CN103214167A - Method for toughening 12mm toughened glass - Google Patents

Method for toughening 12mm toughened glass Download PDF

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Publication number
CN103214167A
CN103214167A CN2013101208411A CN201310120841A CN103214167A CN 103214167 A CN103214167 A CN 103214167A CN 2013101208411 A CN2013101208411 A CN 2013101208411A CN 201310120841 A CN201310120841 A CN 201310120841A CN 103214167 A CN103214167 A CN 103214167A
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CN
China
Prior art keywords
glass
temperature
minute
interval
toughened
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013101208411A
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Chinese (zh)
Inventor
张百庆
韩立平
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HEFEI CHENGXIN GLASS CO Ltd
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HEFEI CHENGXIN GLASS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by HEFEI CHENGXIN GLASS CO Ltd filed Critical HEFEI CHENGXIN GLASS CO Ltd
Priority to CN2013101208411A priority Critical patent/CN103214167A/en
Publication of CN103214167A publication Critical patent/CN103214167A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P40/00Technologies relating to the processing of minerals
    • Y02P40/50Glass production, e.g. reusing waste heat during processing or shaping
    • Y02P40/57Improving the yield, e-g- reduction of reject rates

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  • Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)

Abstract

The invention discloses a method for toughening a piece of 12mm toughened glass. The method comprises the following steps of horizontally placing the glass to be processed onto a roller bed, delivering the glass to be processed into a passage type toughening furnace through the roller bed, sequentially conducting heat treatment at intervals, and cooling two surfaces of the glass through high-pressure air until the surface temperature of the glass reaches 330 to 350 DEG C; placing the glass into 10 to 15 percent potassium nitrate glycerol solution at the temperature of 150 to 160 DEG C to be cooled for 3 to 4 minutes; then placing the glass into the potassium nitrate fused salt at the temperature of 350 to 360 DEG C to be heated for 5 to 6 minutes; and taking out the glass to be naturally cooled in the air. Through the interval heating and cold treatment, the stress distribution on the surface of the glass is adjusted, and the flatness of the toughened glass is guaranteed; and through the treatment in the potassium nitrate glycerol solution and the potassium nitrate fused salt, the toughened degree of the glass surface is increased, the self cracking possibility of the glass in the cooling process can be reduced, the yield of finished products of the toughened glass can be increased, and the performance index requirement of the toughened glass can be met.

Description

12.0mm the tempering processing method of toughened glass
Technical field
The invention belongs to the glass preparation field, be specifically related to the preparation technology of toughened glass.
Technical background
Toughened glass makes it be widely used owing to have higher mechanical strength, good heatproof acute degeneration, good advantages such as security.It is the steel process of heat-eliminating medium that existing toughened glass production process adopts mostly with the air, makes to be heated glass and to carry out Quench at short notice by a large amount of air and handle, thereby finishes the tempering process.In order to guarantee the performance of toughened glass, the air of very big flow need be provided in very short time usually, especially more obvious when tempering approaches glass, select for use the high-power blower of high blast, big flow to dry simultaneously usually.
At present the mode of glass tempering also has the chemical tempering mode, and chemically toughened glass intensity and physical toughened glass are approaching, but overlong time, the low and production cost height of efficient.
Summary of the invention
The tempering processing method that the purpose of this invention is to provide a kind of 12.0mm toughened glass, glass surface stress are evenly, sinuousness, fragment, degree of the temper all meet the requirements.
Technical solution of the present invention is as follows:
12.0mm the tempering processing method of toughened glass is characterized in that may further comprise the steps:
(1), with bath of glass placing flat to be processed to roller-way, deliver in the channel-type annealing furnace by roller-way, heat-treat successively by the interval:
First interval: temperature 280-350 ℃, time 3-5 minute; Second interval: temperature 420-450 ℃, time 4-6 minute; The 3rd interval: temperature 350-380 ℃, 2-3 minute; The 4th interval: temperature 550-600 ℃, time 4-5 minute; The 5th interval: temperature 650-700 ℃, time 5-7 minute;
(2), adopt double-sided glass to carry out high-pressure blast and be cooled to 330-350 ℃ of glass surface temperature;
(3), the saltpetre glycerine solution that glass is added 150-160 ℃ 10-15% cooled off 3-4 minute;
(4), again join in the 350-360 ℃ of saltpetre fused salt, heated 5-6 minute;
(5), take out back air naturally cooling.
 
