CN103145904B - Uniform ion exchange resin granule production equipment - Google Patents

Uniform ion exchange resin granule production equipment Download PDF

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Publication number
CN103145904B
CN103145904B CN201310078307.9A CN201310078307A CN103145904B CN 103145904 B CN103145904 B CN 103145904B CN 201310078307 A CN201310078307 A CN 201310078307A CN 103145904 B CN103145904 B CN 103145904B
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China
Prior art keywords
monomer
tank
ion exchange
exchange resin
heating tank
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CN201310078307.9A
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Chinese (zh)
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CN103145904A (en
Inventor
杨奇
郭小奎
王行
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BENBU TIANXING RESIN CO LTD
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BENBU TIANXING RESIN CO LTD
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Priority to CN201310078307.9A priority Critical patent/CN103145904B/en
Publication of CN103145904A publication Critical patent/CN103145904A/en
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Abstract

The invention relates to uniform ion exchange resin granule production equipment, and belongs to the field of resin production equipment. The uniform ion exchange resin granule production equipment comprises a monomer generation system and a monomer forming system, wherein the monomer generation system comprises a monomer box and a fluidized pipeline; the top of the monomer box is connected with the fluidized pipeline, and the bottom of the monomer box is provided with a raw material inlet and a liquid discharge port; the outer wall of the monomer box is provided with a viewing mirror; the monomer box is internally provided with a shower spray head, and the monomer box is connected with a vibrating motor; the connecting position of the monomer box and the fluidized pipeline is provided with a ripple compensator; the monomer forming system comprises a fluidized tank and a heating tank; the fluidized tank is provided with an upper cover; the upper cover is provided with an air exhaust port; the bottom of the fluidized tank is connected with the heating tank through a flange; the fluidized tank and the heating tank are provided with fluid circulating pipelines; the fluid circulating pipelines are connected with a circulation motor; and the bottom of the heating tank is provided with a discharge port. The uniform ion exchange resin granule production equipment disclosed by the invention can improve the diameter uniformity of ion exchange resin monomer granules, enhances the product spheroidization rate, reduces the cost and increases the production efficiency.

Description

A kind of Uniform ion exchange resin granule production equipment
Technical field
The present invention relates to production of resins equipment technical field, be specifically related to a kind of Uniform ion exchange resin granule production equipment.
Background technology
Ion exchange resin is widely used in the industry such as material purification, water treatment, catalyzed reaction, medical separation and purification and scientific research field, and its matrix is the pearl body generated by suspension copolymerization by vinylbenzene, divinylbenzene.Ion exchange resin bead footpath in practical application all must control in certain scope according to requirements.
In current industrial suspension polymerization technique, main employing reactor stirs to shear and produces monomer particle, owing to stirring the reasons such as shearing force spatial distribution is uneven in reactor, the monomer granularity that produces can be caused uneven and have quite a few Archon granularity undesirable.Production cost can be increased like this, increase energy consumption, waste resource, and larger environmental pollution can be caused.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of structure improvement, the Uniform ion exchange resin granule production equipment that result of use is good.
Technical problem to be solved by this invention realizes by the following technical solutions:
A kind of Uniform ion exchange resin granule production equipment, comprises monomer and produces system and monomer formation system, it is characterized in that: described monomer is produced system and is connected by pipeline with monomer formation system;
Described monomer produces system and comprises one-piece box and fluidisation pipeline, described one-piece box top is connected with fluidisation pipeline, bottom is provided with feed(raw material)inlet, leakage fluid dram, outer wall is provided with visor, for observing monomer, inside is provided with shower nozzle, and described one-piece box is connected with vibration motor, and described one-piece box and fluidisation pipeline junction are provided with FlexbleJoint;
Described monomer formation system comprises streaming tank and heating tank, described streaming tank is provided with upper cover, on cover and be provided with venting port, heating tank is had by Flange joint bottom described streaming tank, streaming tank and heating tank are provided with fluid circulation pipe, fluid circulation pipe is connected with circulation motor, bottom described heating tank, is provided with discharge port, described heating tank and streaming tank are equipped with visor.
The invention has the beneficial effects as follows: the present invention can improve the diameter homogeneity of ion exchange resin monomer particle, improve product and obtain ball rate, reduce costs, enhance productivity.
Accompanying drawing explanation
Fig. 1 is a kind of Uniform ion exchange resin granule production equipment structural representation of the present invention.
Wherein: 1-monomer produces system; 2-monomer formation system; 3-one-piece box; 4-fluidisation pipeline; 5-feed(raw material)inlet; 6-leakage fluid dram; 7-visor; 8-shower nozzle; 9-vibration motor; 10-FlexbleJoint; 11-streaming tank; 12-heating tank; 13-upper cover; 14-venting port; 15-flange; 16-fluid circulation pipe; 17-circulation motor; 18-discharge port.
Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with concrete diagram, setting forth the present invention further.
As shown in Figure 1, a kind of Uniform ion exchange resin granule production equipment, comprises monomer and produces system 1 and monomer formation system 2, and monomer is produced system 1 and is connected by pipeline with monomer formation system 2; Monomer produces system 1 and comprises one-piece box 3 and fluidisation pipeline 4, one-piece box 3 top is connected with fluidisation pipeline 4, bottom is provided with feed(raw material)inlet 5, leakage fluid dram 6, outer wall is provided with visor 7, for observing monomer, inside is provided with shower nozzle 8, and one-piece box 3 is connected with vibration motor 9, and one-piece box 3 and fluidisation pipeline 4 junction are provided with FlexbleJoint 10;
Monomer formation system 2 comprises streaming tank 11 and heating tank 12, streaming tank 11 is provided with upper cover 13, upper cover 13 is provided with venting port 14, heating tank 12 is connected with by flange 15 bottom streaming tank 11, streaming tank 11 and heating tank 12 are provided with fluid circulation pipe 16, fluid circulation pipe 16 is connected with circulation motor 17, bottom heating tank 12, is provided with discharge port 18, heating tank 12 and streaming tank 11 are equipped with visor 7.
Principle of work of the present invention is: raw material injects shower nozzle 8 from feed(raw material)inlet 5, shower nozzle 8 connecting vibration motor 9, the size that shower nozzle 8 ejects monomer is controlled by regulating vibrating motor 9, the monomer formed enters streaming tank 11 through fluidisation pipeline 4, by regulating circulation motor 17 to control the flow velocity of the liquid in streaming tank 11, the temperature controlling liquid in heating tank 12 by regulating heating tank 12 provides optimal temperature for monomer reaction.Because the density before monomer reaction is less than fluid density in streaming tank 11, therefore monomer can flow to the upper end of streaming tank 11 because of the effect of buoyancy, and the monomer of the liquid and floating in streaming tank 11 with certain flow rate produces reactive force, thus make monomer rest on streaming tank 11 internal fixtion region to complete monomer reaction formation finished product, finished product density after monomer reaction is greater than the fluid density in streaming tank 11, finished product sinks to the bottom of heating tank 12 gradually, and draws off from discharge port 18.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.

