CN103191029A - Mouthwash, homemaking machine, preparation method, and application - Google Patents
Mouthwash, homemaking machine, preparation method, and application Download PDFInfo
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- CN103191029A CN103191029A CN2012100011149A CN201210001114A CN103191029A CN 103191029 A CN103191029 A CN 103191029A CN 2012100011149 A CN2012100011149 A CN 2012100011149A CN 201210001114 A CN201210001114 A CN 201210001114A CN 103191029 A CN103191029 A CN 103191029A
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Abstract
The invention discloses a mouthwash, a homemaking machine, a preparation method, and an application. The mouthwash is water containing stably dissolved ozone. According to the homemaking machine and the preparation method, oxygen in air or pure oxygen is converted into ozone gas by using an ozone generation device; the produced ozone gas is delivered into water by using an aeration device, and is converted into stably dissolved ozone in water; and residual un-dissolved ozone gas is absorbed or degraded by using a tail gas absorption or degradation device. As a result of experiments, the mouthwash provided by the invention is nonirritating and causes no chemical residue. The mouthwash can be homemade, and can be used in cleaning oral cavity, removing oral odor, relieving toothache, bleaching teeth, killing oral, gum and dental plaques, and preventing and treating caries, periodontal diseases and orally infectious diseases. When the mouthwash is applied for a long term, no significant side effect is caused.
Description
Technical field
The present invention relates to the collutory field, particularly, relate to a kind of collutory, self-control machine, preparation method and application.
Background technology
Illness finds its way in by the mouth, and the normal person oral cavity often has pathogenic bacterium to exist, and what mainly cause oral disease is the bacterial plaque of growing on the tooth, and removing these bacterial plaques is the main tasks that keep oral cavity cleaning and prevention oral disease.The mode of the bactericidal cleaning speckle in oral cavity has two kinds at present, a kind of is that another kind is to use the collutory that contains chemical constituent, uses the back all to have chemical substance residual in the oral cavity with ordinary toothbrush and the toothpaste that the contains chemical constituent cleaning oral cavity of brushing teeth, can not swallow, the child uses inconvenience.Therefore, a kind of effective collutory that does not have chemical residual of the manufacturing of needs is arranged.
Can cleaning oral cavity with chemical collutory, caries prevention and periodontitis etc., but its constituent complexity depend on the quality of collutory more, and the most effective collutory is Listerin at present.The Listerin collutory has the strong mouthfeel of killing, and the child is reluctant to use.Therefore, there are needs to make a kind of strong effective collutory that kills mouthfeel that do not have.
Periodontal disease is the main cause that the old people falls tooth, also is one of disease that is caused by oral cavity and gingiva pathogenic bacterium.Traditional Therapeutic Method is to use hydrogen peroxide to gargle, and hydrogen peroxide is strong oxidizer, does not kill mouthful, does not have residual chemicals, and the effect of prevention such as strong sterilization taste removal and treatment oral disease is arranged.But the pH value of hydrogen peroxide is not physiological pH, also has the tooth decalcification, can not life-time service, can not make by oneself at home.Therefore, be necessary to seek a kind ofly do not kill mouthful, no chemical residual, the oxidant that can make by oneself at home and the oral cavity is had no side effect safely, cleaning oral cavity, prevention and treat the collutory of oral disease.
Summary of the invention
The objective of the invention is to overcome the shortcoming and defect of above-mentioned prior art, provide a kind of and do not kill mouthful, no chemical residual, can make by oneself at home, to the oral cavity have no side effect safely, the collutory of cleaning oral cavity, prevention and treatment oral disease.
Another object of the present invention is to provide the self-control machine of above-mentioned collutory.
The 3rd purpose of the present invention is to provide the preparation method of above-mentioned collutory.
The 4th purpose of the present invention is to provide the application of above-mentioned collutory.
To achieve these goals, the present invention adopts following technical scheme:
A kind of collutory is for containing the water of stablizing dissolved ozone.
Further, the concentration of described stable dissolved ozone is 0.53-5mg/l.
A kind of collutory self-control machine, comprise the body of being made up of main storehouse and secondary storehouse, described main storehouse is provided with entery and delivery port, and main storehouse comprises sump and the superposed tail gas storehouse that is positioned at the bottom, main storehouse inner bottom part is provided with aerator, is provided with ozone generating-device and control device in the secondary storehouse; Described control device is connected with ozone generating-device, and ozone generating-device is connected with aerator by pipeline; Also be provided with tail gas absorption or decomposition apparatus in the described body.
