CN103223359A - Split-type physical absorption instrument sample pipe - Google Patents
Split-type physical absorption instrument sample pipe Download PDFInfo
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- CN103223359A CN103223359A CN2013100981741A CN201310098174A CN103223359A CN 103223359 A CN103223359 A CN 103223359A CN 2013100981741 A CN2013100981741 A CN 2013100981741A CN 201310098174 A CN201310098174 A CN 201310098174A CN 103223359 A CN103223359 A CN 103223359A
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- sample cell
- pipe body
- split
- type physical
- physical absorption
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Abstract
The invention belongs to physical experiment instruments, and particularly relates to a split-type physical absorption instrument sample pipe. The split-type physical absorption instrument sample pipe is characterized by being divided into an upper part and a lower part, wherein sand plates or sand cores are accommodated in an upper portion pipe body, the lower end of a lower portion pipe body is closed, and the upper end of the lower portion pipe body is connected with the lower end of the upper portion pipe body in a sealing mode. The lower end of the upper portion pipe body can be a polished opening, the upper end of the lower portion pipe body can be a polished opening, and the lower end of the upper portion pipe body or the upper end of the lower portion pipe body can be cone-shaped bodies or cylindrical bodies. The split-type physical absorption instrument sample pipe can prevent powder or tiny particle samples from being pumped into a system, is simple in structure, is more practical and more convenient to use because of split-type combination on the basis that the basic structure of a prior physical absorption instrument sample pipe is not changed.
Description
Technical field
The invention belongs to a kind of physical experiment apparatus, particularly relate to a kind of split type physical adsorption appearance sample cell.
Background technology
Can obtain the physical parameters such as specific area, pore size distribution, pore volume of material by the physical absorption performance of gases such as test nitrogen etc., at present, normally testing sample is packed in the physical adsorption appearance sample cell (Fig. 1), the sample cell that will contain testing sample then connects with physical adsorption appearance to be tested.In the sample test process, need carry out evacuation processes to remove the impurity of sample surfaces absorption to articles for use.Yet when testing sample is a powder or during than granule, sample is drawn in the system probably in the process of evacuation processes, and then pollutes and damage physical adsorption appearance.
Summary of the invention
At the problems referred to above, the invention provides a kind of split type physical adsorption appearance sample cell, be that a kind of powder or less particulate samples avoided is drawn into sample cell in the system.
Technical scheme of the present invention is as follows:
A kind of split type physical adsorption appearance sample cell, this sample cell are divided into two parts up and down, and the top body contains sand plate or core, the lower end closed of bottom body, and the lower end of the upper end of bottom body and top body is tightly connected.
Further feature, the lower end of top body is a ground, the upper end of bottom body is a ground.
Further feature, the upper end of the lower end of top body or bottom body is a cone, by cone upper and lower port is closely linked together, sealing effectiveness is better.
Further feature, a kind of split type physical adsorption appearance sample cell according to claim 1 is characterized in that the upper end of the lower end of top body and bottom body is a column, and is middle by the column sealed attachment.
The invention has the beneficial effects as follows simple in structurely, on basis on the basic structure that does not change original physical adsorption appearance sample cell, connect by split type, make the physical adsorption appearance sample cell more practical, make things convenient for.
Description of drawings
Fig. 1 is the structural representation of existing physical adsorption appearance sample cell.
The split type physical adsorption appearance sample cell structural representation that Fig. 2 connects for the taper connection.
The split type physical adsorption appearance sample cell structural representation that Fig. 3 connects for the ground connection.
The split type physical adsorption appearance sample cell structural representation that Fig. 4 connects for the column connection.
The specific embodiment
Be described in detail embodiments of the invention below in conjunction with technical scheme and accompanying drawing.
This sample cell structure as shown in Figure 2, this sample cell is divided into two parts up and down: sample cell top is the body of both ends open, sand plate or core A1 are contained in body inside, the sand plate of body inside or core help to prevent that sample is pumped in the system when the sample evacuation processes, play the effect of protection physical adsorption appearance, the lower end of top body is ground A2, mainly is in order to connect the effect of playing sealing with the ground B2 of bottom body; The sample cell bottom is the body of lower end closed upper end band ground B2, and the ground B2 of sample cell bottom body upper end is in order to connect the effect of playing sealing with the ground A2 of top body.
