N (2s)-2-amino-6-(dodecanoylamino)hexanoic acid Chemical compound CCCCCCCCCCCC(=O)NCCCC[C@H](N)C(O)=O GYDYJUYZBRGMCC-INIZCTEOSA-N 0.000 title claims abstract description 25
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims abstract description 4
- 208000001840 Dandruff Diseases 0.000 claims description 13
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 claims description 13
- -1 isostearic acid ester Chemical class 0.000 claims description 9
- RHZNQEWFWUODFC-UHFFFAOYSA-N ethyl(dimethyl)azanium;ethyl sulfate Chemical compound CC[NH+](C)C.CCOS([O-])(=O)=O RHZNQEWFWUODFC-UHFFFAOYSA-N 0.000 claims description 8
- XDOFQFKRPWOURC-UHFFFAOYSA-N iso-octadecanoic acid Natural products CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 claims description 8
- WBHHMMIMDMUBKC-XLNAKTSKSA-N ricinelaidic acid Chemical compound CCCCCC[C@@H](O)C\C=C\CCCCCCCC(O)=O WBHHMMIMDMUBKC-XLNAKTSKSA-N 0.000 claims description 8
- 229960003656 ricinoleic acid Drugs 0.000 claims description 8
- FEUQNCSVHBHROZ-UHFFFAOYSA-N ricinoleic acid Natural products CCCCCCC(O[Si](C)(C)C)CC=CCCCCCCCC(=O)OC FEUQNCSVHBHROZ-UHFFFAOYSA-N 0.000 claims description 8
- 239000003795 chemical substances by application Substances 0.000 claims description 7
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 claims description 6
- 239000005770 Eugenol Substances 0.000 claims description 6
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 claims description 6
- 229960002217 eugenol Drugs 0.000 claims description 6
- XVPBINOPNYFXID-JARXUMMXSA-N 85u4c366qs Chemical compound C([C@@H]1CCC[N@+]2(CCC[C@H]3[C@@H]21)[O-])N1[C@@H]3CCCC1=O XVPBINOPNYFXID-JARXUMMXSA-N 0.000 claims description 5
- 229930015582 oxymatrine Natural products 0.000 claims description 5
- 229940043810 zinc pyrithione Drugs 0.000 claims description 5
- PICXIOQBANWBIZ-UHFFFAOYSA-N zinc;1-oxidopyridine-2-thione Chemical compound [Zn+2].[O-]N1C=CC=CC1=S.[O-]N1C=CC=CC1=S PICXIOQBANWBIZ-UHFFFAOYSA-N 0.000 claims description 5
- UUHBCYOCNFWRAH-UHFFFAOYSA-N decyl 16-methylheptadecanoate Chemical compound CCCCCCCCCCOC(=O)CCCCCCCCCCCCCCC(C)C UUHBCYOCNFWRAH-UHFFFAOYSA-N 0.000 abstract description 3
- VDNMPXDJBJILBP-UNUNFZTGSA-N ethyl-[3-[[(z,12r)-12-hydroxyoctadec-9-enoyl]amino]propyl]-dimethylazanium;ethyl sulfate Chemical compound CCOS([O-])(=O)=O.CCCCCC[C@@H](O)C\C=C/CCCCCCCC(=O)NCCC[N+](C)(C)CC VDNMPXDJBJILBP-UNUNFZTGSA-N 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 9
- 239000002994 raw material Substances 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000002453 shampoo Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 3
- 230000005764 inhibitory process Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XVPBINOPNYFXID-LHDUFFHYSA-N Ammothamnine Chemical compound C([C@@H]1CCC[N+]2(CCC[C@H]3[C@@H]21)[O-])N1[C@@H]3CCCC1=O XVPBINOPNYFXID-LHDUFFHYSA-N 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 239000008236 heating water Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 239000000118 hair dye Substances 0.000 description 1
- 230000003699 hair surface Effects 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 229940087096 ricinoleamidopropyl ethyldimonium ethosulfate Drugs 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses lauroyl lysine silky hair conditioner which comprises the following compositions in percentage by weight: 0.2-0.6% of lauroyl lysine, 2-5% of N-(ricinoleamidopropyl)-ethyldimonium ethosulfate, 3-6% of decyl isostearate, 1-3% of glycerol and the balance of water. The lauroyl lysine silky hair conditioner is moistening and soft, capable of increasing hair shining, smooth and fine, and soft like silks.
Description
Technical field:
The present invention relates to a kind of hair conditioner, particularly a kind of Lauroyl lysine silky hair conditioner.
Background technology:
Hair conditioner, also known as Rinsing, general to use with shampoo in pairs, after hair washing by appropriate hair conditioner uniform application on hair, gently rub about one minute, then use clear water rinsed clean, therefore also have person to be rinsing conditioner, belong to hair cosmetic.