Further, also comprise a pure oxygen generator that is connected with ozone generating-device.
Further, described ozone generating-device comprises the air pump that has the gas access and the ozonator that is connected with described air pump, comprises that also is arranged on a fan that is connected with ozonator in the secondary storehouse.
Further, described tail gas absorption or decomposition apparatus are arranged in the secondary storehouse, and are communicated with by the tail gas storehouse of pipeline with top, main storehouse, and described tail gas absorption or decomposition apparatus are activated-charcoal column, uviol lamp, ultraviolet is in conjunction with photocatalyst degraded post or add the thermal degradation post.
Further, described control device comprises power supply and the transformator that is connected with power supply.
Further, the outside, secondary storehouse of described body also is provided with handle.
A kind of preparation method of collutory, at first adopt ozone generating-device that airborne oxygen or pure oxygen are converted into gas ozone, the recycling aerator feeds the stable dissolved ozone that changes in the water in the water with the gas ozone that produces, and remaining undissolved gas ozone is by tail gas absorption or decomposition apparatus absorption or degraded.
Above-mentioned collutory can be applicable to cleaning oral cavity, remove halitosis, alleviate have a toothache, bleaching teeth, kill, the bacterial plaque on gingiva and the tooth, prevention and treating in dental caries, periodontal disease and the peroral infection disease in the oral cavity in.
Compared with prior art, the present invention has following beneficial effect:
1, the stable dissolved ozone that contains in the collutory of the present invention is one of the most effective oxidant, its efficient sterilizing (stronger nearly 1,000 times than chlorine efficient), kill the virus, eliminate the unusual smell, bleaching teeth, do not kill mouthful, final catabolite is oxygen, the noresidue chemical substance, can make by oneself at home, be desirable prevention and the collutory for the treatment of oral disease.
2, collutory self-control machine of the present invention use gas ozone by aeration in water in the short time (in two minutes) make the stable dissolved ozone of valid density, do not have harmful gas ozone to leak simultaneously, the harm environment.
3, the preparation method of collutory of the present invention is to utilize ozone generating-device that air (containing 21% oxygen) or pure oxygen are converted into ozone, adopts the bottom aeration process, makes dissolved ozone in the water.Simultaneously, the present invention overcomes deficiency of the prior art, adopt ozone tail gas absorption or decomposition apparatus (comprising that active carbon or other adsorbents or ultraviolet or ultraviolet are in conjunction with photocatalyst or heating ozone degradation technology) effectively to remove unemployed residual gas ozone, the manufacturing high-concentration ozone water of safety.
4, collutory self-control machine of the present invention mainly is divided into amphitypy, first type is air source collutory self-control machine, second type is the pure oxygen source collutory self-control machine that has the pure oxygen generator, through experimental verification, adopt collutory of the present invention in the collutory that making mechanism is equipped with, to contain the stable dissolved ozone of high concentration, can effectively prevent and treat oral disease, keep oral hygiene and health, life-time service has no side effect simultaneously, tests as follows:
(1) first type collutory self-control machine each run two minutes, the collutory that produces after testing, find no detectable gas ozone spill (＜0.05ppm), prove that this machine security performance is good.
(2) first type collutorys self-control machine each run two minutes, the collutory that produces is dissolved ozone in potassium iodide titration measuring water, finds that the dissolved oxygen level of ozone at 0.6 ± 0.07mg/l, proves that collutory contains the high concentration dissolved ozone.
(3) first type collutorys self-controls machine each run two minutes moves twice every day, finds no gas ozone through trial run in a year and leaks, and proves the collutory of can safe manufacturing stablize dissolved ozone and makes machine by oneself.
The Ozone Water that the operation of (4) first type collutory self-control machines produced in two minutes, bright through the checking of human body exterior-excess, 100% bactericidal action is arranged, in human oral cavity, gargle and experimental results show that the effect of removing halitosis, dental bleaching, killing oral cavity bacterium, also mouthfeel and abnormal flavour sense extremely of proof of experiment in body, life-time service can obviously reduce the toothache frequency.The Ozone Water that the operation of the first type collutory self-control machine produced in two minutes meets the standard of desirable collutory, comprise efficient sterilizing, eliminate the unusual smell, bleaching teeth, do not kill mouthful, final catabolite is oxygen, the noresidue chemical substance, can make by oneself at home, be desirable prevention and the collutory for the treatment of oral disease.