This sample cell structure as shown in Figure 3, this sample cell is divided into two parts up and down: sample cell top is the body of both ends open, sand plate or core A3 are contained in body inside, the sand plate of body inside or core help to prevent that sample is pumped in the system when the sample evacuation processes, play the effect of protection physical adsorption appearance, the lower end of top body is ground A4, mainly is in order to connect the effect of playing sealing with the ground B4 of bottom body; The sample cell bottom is the body of lower end closed upper end band ground B4, and the ground B4 of sample cell bottom body upper end is in order to connect the effect of playing sealing with the ground A4 of top body.
This sample cell structure as shown in Figure 4, this sample cell is divided into two parts up and down: sample cell top is the body of both ends open, sand plate or core A5 are contained in body inside, the sand plate of body inside or core help to prevent that sample is pumped in the system when the sample evacuation processes, play the effect of protection physical adsorption appearance, the lower end of top body is a column; The sample cell bottom is the column of lower end closed upper end open, passes through column A6 sealed attachment between the sample cell upper and lower.
Claims (5)
1. a split type physical adsorption appearance sample cell is characterized in that, this sample cell is divided into two parts up and down, and the top body contains sand plate or core, the lower end closed of bottom body, and the lower end of the upper end of bottom body and top body is tightly connected.
2. a kind of split type physical adsorption appearance sample cell according to claim 1 is characterized in that the lower end of top body is a ground, and the upper end of bottom body is a ground.
3. a kind of split type physical adsorption appearance sample cell according to claim 1 and 2 is characterized in that the upper end of the lower end of top body or bottom body is a cone.
4. a kind of split type physical adsorption appearance sample cell according to claim 1 and 2 is characterized in that the upper end of the lower end of top body and bottom body is a column, and is middle by the column sealed attachment.
5. a kind of split type physical adsorption appearance sample cell according to claim 3 is characterized in that the upper end of the lower end of top body and bottom body is a column, and is middle by the column sealed attachment.
Priority Applications (1)
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CN2013100981741A CN103223359A (en) | 2013-03-25 | 2013-03-25 | Split-type physical absorption instrument sample pipe |
Applications Claiming Priority (1)
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CN2013100981741A CN103223359A (en) | 2013-03-25 | 2013-03-25 | Split-type physical absorption instrument sample pipe |
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CN103223359A true CN103223359A (en) | 2013-07-31 |
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CN2013100981741A Pending CN103223359A (en) | 2013-03-25 | 2013-03-25 | Split-type physical absorption instrument sample pipe |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109030116A (en) * | 2018-06-08 | 2018-12-18 | 海南大学 | A kind of gas absorption adsorption tube |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1024354A1 (en) * | 1997-10-13 | 2000-08-02 | Kikkoman Corporation | Sample collecting member and wiping inspection instrument |
JP2003130764A (en) * | 2001-10-29 | 2003-05-08 | Fukae Kasei Kk | Mini test tube |
EP1752220A1 (en) * | 2005-07-27 | 2007-02-14 | The Automation Partnership (Cambridge) Limited | Sample tube |
CN202061633U (en) * | 2011-02-18 | 2011-12-07 | 中国热带农业科学院分析测试中心 | Novel high-efficiency filtering test tube |
CN202270533U (en) * | 2011-08-30 | 2012-06-13 | 唐煜寒 | Test tube suitable for experiment |
-
2013
- 2013-03-25 CN CN2013100981741A patent/CN103223359A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1024354A1 (en) * | 1997-10-13 | 2000-08-02 | Kikkoman Corporation | Sample collecting member and wiping inspection instrument |
JP2003130764A (en) * | 2001-10-29 | 2003-05-08 | Fukae Kasei Kk | Mini test tube |
EP1752220A1 (en) * | 2005-07-27 | 2007-02-14 | The Automation Partnership (Cambridge) Limited | Sample tube |
CN202061633U (en) * | 2011-02-18 | 2011-12-07 | 中国热带农业科学院分析测试中心 | Novel high-efficiency filtering test tube |
CN202270533U (en) * | 2011-08-30 | 2012-06-13 | 唐煜寒 | Test tube suitable for experiment |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109030116A (en) * | 2018-06-08 | 2018-12-18 | 海南大学 | A kind of gas absorption adsorption tube |
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Application publication date: 20130731 |