It is generally acknowledged, hair is with negative charge.After shampoo (mainly anionic detergent, soap also belongs to this type of) hair washing, hair can be made with more negative charge, thus produce electrostatic, cause combing inconvenience.Employ hair conditioner, main component cation quaternary ammonium salt wherein can neutralize the molecule remaining in hair surface band anion, and leave the uniform monomolecular film of one deck, this layer of marvellous thing can bring a series of benefit to hair: softness, gloss, be easy to combing, antistatic, and the mechanical damage of hair and chemistry scalded, perm, damage that hair dye brings is by reparation to a certain extent.
Summary of the invention:
For prior art above shortcomings, technical problem to be solved by this invention is to provide a kind of Lauroyl lysine silky hair conditioner.
Technical problem of the present invention, is achieved by following technical proposals:
A kind of Lauroyl lysine silky hair conditioner, be made up of following compositions in weight percentage: lauroyl lysine 0.2-0.6%, ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate 2-5%, isostearic acid ester in last of the ten Heavenly stems 3-6%, glycerol 1-3%, surplus is water.
A kind of Lauroyl lysine silky hair conditioner, is made up of following compositions in weight percentage: lauroyl lysine 0.2-0.6%, ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate 2-5%, isostearic acid ester in last of the ten Heavenly stems 3-6%, glycerol 1-3%, anti-dandruff agent 0.4-0.8%, surplus is water.
Described anti-dandruff agent is made up of by weight following component: 20-40 part oxymatrine, 10-30 part eugenol, 40-60 part Zinc Pyrithione.Oxymatrine, eugenol and Zinc Pyrithione simple agitation evenly can be obtained this anti-dandruff agent.
Adopt industry universal method to be prepared, as described in basis " cosmetics principle, formula, production technology " (Wang Peiyi, version in 1999, Chemical Industry Press), the common process of hair conditioner class cosmetics prepares hair conditioner of the present invention.
Further, the preparation method of described Lauroyl lysine silky hair conditioner, comprises the following steps:
(1) ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate and isostearic acid ester in the last of the ten Heavenly stems are stirred at 70-80 DEG C, fusing;
(2), when heating water to 70-80 DEG C, the ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate after above-mentioned fusing and isostearic acid ester in the last of the ten Heavenly stems is added, stirring and emulsifying 10-20 minute;
(3) when being cooled to 40-50 DEG C, add lauroyl lysine, glycerol and anti-dandruff agent, stir 10-20 minute;
(4) be cooled to 25-30 DEG C, obtain described Lauroyl lysine silky hair conditioner.
Concrete, in the present invention:
Lauroyl lysine, English name: LAUROYL LYSINE, CAS accession number: 52315-75-0.
Ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate, No. CAS: 112324-16-0, RICINOLEAMIDOPROPYL ETHYLDIMONIUM ETHOSULFATE.
Glycerol, Glycerol, No. CAS: 56-81-5.
Isostearic acid ester in the last of the ten Heavenly stems, English name: DECYL ISOSTEARATE, No. CAS: 84605-08-3.
Oxymatrine, English name Ammothamnine, No. CAS: 16837-52-8.
Eugenol, English name: Eugenol, No. CAS: 97-53-0.
Zinc Pyrithione, also known as: ZPT; 2-pyridine mercaptan-1-oxygen zinc, English name: PyrithioncZinc, ZPT, No. CAS: 13463-41-7.
Lauroyl lysine silky hair conditioner of the present invention, moistens submissive, and order increases hair gloss, smooth exquisiteness, as fine as silk.Especially, effectively scurf can be dispelled.
Detailed description of the invention:
Embodiment further illustrates of the present invention below, instead of limit the scope of the invention.In the present invention, if no special instructions, each raw material all in working substance content for 100%.
Embodiment 1
Each raw material is taken by embodiment 1 data of table 1 correspondence.
(1) ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate and isostearic acid ester in the last of the ten Heavenly stems are stirred at 75 DEG C, fusing;
(2), when heating water to 75 DEG C, the ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate and isostearic acid ester in the last of the ten Heavenly stems that have melted is added, stirring and emulsifying 15 minutes;
(3) when being cooled to 45 DEG C, add lauroyl lysine, glycerol and anti-dandruff agent, stir 15 minutes;
(4) be cooled to 25 DEG C, obtain described Lauroyl lysine silky hair conditioner.
Table 1: hair conditioner formula table unit: kilogram
Embodiment 2
Each raw material is taken by embodiment 2 data of table 1 correspondence.The method of embodiment 1 is adopted to prepare described Lauroyl lysine silky hair conditioner.
