CN103194884A - One-dose one-bath low-temperature type pre-treatment compound preparation - Google Patents
One-dose one-bath low-temperature type pre-treatment compound preparation Download PDFInfo
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- CN103194884A CN103194884A CN2013101197826A CN201310119782A CN103194884A CN 103194884 A CN103194884 A CN 103194884A CN 2013101197826 A CN2013101197826 A CN 2013101197826A CN 201310119782 A CN201310119782 A CN 201310119782A CN 103194884 A CN103194884 A CN 103194884A
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Abstract
The invention relates to a one-dose one-bath low-temperature type pre-treatment compound preparation which comprises the following components in mass percentage: 35.3-52.1% of hydrogen peroxide additive, 11.1-23.1% of peroxysulphate, 2.7-8.0% of sodium hydroxide, 5.5-15.4% of multifunctional additives, 11.8-28.6% of metasilicic acid alkali metal and 2.7-8.0% of surface active agent. According to the compound preparation, multiple functions, such as a refining function, a bleaching function, a permeating function and the like, are integrated into a whole; one-dose effect of a pre-treatment agent is realized; inconvenient operation caused by a plurality of dosage forms and troubles, such as time consumption, labour consumption, material consumption and the like, in the production process are avoided; the use amount of auxiliary additives, such as sodium hydroxide and the like, is reduced; annealing, boiling and bleaching processes in pre-treatment are combined into the one-bath method; the process flow is simplified; simultaneously, the pre-treatment temperature is reduced; the comprehensive production cost is also reduced; and the one-dose one-bath low-temperature type pre-treatment compound preparation disclosed by the invention has good application prospect.
Description
Technical field
The invention belongs to pre-treatment compound formulation field, particularly a kind of potion one is bathed low form pre-treatment compound formulation.
Background technology
The traditional pretreating technology for printing and dyeing of the many employings of textile industry relies on strong acid, highly basic and high temperature that COTTON FABRIC is handled, and this has not only damaged fibre strength, and has increased the wastewater treatment difficulty, causes serious environmental to pollute.Along with the enhancing of people's environmental consciousness and the raising of environmental regulation threshold, energy-conserving and environment-protective technology has become the technology of printing and dyeing producer active demand.
CN102587121A discloses a kind of solid low temperature pre-treatment compound formulation.Can reduce treatment temperature though the enzyme preparation in the above-mentioned file and oxygen float activator, still have following a few point defect: the composition of one, composite enzyme preparation changes, and has a strong impact on the effect to kiering and bleaching; Two, enzyme is to the sensitiveness of temperature, pH, oxidant, with the reappearance of the whole technology of influence; Three, the consumption of bleach-activating is higher, and the auxiliary agent cost is higher.
CN102704259A discloses a kind of low temperature scouring and bleaching agent and the application in cotton and BLENDED FABRIC pre-treatment process thereof thereof.Though the low temperature in the above-mentioned file is scouringed and bleaching agent with most of auxiliary agent in the pre-treatment process in addition compounded combination become potion, still need hydrogen peroxide to cooperate during its bleaching and bleach, thereby can not be referred to as the pre-treatment preparation of a real formulation.
Summary of the invention
Technical problem to be solved by this invention provides a kind of potion one and bathes low form pre-treatment compound formulation, this compound formulation can be with traditional high temperature high alkaline scouring bleaching process be improved to the few soda boiling of low temperature one of the unification of scouringing and bleaching and bathe abbreviated system, economic environmental protection and to the pre-treatment effect excellence of COTTON FABRIC.
A kind of potion one of the present invention is bathed low form pre-treatment compound formulation, by mass percentage, by hydrogen peroxide additive 35.3%～52.1%, persulfate 11.1%～23.1%, caustic soda 2.7%～8.0%, multifunctional assistant 5.5%～15.4%, metasilicic acid alkali metal 11.8%～28.6% and surfactant 2.7%～8.0% are formed.
Described hydrogen peroxide additive is one or both in perborate, the percarbonate.
Described percarbonate is SODIUM PERCARBONATE 2Na
2CO
33H
2O
2
Described persulfate is potassium peroxydisulfate K
2S
2O
8, sodium peroxydisulfate Na
2S
2O
8, ammonium persulfate (NH
4)
2S
2O
8In one or more.
Described persulfate is sodium peroxydisulfate Na
2S
2O
8
Described multifunctional assistant is anionic scouring agent, nonionic scouring agent or by they composite scouring agents that obtains.Selected multifunctional assistant is required to be solid forms and will has the good penetration performance, for example multifunctional assistant KF-110 or DM-1116 etc.
Described metasilicic acid alkali metal is one or both in sodium metasilicate, the potassium metasilicate.
Described sodium metasilicate is anhydrous or moisture, for example anhydrous sodium metasilicate Na
2SiO
3With metasilicate pentahydrate sodium Na
2SiO
35H
2O.
Described surfactant is anion or the nonionic solid bleeding agent with good wet osmotic effect, as Nekal BX.