(5) twice experiment in totally one year of gargling every day in human oral cavity, the result shows and does not see oral mucosa, gingiva, tooth, parageusia namely do not have significant side effects.
The Ozone Water that the operation of (6) first type collutory self-control machines produced in two minutes was gargled after six seconds, the collutory that spues do not measure dissolved ozone (＜0.05mg/l), show in the collutory dissolved ozone with intraoral substance reaction, all be transformed into oxygen and noresidue, can swallow.
(7) second type collutorys self-controls machine each run two minutes, the collutory that produces detects through gas ozone, find no detectable gas ozone spill (＜0.05ppm), prove that this machine security performance is good.
(8) second type collutorys self-control machine each run two minutes, the collutory that produces is dissolved ozone in potassium iodide titration measuring water, finds that the dissolved oxygen level of ozone at 4.8 ± 0.2mg/l, proves that collutory contains the high concentration dissolved ozone.
(9) second type collutorys self-controls machine each run two minutes moves twice every day, finds no gas ozone through trial run in a year and leaks, and proves the collutory of can safe manufacturing stablize dissolved ozone and makes machine by oneself.
To the treatment experiment of periodontal disease, gargling altogether twice every day, trimestral result shows that the second type collutory machine has good therapeutical effect to the periodontal disease patient to (10) second type collutorys self-controls machine in human oral cavity.
The twice trimestral experiment altogether of gargling every day in human oral cavity of (11) second type collutorys self-controls machine, the result shows and does not see oral mucosa, gingiva, tooth, parageusia namely do not have significant side effects.
Below by drawings and Examples, technical scheme of the present invention is described in further detail.
Description of drawings
Fig. 1 is collutory self-control machine structure principle chart of the present invention;
Fig. 2 looks sketch map for a collutory self-control machine structure of the present invention left side;
Fig. 3 looks sketch map for the collutory self-control machine structure of the present invention right side;
Fig. 4 looks sketch map for collutory self-control machine structure master of the present invention;
Fig. 5 is collutory self-control machine structure schematic rear view of the present invention;
Fig. 6 is collutory self-control machine structure schematic top plan view of the present invention;
Fig. 7 is collutory self-control machine structure elevational schematic view of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing the preferred embodiments of the present invention are described, should be appreciated that preferred embodiment described herein only is used for description and interpretation the present invention, and be not used in restriction the present invention.
Shown in Fig. 2-7, collutory self-control machine (first type) of the present invention, comprise the body of being formed by main storehouse 1 and secondary storehouse 2, main storehouse 1 is provided with entery and delivery port 3, main storehouse 1 comprises sump 4 and the superposed tail gas storehouse 5 that is positioned at the bottom, main storehouse 1 inner bottom part is provided with aerator 6, is provided with ozone generating-device 7 and control device 8 in the secondary storehouse 2; Ozone generating-device 7 comprises the air pump 10 that has gas access 9 and the ozonator 11 that is connected with air pump 10, comprises that also is arranged on a fan 12 that is connected with ozonator 11 in the secondary storehouse 2; Control device 8 comprises power supply and the transformator that is connected with power supply; Control device 8 is connected with the air pump 10 of ozone generating-device 7, and the ozonator 11 of ozone generating-device 7 is connected with aerator 6 by pipeline; In the secondary storehouse 2 of body, also be provided with tail gas absorption or decomposition apparatus 13, tail gas absorption or decomposition apparatus 13 bottoms are provided with tail gas outlet 14, the top of tail gas absorption or decomposition apparatus 13 is communicated with by the tail gas storehouse 5 of pipeline with 1 top, main storehouse, and tail gas absorption or decomposition apparatus 13 are activated-charcoal column, uviol lamp, ultraviolet is in conjunction with photocatalyst degraded post or add the thermal degradation post.
2 outsides, secondary storehouse at body also are provided with handle 15.
As shown in Figure 1, collutory self-control machine of the present invention (first type) is that air (containing 21% oxygen) is produced gas ozone (by control device control) through ozone generating-device (air pump and ozonator), recycling sump bottom aerator imported it into the stable dissolved ozone of making valid density in the water in the water in two minutes, remaining ozone tail gas utilizes tail gas absorption or decomposition apparatus all to adsorb or degrade the no residual ozone leakage of safety in the tail gas storehouse.This Ozone Water (collutory) has and protects the health of one's mouth, caries prevention and periodontal disease, prevention import communicate illness, removes halitosis and bleaching teeth effect.The no chemical residual material of this Ozone Water (collutory) can be swallowed after gargling, and is applicable to the crowd of all age brackets.
