CN103204563A - Preparation method for disinfectant fluid based on low temperature plasma - Google Patents
Preparation method for disinfectant fluid based on low temperature plasma Download PDFInfo
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- CN103204563A CN103204563A CN2013100213041A CN201310021304A CN103204563A CN 103204563 A CN103204563 A CN 103204563A CN 2013100213041 A CN2013100213041 A CN 2013100213041A CN 201310021304 A CN201310021304 A CN 201310021304A CN 103204563 A CN103204563 A CN 103204563A
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Abstract
The invention aims to overcome the problems of a peculiar odor and toxic and side effects like residues of a conventional disinfectant fluid and provides a preparation method for a disinfectant fluid based on low temperature plasma. The preparation method comprises the following concrete steps: introducing a certain amount of working gas into a low temperature plasma generating apparatus in virtue of a physical device, i.e., low temperature plasma, and driving the low temperature plasma generating apparatus by using electricity; and weighing a certain amount of water, disposing the apparatus at a position a certain distance above or below a liquid level of an aqueous solution and exciting interaction between plasma and water, wherein after the plasma and the water interact for a certain period of time, the water turns into the disinfectant fluid based on low temperature plasma. The method provided by the invention is simple, highly efficient and environment-friendly; the disinfectant fluid has broad-spectrum high-efficiency sterilization effects and is free of a peculiar odor, corrosivity and chemical residues.
Description
Technical field
The invention belongs to the sterilized water preparation method, be specifically related to the sterilized water preparation method based on low-temperature plasma.
Background technology
Medicine equipment, the sterilization and disinfection of life and office daily necessities etc. is very important.Although present existing sterilization and disinfection product is very many, yet most product adopts the method for chemistry, and often with pungent odour is arranged, corrodibility or toxic side effect such as residual are arranged causes certain threat to HUMAN HEALTH.Be example with the chlorine-containing disinfectant, chlorine-containing disinfectant has cheapness, advantage such as efficient, is widely used in drinking water disinfection, environment disinfected, fields such as health care sterilization, be use in the world at present a class sterilizing agent the most widely.Yet chlorine-containing disinfectant has following shortcoming: (1) hypochlorous acid molecule decomposes in water and discharges gas Cl2, and gas Cl2 is contaminate environment not only, but also can cause shed tears, cough, skin irritation and mucous membrane, severe patient causes poisoning, is choked to death and dies.When working concentration was big, the people was unsuitable on the scene.Therefore, chlorine-containing disinfectant generally should not be applied to disinfection of indoor air.(2) stronger pungency is arranged, generally should not be applied to the sterilization of human body skin and mucous membrane.Therefore a kind of safe, sterilized water is to the protection environment efficiently, human body health has great importance, social benefit is far-reaching.
Plasma body is material the 4th attitude after solid-state, liquid, gaseous state, and when impressed voltage reached the firing voltage of gas, gas molecule was breakdown, produces the mixture that comprises electronics, various ion, atom and free radical.Plasma body can be divided into different classifications: by the thermodynamic(al)equilibrium classification, plasma body can be divided into thermal equilibrium plasma body and nonthermal plasma; Press the system temperature classification, plasma body is divided into low-temperature plasma and high-temperature plasma.The temperature of all particles is all the same in the thermal equilibrium plasma body, shows as high-temperature plasma on the macroscopic view.In nonthermal plasma, the temperature of electronics can be up to tens thousand of degree, and the temperature of ion and neutral particle is much smaller than electronic temp, and whole system presents low-temperature condition, so be also referred to as low-temperature plasma.Low-temperature plasma exists a large amount of, miscellaneous active particle, so nonthermal plasma can be used as the high reactivity reagent utilization in multiple practical applications.
Summary of the invention
The objective of the invention is in order to solve existing sterilized water above shortcomings, a kind of preparation method of the sterilized water based on low-temperature plasma is provided.