Described compound formulation by mass percentage, by SODIUM PERCARBONATE 2Na
2CO
33H
2O
242.9%, sodium peroxydisulfate Na
2S
2O
814.3%, caustic soda 7.1%, KF-1107.1%, sodium metasilicate Na
2SiO
321.4% and Nekal BX 7.2% form.
Further improvement of the present invention is: one, the oxidation system that adopts two oxidants to work in coordination with bleaching have overcome the bad bleachability of percarbonate bleach; Two, replace the dyeing and finishing processing method of the mode replace complex of multi-agent with a kind of potion, improved production efficiency, and energy-saving and environmental protection.
Beneficial effect
Multiple functions such as that the present invention integrates is concise, bleaching, infiltration have realized a thinner of pretreating reagent, the operation inconvenience that multi-form brings in having avoided producing, troubles such as consuming time, consumption worker, consumptive material; Reduce the consumption of auxiliary addition agents such as caustic soda, with single bath process moving back of pre-treatment boiled and float unification, simplified technological process; Reduced the temperature of pre-treatment simultaneously, also reduced the integrated cost of producing, had a good application prospect.
The specific embodiment
Below in conjunction with specific embodiment, further set forth the present invention.Should be understood that these embodiment only to be used for explanation the present invention and be not used in and limit the scope of the invention.Should be understood that in addition those skilled in the art can make various changes or modifications the present invention after the content of having read the present invention's instruction, these equivalent form of values fall within the application's appended claims institute restricted portion equally.
Embodiment 1
Bathe low form pre-treatment compound formulation according to table 1 ratio preparation potion one:
Table 1
Embodiment 2
Bathe low form pre-treatment compound formulation according to table 2 ratio preparation potion one:
Table 2
Embodiment 3
According to bathing low form pre-treatment compound formulation as following table 3 ratios preparation potion one:
Table 3
Embodiment 4
According to bathing low form pre-treatment compound formulation as following table 4 ratios preparation potion one:
Table 4
The low form potion that obtains among the above embodiment one is bathed the pre-treatment compound formulation preparation pre-treatment solution 1～4 that is added to the water, and in 80 ℃ pure cotton knitted fabric is carried out pre-treatment, obtain table 5 corresponding data:
Table 5
By table 5 as seen, reached the quality requirement of textiles pre-treatment through the product quality of potion one bath low form pre-treatment compound formulation pre-treatment provided by the present invention, when effectively reducing the pre-treatment temperature, processing mode with potion one bath, shortened technological process, simplify operation, reduced the integrated cost of pre-treatment.
Claims (10)
1. a potion one is bathed low form pre-treatment compound formulation, it is characterized in that: by mass percentage, by hydrogen peroxide additive 35.3%～52.1%, persulfate 11.1%～23.1%, caustic soda 2.7%～8.0%, multifunctional assistant 5.5%～15.4%, metasilicic acid alkali metal 11.8%～28.6% and surfactant 2.7%～8.0% are formed.
2. a kind of potion one according to claim 1 is bathed low form pre-treatment compound formulation, and it is characterized in that: described hydrogen peroxide additive is one or both in perborate, the percarbonate.
3. a kind of potion one according to claim 2 is bathed low form pre-treatment compound formulation, and it is characterized in that: described percarbonate is SODIUM PERCARBONATE 2Na
2CO
33H
2O
2
4. a kind of potion one according to claim 1 is bathed low form pre-treatment compound formulation, and it is characterized in that: described persulfate is potassium peroxydisulfate K
2S
2O
8, sodium peroxydisulfate Na
2S
2O
8, ammonium persulfate (NH
4)
2S
2O
8In one or more.
5. a kind of potion one according to claim 4 is bathed low form pre-treatment compound formulation, and it is characterized in that: described persulfate is sodium peroxydisulfate Na
2S
2O
8
6. a kind of potion one according to claim 1 is bathed low form pre-treatment compound formulation, and it is characterized in that: described multifunctional assistant is KF-110 or DM-1116.
7. a kind of potion one according to claim 1 is bathed low form pre-treatment compound formulation, and it is characterized in that: described metasilicic acid alkali metal is one or both in sodium metasilicate, the potassium metasilicate.
8. a kind of potion one according to claim 7 is bathed low form pre-treatment compound formulation, and it is characterized in that: described sodium metasilicate is anhydrous or moisture.
9. a kind of potion one according to claim 1 is bathed low form pre-treatment compound formulation, and it is characterized in that: described surfactant is Nekal BX.