The present invention is by adopting by stages heating, deepfreeze, regulate the glass surface stress distribution, guaranteed the planeness of toughened glass, handle by saltpetre glycerine solution and saltpetre fused salt, increased the degree of the temper of glass surface, reduce the probability that glass is revealed in process of cooling, improved the yield rate of toughened glass, satisfied the performance index requirement of toughened glass.
Embodiment
12.0mm the tempering processing method of toughened glass may further comprise the steps:
(1), just the bath of glass placing flat is delivered in the channel-type annealing furnace by roller-way to roller-way, heat-treat successively by the interval:
First interval: temperature 320-340 ℃, time 4-5 minute; Second interval: temperature 420-430 ℃, time 4-6 minute; The 3rd interval: temperature 350-380 ℃, 2-3 minute; The 4th interval: temperature 560-600 ℃, time 4-5 minute; The 5th interval: temperature 680-700 ℃, time 5-7 minute;
(2), adopt double-sided glass to carry out high-pressure blast and be cooled to 330-350 ℃ of glass surface temperature;
(3), 15% the saltpetre glycerine solution cooling 4 minutes that glass is added 150-160 ℃;
(4), again glass is joined in the 350-360 ℃ of saltpetre fused salt, heated 5-6 minute;
(5), glass takes out back air naturally cooling.
The toughened glass that processes is detected, and its sinuousness reaches 0.6 ‰, 52 of 50 * 50mm internal fragments, conformance with standard; Degree of the temper=3.4N/cm, the self-destruction rate is 1 ~ 3 ‰.

Claims (1)

1.12.0mm the tempering processing method of toughened glass is characterized in that may further comprise the steps:
(1), with bath of glass placing flat to be processed to roller-way, deliver in the channel-type annealing furnace by roller-way, heat-treat successively by the interval:
First interval: temperature 280-350 ℃, time 3-5 minute; Second interval: temperature 420-450 ℃, time 4-6 minute; The 3rd interval: temperature 350-380 ℃, 2-3 minute; The 4th interval: temperature 550-600 ℃, time 4-5 minute; The 5th interval: temperature 650-700 ℃, time 5-7 minute;
(2), adopt double-sided glass to carry out high-pressure blast and be cooled to 330-350 ℃ of glass surface temperature;
(3), the saltpetre glycerine solution that glass is added 150-160 ℃ 10-15% cooled off 3-4 minute;
(4), again join in the 350-360 ℃ of saltpetre fused salt, heated 5-6 minute;
(5), take out back air naturally cooling.
CN2013101208411A 2013-04-09 2013-04-09 Method for toughening 12mm toughened glass Pending CN103214167A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013101208411A CN103214167A (en) 2013-04-09 2013-04-09 Method for toughening 12mm toughened glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2013101208411A CN103214167A (en) 2013-04-09 2013-04-09 Method for toughening 12mm toughened glass

Publications (1)

Publication Number Publication Date
CN103214167A true CN103214167A (en) 2013-07-24

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CN2013101208411A Pending CN103214167A (en) 2013-04-09 2013-04-09 Method for toughening 12mm toughened glass

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CN (1) CN103214167A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103539341A (en) * 2013-10-31 2014-01-29 南京飞天玻璃实业有限公司 Toughening furnace temperature raising method
CN104045229A (en) * 2014-07-01 2014-09-17 福建省港达玻璃制品有限公司 Preparation process of tempered glass
CN104445896A (en) * 2014-11-28 2015-03-25 张家港市德力特新材料有限公司 Method for preparing tempered glass
CN105216402A (en) * 2014-06-23 2016-01-06 张鹏举 Stained glass panel and its preparation method and application
CN109678329A (en) * 2018-11-27 2019-04-26 安徽友谊钢化玻璃有限公司 A kind of tempered glass preparation process

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1559942A (en) * 2004-02-21 2005-01-05 广东金刚玻璃科技股份有限公司 Method for mfg. high strength fireproof signle sheet cesium potash glass
CN1824619A (en) * 2006-03-17 2006-08-30 中国建筑材料科学研究院 Preparation method of air strengthened glass
US7367205B1 (en) * 2001-09-19 2008-05-06 Boaz Premakaran T System for simultaneously heating and cooling glass

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7367205B1 (en) * 2001-09-19 2008-05-06 Boaz Premakaran T System for simultaneously heating and cooling glass
CN1559942A (en) * 2004-02-21 2005-01-05 广东金刚玻璃科技股份有限公司 Method for mfg. high strength fireproof signle sheet cesium potash glass
CN1824619A (en) * 2006-03-17 2006-08-30 中国建筑材料科学研究院 Preparation method of air strengthened glass

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
上海市硅酸盐学会: "《玻璃译丛 第五辑》", 31 December 1964, article "玻璃的表面钢化", pages: 28 *

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103539341A (en) * 2013-10-31 2014-01-29 南京飞天玻璃实业有限公司 Toughening furnace temperature raising method
CN103539341B (en) * 2013-10-31 2016-04-13 南京飞天玻璃实业有限公司 A kind of temperature-rising method of annealing furnace
CN105216402A (en) * 2014-06-23 2016-01-06 张鹏举 Stained glass panel and its preparation method and application
CN105216402B (en) * 2014-06-23 2017-12-26 张鹏举 Stained glass panel and its preparation method and application
CN104045229A (en) * 2014-07-01 2014-09-17 福建省港达玻璃制品有限公司 Preparation process of tempered glass
CN104045229B (en) * 2014-07-01 2016-06-22 福建省港达玻璃制品有限公司 A kind of preparation technology of safety glass
CN104445896A (en) * 2014-11-28 2015-03-25 张家港市德力特新材料有限公司 Method for preparing tempered glass
CN109678329A (en) * 2018-11-27 2019-04-26 安徽友谊钢化玻璃有限公司 A kind of tempered glass preparation process

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Application publication date: 20130724