Described a kind of sterilized water preparation method based on low-temperature plasma of the present invention, its concrete preparation method is:
(1) with the logical a certain amount of working gas of low-temperature plasma generating unit.
(2) drive the low-temperature plasma generating unit by electricity.
(3) get a certain amount of water, device is positioned on the liquid level of the aqueous solution or certain distance, activated plasma and water mutual effect under the liquid level.
(4) behind plasma body and the water mutual effect certain hour, water namely becomes the sterilized water based on low-temperature plasma of the present invention.
A kind of sterilized water preparation method based on low-temperature plasma of the present invention is characterized in that working gas can be air, the arbitrary proportion mixed gas of gases such as simple substance rare gas or rare gas and oxygen, nitrogen.
A kind of sterilized water preparation method based on low-temperature plasma of the present invention, it is characterized in that described working gas flow velocity be the 0.01-1000 liter/minute.
A kind of sterilized water preparation method based on low-temperature plasma of the present invention is characterized in that described electric driving can be alternating-current or direct current.
A kind of sterilized water preparation method based on low-temperature plasma of the present invention is characterized in that described water can be tap water, distilled water, or ultrapure water.
A kind of sterilized water preparation method based on low-temperature plasma of the present invention is characterized in that scope action time of described plasma body and water is 1ms~10000h.
A kind of sterilized water preparation method based on low-temperature plasma of the present invention, the sterilization and disinfection efficient that it is characterized in that described sterilized water can be according to necessary requirement by adjusting gas ratio, adjusts the interaction time of the volume of water and plasma body and water and regulate.
A kind of sterilized water preparation method based on low-temperature plasma of the present invention is simple, environmental protection.This sterilized water is the spectrum sterilization and disinfection efficiently, nonirritant, and free from extraneous odour uses the back noresidue.
Description of drawings
Fig. 1 acts on the transmission electron microscope picture of streptococcus aureus front and back for sterilized water of the present invention;
Embodiment
The present invention is described in detail with the following Examples.
Embodiment 1:
(1) with the low-temperature plasma generating unit with the 0.01-100 liter/minute flow velocity pass to working gas, working gas is 98% high-purity argon gas (Ar) and 2% high-purity (0
2) mixed gas.
(2) driving power is AC power.
(3) get 20ml distilled water, water is placed 1cm distance under the excitation device, power-on makes plasma body and water mutual effect.
(4) behind plasma body and the water mutual effect 20min, this water becomes sterilized water of the present invention.
In this sterilized water, add 10
8Streptococcus aureus about individual can all be killed all bacteriums in 10min.Fig. 1 acts on the transmission electron microscope picture of streptococcus aureus front and back for sterilized water of the present invention; Before being the sterilized water effect among Figure 1A, bacterial cytoplasm is even, rare cavity, and cell walls is complete.After being the sterilized water effect among Figure 1B, the bacterium interior void increases, the tenuigenin inequality, and cell walls has fragmentation, bacterium death.
Embodiment 2:
(1) with the low-temperature plasma generating unit with the 0.01-100 liter/minute flow velocity pass to working gas, working gas is 98% high-purity helium (He) and 2% high-purity (0
2) mixed gas.
(2) driving power is direct supply.
(3) get 40ml distilled water, water is placed 2cm distance under the excitation device, power-on makes plasma body and water mutual effect.
(4) behind plasma body and the water mutual effect 30min, this water becomes sterilized water of the present invention.
This sterilized water is used for soaking medicine equipments such as medical tweezers, can effectively kills its surperficial objectionable constituent such as bacterium.
The above, it only is one of embodiment of the invention, be not that the present invention is done any pro forma restriction, every technical spirit according to the present invention all still belongs in the scope of technical solution of the present invention any simple modification, equivalent variations and modification that above embodiment does.
Claims (7)
1. sterilized water preparation method based on low-temperature plasma is characterized in that:
(1) with the logical a certain amount of working gas of low-temperature plasma generating unit.