The collutory self-control machine (second type) of present embodiment is on the basis of embodiment 1, subsidiary have one can control flow at the pure oxygen generator of 1-3l/min, use pure oxygen through the dissolved ozone of ozone generating-device generation high-concentrated ozone and water middle and high concentration, this ozone with high concentration water (collutory) has the effect for the treatment of periodontal disease.
Experimental example 1
Purpose: the oxidation treatment method oxidability experiment of collutory self-control machine of the present invention.
Method: use collutory self-control machine of the present invention, basic parameter sees Table 1, and ozone generating-device can be converted into ozone (O with oxygen in the air
3), utilize the bottom aerator further to make dissolved ozone.Ozone (O
3) be a kind of strong oxidizer, with potassium iodide (KI) the reactant aqueous solution elemental iodine that dissociates.As indicator, elemental iodine and starch reaction manifest blueness with starch solution, with finite concentration sodium thiosulfate (Na
2S
2O
3) standard solution carries out titration, just can calculate ozone amount according to the consumption of sodium thiosulfate standard solution.Its reaction equation is:
O
3+2KI+H
2O——O
2+I
2+2KOH (1)
I
2+2Na
2S
2O
3——2NaI+Na
2S
4O
6 (2)
Table 1 experiment basic parameter table
Table 2 is measured in the water and ozone amount in the tail gas
1. air is source of the gas; 2. pure oxygen is source of the gas; Temperature is room temperature 22 degree.
Conclusion: the oxidation treatment method of collutory of the present invention self-control machine can produce stable dissolved ozone, and very strong oxidability is arranged, and ozone tail gas is oxygen after activated-charcoal column decomposes, and human body is not had potential safety hazard.The generation dissolved ozone can also be removed the chlorine residue in the tap water in two minutes, the mouthfeel extremely that can avoid chlorine residue to cause in water.
Experimental example 2
Purpose: the removal of bacteria effect experiment of collutory self-control machine of the present invention.
Method: use collutory self-control machine of the present invention, basic parameter sees Table 3, uses air or pure oxygen to do source of the gas, and (the control bacterial density is 1.5 * 10 with escherichia coli
4Cfu/ml), be inoculated in the collutory that collutory self-control machine of the present invention produces, compare experiment in the tap water with being inoculated into, determine the bactericidal effect of this collutory.
Table 3 experiment basic parameter table
The bactericidal effect of table 4 collutory
1. air is source of the gas; 2. pure oxygen is source of the gas.
Conclusion: collutory of the present invention self-control machine, no matter with air still be oxygen as source of the gas, the Ozone Water of generation is collutory, efficiently kill bacteria.
Experimental example 3
Purpose: determine that collutory self-control machine of the present invention is to removal of bacteria effect in the human mouth.
Method: use collutory self-control machine of the present invention, basic parameter sees Table 5, as follows to the mode of gargling taked for examination crowd (experiment totally 7 people): matched group uses pure water to gargle earlier 4 seconds, back calibrating bacterial population (cfu/ml) spues, re-use sterilized water and gargled 2 seconds, back calibrating clump count (cfu/ml) spues; First kind of first collutory that uses the first type collutory to make from making mechanism of situation gargled 4 seconds, re-used sterilized water and gargled 2 seconds, and back calibrating clump count (cfu/ml) spues; Second kind of situation is that the collutory that uses the second type collutory to make from making mechanism was earlier gargled 4 seconds, re-uses sterilized water and gargles 2 seconds, and back calibrating clump count (cfu/ml) spues.The removal of bacteria rate of the collutory of making from making mechanism and second mouthful of clump count that produces of matched group compare.
Table 5 experiment basic parameter table
Table 6 removal of bacteria situation
1. first kind of situation is the air source of the gas; 2. second kind of situation is the pure oxygen source of the gas.
Conclusion: collutory of the present invention self-control machine, no matter with air still be oxygen as source of the gas, the Ozone Water of generation is collutory, can efficiently kill oral cavity bacterium.Experimental result is also pointed out, and repeatedly gargles and may utterly destroy intraoral pathogenic flora with life-time service.
Experimental example 4
Purpose: determine that collutory self-control machine of the present invention is to cleaning and the nursing experiment of human mouth.