Embodiment 3
Each raw material is taken by embodiment 3 data of table 1 correspondence.The method of embodiment 1 is adopted to prepare described Lauroyl lysine silky hair conditioner.
Embodiment 4
Each raw material is taken by embodiment 4 data of table 1 correspondence.The method of embodiment 1 is adopted to prepare described Lauroyl lysine silky hair conditioner.
Test case:
The hair conditioner obtained to embodiment according to the method disclosed in " foundation of the anti-dandruff effect detection evaluation methodology of shampoo and applied research " carries out inhibition zone diameter test, evaluates anti-dandruff effect of hair conditioner product.Wherein, according to the method for the document, directly change test raw material shampoo into hair conditioner, carry out testing.Inhibition zone diameter is larger, and anti-dandruff effect is better.Test data is in table 2.
Wherein, " foundation of the anti-dandruff effect detection evaluation methodology of shampoo and applied research ", where, Wang Tan, Jia Zebao, Hong Xiaopeng, Peng Jin, research and development department of Si Bao daily use chemicals company limited, household chemicals science, 2009 years o. 11ths.
Table 2: test data table
| Inhibition zone diameter, mm | |
| Embodiment 1 | 14.8 |
| Embodiment 2 | 14.1 |
| Embodiment 3 | 15.2 |
| Embodiment 4 | 17.4 |
Associative list 2 experimental data, can find out: the present invention, initiatively by composite to oxymatrine, eugenol and Zinc Pyrithione use, for anti-dandruff effect, serves obvious synergistic function significantly.
Claims (1)
1. a Lauroyl lysine silky hair conditioner, it is characterized in that, be made up of following compositions in weight percentage: lauroyl lysine 0.2-0.6%, ricinoleic acid amide ethyl dimethyl ammonium ethylsulfate 2-5%, isostearic acid ester in last of the ten Heavenly stems 3-6%, glycerol 1-3%, anti-dandruff agent 0.4-0.8%, surplus is water;
Described anti-dandruff agent is made up of by weight following component: 20-40 part oxymatrine, 10-30 part eugenol, 40-60 part Zinc Pyrithione.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310270983.6A CN103301028B (en) | 2013-06-29 | 2013-06-29 | Lauroyl lysine silky hair conditioner |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310270983.6A CN103301028B (en) | 2013-06-29 | 2013-06-29 | Lauroyl lysine silky hair conditioner |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103301028A CN103301028A (en) | 2013-09-18 |
| CN103301028B true CN103301028B (en) | 2015-07-08 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310270983.6A Expired - Fee Related CN103301028B (en) | 2013-06-29 | 2013-06-29 | Lauroyl lysine silky hair conditioner |
Country Status (1)
| Country | Link |
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| CN (1) | CN103301028B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102011085694A1 (en) * | 2011-11-03 | 2013-05-08 | Beiersdorf Ag | Cosmetic preparation with powdered hydrophilic substances |
| DE102011085688A1 (en) * | 2011-11-03 | 2013-05-08 | Beiersdorf Ag | Cosmetic preparations with powdered hydrophobic substances |
| CN109453084A (en) * | 2018-12-21 | 2019-03-12 | 深圳市萱嘉生物科技有限公司 | A kind of mildy wash and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1557156A1 (en) * | 2003-12-23 | 2005-07-27 | Beiersdorf AG | Cosmetic hair-care composition comprising lauroyl lysine |
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- 2013-06-29 CN CN201310270983.6A patent/CN103301028B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1557156A1 (en) * | 2003-12-23 | 2005-07-27 | Beiersdorf AG | Cosmetic hair-care composition comprising lauroyl lysine |
Non-Patent Citations (1)
| Title |
|---|
| 植物去屑止痒剂的研究现状与展望;胡梅等;《日用化学品科学》;20110228;第34卷(第2期);13-15 * |
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| Publication number | Publication date |
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| CN103301028A (en) | 2013-09-18 |
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| C14 | Grant of patent or utility model | ||
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Effective date of registration: 20170526 Address after: Private science and Technology Park Branch Road No. C03, Baiyun District of Guangzhou City, Guangdong province 510000 Patentee after: Guangzhou thousand fine silk Industrial Development Co.,Ltd. Address before: 510000 unit 2414-2416, building, No. five, No. 371, Tianhe District, Guangdong, China Patentee before: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Effective date of registration: 20170526 Address after: 510000 unit 2414-2416, building, No. five, No. 371, Tianhe District, Guangdong, China Patentee after: GUANGDONG GAOHANG INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: 201111 Shanghai city Minhang District Yuanjiang Road No. 5500 building first room E2128 Patentee before: SHANGHAI YANZI CHEMICAL TECHNOLOGY Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150708 Termination date: 20200629 |