10. a kind of potion according to claim 1 is bathed low form pre-treatment compound formulation, it is characterized in that: described compound formulation by mass percentage, by SODIUM PERCARBONATE 2Na
2CO
33H
2O
242.9%, sodium peroxydisulfate Na
2S
2O
814.3%, caustic soda 7.1%, KF-1107.1%, sodium metasilicate Na
2SiO
321.4% and Nekal BX 7.2% form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310119782.6A CN103194884B (en) | 2013-04-08 | 2013-04-08 | One-dose one-bath low-temperature type pre-treatment compound preparation |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310119782.6A CN103194884B (en) | 2013-04-08 | 2013-04-08 | One-dose one-bath low-temperature type pre-treatment compound preparation |
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|---|---|
| CN103194884A true CN103194884A (en) | 2013-07-10 |
| CN103194884B CN103194884B (en) | 2015-01-21 |
Family
ID=48717691
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|---|---|---|---|
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103590238A (en) * | 2013-11-25 | 2014-02-19 | 南通泰慕士服装有限公司 | Low-temperature pretreatment process of cotton fabrics |
| CN103774412A (en) * | 2013-12-26 | 2014-05-07 | 江苏华超纺织实业有限公司 | Wool pretreatment method |
| CN105350337A (en) * | 2015-12-18 | 2016-02-24 | 常熟市爱尚纺织科技有限公司 | Printing and dyeing pre-treatment process of cotton fabric |
| CN106758390A (en) * | 2016-12-08 | 2017-05-31 | 佛山迅拓奥科技有限公司 | Bath processing Polyfunctional Compounded Agent of a kind of refining bleaching dyeing one and its preparation method and application |
| CN111733022A (en) * | 2020-07-21 | 2020-10-02 | 何结平 | Cleaning agent for printing and dyeing soaping and preparation method thereof |
| CN111962285A (en) * | 2020-08-04 | 2020-11-20 | 天津工业大学 | Bleaching agent for yakwool and processing method |
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|---|---|---|---|---|
| EP0315848A2 (en) * | 1987-11-07 | 1989-05-17 | BASF Aktiengesellschaft | Process for the pretreatment of textile materials |
| CN101418513A (en) * | 2008-10-28 | 2009-04-29 | 宁波新阳纺织印染有限公司 | One dosage form solid additive for cotton knitted fabric one bath boiling and bleaching process at low temperature |
| CN102505472A (en) * | 2011-11-22 | 2012-06-20 | 东华大学 | Method for low-temperature one-bath-one-step pretreatment of pure cotton woven fabric through biomimetic metal |
| CN102587111A (en) * | 2012-02-09 | 2012-07-18 | 武汉新华扬生物股份有限公司 | Low-temperature scouring and bleaching one-bath-process pretreatment process of cotton knitted fabrics |
| CN102839533A (en) * | 2012-09-15 | 2012-12-26 | 濮阳宏业汇龙化工有限公司 | Short-process pre-treatment scouring agent for textile and preparation method thereof |
-
2013
- 2013-04-08 CN CN201310119782.6A patent/CN103194884B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0315848A2 (en) * | 1987-11-07 | 1989-05-17 | BASF Aktiengesellschaft | Process for the pretreatment of textile materials |
| CN101418513A (en) * | 2008-10-28 | 2009-04-29 | 宁波新阳纺织印染有限公司 | One dosage form solid additive for cotton knitted fabric one bath boiling and bleaching process at low temperature |
| CN102505472A (en) * | 2011-11-22 | 2012-06-20 | 东华大学 | Method for low-temperature one-bath-one-step pretreatment of pure cotton woven fabric through biomimetic metal |
| CN102587111A (en) * | 2012-02-09 | 2012-07-18 | 武汉新华扬生物股份有限公司 | Low-temperature scouring and bleaching one-bath-process pretreatment process of cotton knitted fabrics |
| CN102839533A (en) * | 2012-09-15 | 2012-12-26 | 濮阳宏业汇龙化工有限公司 | Short-process pre-treatment scouring agent for textile and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103590238A (en) * | 2013-11-25 | 2014-02-19 | 南通泰慕士服装有限公司 | Low-temperature pretreatment process of cotton fabrics |
| CN103774412A (en) * | 2013-12-26 | 2014-05-07 | 江苏华超纺织实业有限公司 | Wool pretreatment method |
| CN105350337A (en) * | 2015-12-18 | 2016-02-24 | 常熟市爱尚纺织科技有限公司 | Printing and dyeing pre-treatment process of cotton fabric |
| CN106758390A (en) * | 2016-12-08 | 2017-05-31 | 佛山迅拓奥科技有限公司 | Bath processing Polyfunctional Compounded Agent of a kind of refining bleaching dyeing one and its preparation method and application |
| CN111733022A (en) * | 2020-07-21 | 2020-10-02 | 何结平 | Cleaning agent for printing and dyeing soaping and preparation method thereof |
| CN111962285A (en) * | 2020-08-04 | 2020-11-20 | 天津工业大学 | Bleaching agent for yakwool and processing method |
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| Publication number | Publication date |
|---|---|
| CN103194884B (en) | 2015-01-21 |
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Address after: 201620 No. 2999 Renmin Road, Songjiang District new town, Shanghai Co-patentee after: Jiangsu Tamus Textile Technology Co., Ltd Patentee after: DONGHUA University Address before: 201620 No. 2999 Renmin Road North, Songjiang new town, Shanghai, Songjiang District Co-patentee before: NANTONG TIMES CLOTHING Co.,Ltd. Patentee before: DONGHUA University |