Method: the collutory that uses collutory self-control machine of the present invention (basic parameter sees Table 7) to produce, the experiment in totally one year of gargling for twice for each person every day (the experiment number is 5 people), observation experiment result.
Table 7 experiment basic parameter table
Conclusion: collutory self-control machine of the present invention, no matter adopt air still be pure oxygen be source of the gas, move the Ozone Water of generation in two minutes, there is 100% bactericidal action in oral cavity to the people, first six months is observed halitosis, the dental bleaching of removing, kill oral cavity bacterium, reduces the effect of gingival hemorrhage and toothache.
Back continuation in six months long term test, result show does not see oral mucosa, gingiva, tooth, parageusia, does not namely have significant side effects.
Experimental example 5
Purpose: first type collutory self-control machine is to the preventive effect of dental caries.
Method: 24 of 7 years old children at selection multiple age of dental caries, 14 of men, 10 of woman are divided into two groups, every group of 12 people at random.Check the dental caries situation of suffering from, and the existing dental caries situation of record.Matched group is non-treatment group, and experimental group is the collutory treatment group of collutory self-control machine first type preparation.The collutory 150ml that experimental group uses the preparation of collutory self-control machine first type gargled for 4 seconds at every turn, till 150ml has gargled, every day sooner or later respectively twice, treated altogether 1 year.The laboratory observation index is for finding the number of new dental caries.
Experimental result: experimental result shows that the collutory that uses the preparation of collutory self-control machine first type (150ml gargled for 4 seconds at every turn, till 150ml has gargled, respectively twice sooner or later of every day) has prevented the generation of dental caries fully.
Table 8 first type collutory self-control machine is to the preventive effect of dental caries
| Group | Observe | The new trouble dental caries | Caries prevalence rate |
| Number | The tooth number | (％) | |
| Matched |
12 | 3 | 25 |
| |
12 | 0 | 0 |
Discuss and conclusion: the collutory that uses the preparation of collutory self-control machine first type is in external kill bacteria that can 100%, (150ml repeatedly gargles in human oral cavity, gargled for 4 seconds at every turn, till 150ml has gargled, each twice sooner or later of every day) obviously having prevented the generation of dental caries, may be by the powerful bactericidal effect of collutory (collutory contain stablize dissolved ozone 0.6mg/l).Analyze through an example, find that the collutory of collutory self-control machine first type preparation has tangible antihalitosis, prevent from having a toothache and the function of cleaning oral cavity.In addition, also find to use the collutory of collutory self-control machine first type preparation that existing dental caries is had the obvious treatment effect, comprise stoping that dental caries is made progress, relieved the pain etc.By analysis, think that the superpower Oxidation of collutory with dental caries sealing, sterilization, has prevented further developing of dental caries.
Experimental example 6
Purpose: the application of collutory self-control machine.
Method: (the collutory ozone concentration of first type preparation is 0.6 ± 0.07mg/L to use collutory of the present invention to make the collutory of machine generation in 2 minutes by oneself; The Ozone Water ozone concentration of collutory self-control machine second type (collutory self-control machine first type+oxygen cylinder) preparation is that 4.8 ± 0.2mg/L and 0.2% hibitane contrast, the crowd is chosen as: subjects is healthy various odontopathy patients, totally 28 examples, male 18 examples, women 10 examples; Age 35～65.Patient's gingival hemorrhage, redness, pain, swelling, plaque index has halitosis more than 2 grades.Be divided into four groups at random, every group of 7 people.First group is non-treatment matched group, and second group is 0.2% hibitane treatment matched group, and the 3rd group is the collutory treatment group of collutory self-control machine first type preparation, and the 4th group is the collutory treatment group of collutory self-control machine second type preparation.Do not use other any medicine in 2 weeks, do not discontinue medication midway.
Administrated method: the matched group water is gargled, and each 150ml gargled for 4 seconds, till 150ml has gargled at every turn; The each 10ml of 0.2% hibitane, every day 3 times.After tasty and refreshing, more than the rinsing the mouth 2min clock.The collutory 150ml of collutory self-control machine first type and the preparation of second type gargled for 4 seconds at every turn, and till 150ml had gargled, each treatment group treated for 2 weeks altogether.