(2) this low-temperature plasma generating unit is driven by electricity.
(3) get a certain amount of water, device is positioned on the liquid level of the aqueous solution or under the liquid level activated plasma and water mutual effect.
(4) behind plasma body and the water mutual effect certain hour, water namely becomes the sterilized water based on low-temperature plasma of the present invention.
2. working gas according to claim 1 can be air, the arbitrary proportion mixed gas of gases such as rare gas or rare gas and oxygen, nitrogen.
Working gas flow velocity according to claim 1 be the 0.01-1000 liter/minute.
4. electric driving according to claim 1 can be alternating-current or direct current.
5. scope action time of plasma body according to claim 1 and water is 1ms~10000h.
6. water according to claim 1 can be tap water, distilled water, or ultrapure water.
7. the sterilization and disinfection efficient of sterilized water according to claim 1 can be by adjusting gas ratio, adjusts the interaction time of the volume of water and plasma body and water and regulate.
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CN2013100213041A CN103204563A (en) | 2013-01-21 | 2013-01-21 | Preparation method for disinfectant fluid based on low temperature plasma |
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CN2013100213041A CN103204563A (en) | 2013-01-21 | 2013-01-21 | Preparation method for disinfectant fluid based on low temperature plasma |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104529044A (en) * | 2015-01-06 | 2015-04-22 | 北京隆冠世纪科技有限公司 | Pure-physical-mode sterilization and disinfection compound water generation device and method |
CN107715141A (en) * | 2017-09-29 | 2018-02-23 | 北京市农林科学院 | A kind of method based on atmos low-temperature plasma activated solution inactivation of viruses |
CN112978847A (en) * | 2021-02-24 | 2021-06-18 | 西安交通大学 | Nitrogen-oxygen ratio-based plasma activated water disinfection device and method |
Citations (5)
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CN2241689Y (en) * | 1996-02-07 | 1996-12-04 | 郭战河 | Activated water generator |
CN2351426Y (en) * | 1997-09-29 | 1999-12-01 | 深圳市精锐实业有限公司 | Plasma oxygen sterilizing water generator |
CN101156955A (en) * | 2007-11-21 | 2008-04-09 | 中山大学 | Non-equilibrium plasma type spray disinfection sanitizer generating apparatus |
WO2011027542A1 (en) * | 2009-09-03 | 2011-03-10 | 国立大学法人大阪大学 | Method and device for supplying ions to liquid, and method and device for sterilizing |
CN102040265A (en) * | 2010-11-09 | 2011-05-04 | 浙江大学 | Method for sterilizing liquid by using along-surface resonant pulse discharge plasma |
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2013
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Patent Citations (5)
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CN2241689Y (en) * | 1996-02-07 | 1996-12-04 | 郭战河 | Activated water generator |
CN2351426Y (en) * | 1997-09-29 | 1999-12-01 | 深圳市精锐实业有限公司 | Plasma oxygen sterilizing water generator |
CN101156955A (en) * | 2007-11-21 | 2008-04-09 | 中山大学 | Non-equilibrium plasma type spray disinfection sanitizer generating apparatus |
WO2011027542A1 (en) * | 2009-09-03 | 2011-03-10 | 国立大学法人大阪大学 | Method and device for supplying ions to liquid, and method and device for sterilizing |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104529044A (en) * | 2015-01-06 | 2015-04-22 | 北京隆冠世纪科技有限公司 | Pure-physical-mode sterilization and disinfection compound water generation device and method |
CN107715141A (en) * | 2017-09-29 | 2018-02-23 | 北京市农林科学院 | A kind of method based on atmos low-temperature plasma activated solution inactivation of viruses |
CN112978847A (en) * | 2021-02-24 | 2021-06-18 | 西安交通大学 | Nitrogen-oxygen ratio-based plasma activated water disinfection device and method |
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Application publication date: 20130717 |