Criterion: produce effects: the gingiva outward appearance is normal, and pain disappears, and halitosis disappears, and spy is examined not hemorrhage, and plaque index improves 1 more than the rank; Effectively: the gingiva outward appearance is normal substantially, pain relief, and halitosis alleviates, and spy gum bottom of trench has hemorrhage, and plaque index improves 0.5 more than the rank; Invalid: no significant change before and after the treatment.
Result and conclusion:
The result shows that the collutory of collutory self-control machine first type preparation is suitable with 0.2% hibitane effect, and the collutory of collutory self-control machine second type preparation is obviously better than 0.2% hibitane effect.Individual example the analysis showed that the collutory of collutory self-control machine first type and the preparation of second type all has the positive effect of eliminating and easing toothache, eliminate and alleviate halitosis, elimination and the swelling of minimizing gingival hemorrhage and reduction bacterial plaque.
Table 9 therapeutic test result
1. collutory is made the collutory of machine first type preparation by oneself; 2. collutory is made the collutory of machine second type preparation by oneself.
Can prove that by above experimental example collutory self-control facility of the present invention have safe use value.
It should be noted that at last: the above only is the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment the present invention is had been described in detail, for a person skilled in the art, it still can be made amendment to the technical scheme that previous embodiment is put down in writing, and perhaps part technical characterictic wherein is equal to replacement.Within the spirit and principles in the present invention all, any modification of doing, be equal to replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. a collutory is characterized in that, for containing the water of stablizing dissolved ozone.
2. collutory according to claim 1 is characterized in that, the concentration of described stable dissolved ozone is 0.53-5mg/l.
3. a collutory is made machine by oneself, it is characterized in that, comprise the body of being formed by main storehouse and secondary storehouse, described main storehouse is provided with entery and delivery port, main storehouse comprises sump and the superposed tail gas storehouse that is positioned at the bottom, main storehouse inner bottom part is provided with aerator, is provided with ozone generating-device and control device in the secondary storehouse;
Described control device is connected with ozone generating-device, and ozone generating-device is connected with aerator by pipeline;
Also be provided with tail gas absorption or decomposition apparatus in the described body.
4. collutory self-control machine according to claim 3 is characterized in that, also comprises a pure oxygen generator that is connected with ozone generating-device.
5. according to claim 3 or 4 described collutory self-control machines, it is characterized in that, described ozone generating-device comprises the air pump that has the gas access and the ozonator that is connected with described air pump, comprises that also is arranged on a fan that is connected with ozonator in the secondary storehouse.
6. according to claim 3 or 4 described collutory self-control machines, it is characterized in that, described tail gas absorption or decomposition apparatus are arranged in the secondary storehouse, and be communicated with by the tail gas storehouse of pipeline with top, main storehouse, described tail gas absorption or decomposition apparatus are activated-charcoal column, uviol lamp, ultraviolet is in conjunction with photocatalyst degraded post or add the thermal degradation post.
7. according to claim 3 or 4 described collutory self-control machines, it is characterized in that described control device comprises power supply and the transformator that is connected with power supply.
8. according to claim 3 or 4 described collutory self-control machines, it is characterized in that the outside, secondary storehouse of described body also is provided with handle.
9. the preparation method of a collutory, it is characterized in that, at first adopt ozone generating-device that airborne oxygen or pure oxygen are converted into gas ozone, the recycling aerator feeds the stable dissolved ozone that changes in the water in the water with the gas ozone that produces, and remaining undissolved gas ozone is by tail gas absorption or decomposition apparatus absorption or degraded.
Collutory according to claim 1 and 2 can be applied in cleaning oral cavity, remove halitosis, alleviate have a toothache, bleaching teeth, kill, the bacterial plaque on gingiva and the tooth, prevention and treating in dental caries, periodontal disease and the peroral infection disease in the oral cavity in.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100011149A CN103191029A (en) | 2012-01-04 | 2012-01-04 | Mouthwash, homemaking machine, preparation method, and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012100011149A CN103191029A (en) | 2012-01-04 | 2012-01-04 | Mouthwash, homemaking machine, preparation method, and application |
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| CN103191029A true CN103191029A (en) | 2013-07-10 |
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| CN111467266A (en) * | 2020-05-14 | 2020-07-31 | 深圳市陆讯纳米科技有限公司 | Ozone nano-bubble mouthwash and preparation method thereof |
| CN111467266B (en) * | 2020-05-14 | 2022-10-28 | 深圳市陆讯纳米科技有限公司 | Ozone nano-bubble gargle and preparation method thereof |
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