Claims (1)

1. a Uniform ion exchange resin granule production equipment, comprises monomer and produces system and monomer formation system, it is characterized in that: described monomer is produced system and is connected by pipeline with monomer formation system;
Described monomer produces system and comprises one-piece box and fluidisation pipeline, described one-piece box top is connected with fluidisation pipeline, bottom is provided with feed(raw material)inlet, leakage fluid dram, outer wall is provided with visor, for observing monomer, inside is provided with shower nozzle, and described one-piece box is connected with vibration motor, and described one-piece box and fluidisation pipeline junction are provided with FlexbleJoint;
Described monomer formation system comprises streaming tank and heating tank, described streaming tank is provided with upper cover, on cover and be provided with venting port, heating tank is had by Flange joint bottom described streaming tank, streaming tank and heating tank are provided with fluid circulation pipe, fluid circulation pipe is connected with circulation motor, bottom described heating tank, is provided with discharge port, described heating tank and streaming tank are equipped with visor.
CN201310078307.9A 2013-03-12 2013-03-12 Uniform ion exchange resin granule production equipment Active CN103145904B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310078307.9A CN103145904B (en) 2013-03-12 2013-03-12 Uniform ion exchange resin granule production equipment

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Application Number Priority Date Filing Date Title
CN201310078307.9A CN103145904B (en) 2013-03-12 2013-03-12 Uniform ion exchange resin granule production equipment

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CN103145904A CN103145904A (en) 2013-06-12
CN103145904B true CN103145904B (en) 2015-04-29

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103657542A (en) * 2013-10-17 2014-03-26 刘东升 Particle surface treating plant
CN103657541A (en) * 2013-10-17 2014-03-26 刘东升 Particle surface treating plant

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4487898A (en) * 1981-06-12 1984-12-11 Kanegafuchi Chemical Industry Co., Ltd. Process of continuous suspension polymerization
CN102086240A (en) * 2010-12-22 2011-06-08 天津大学 Equipment and method for producing uniform particle ion exchange resin beads
CN102502646A (en) * 2011-10-10 2012-06-20 中国科学院过程工程研究所 Equipment and method for preparing polysilicon by fast circulating fluidized bed-based chemical vapor deposition
CN202527137U (en) * 2012-03-09 2012-11-14 中国石油天然气股份有限公司 Preparation device for spherical particles
CN203174013U (en) * 2013-03-12 2013-09-04 蚌埠市天星树脂有限责任公司 Uniform ion exchange resin particle production equipment

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4487898A (en) * 1981-06-12 1984-12-11 Kanegafuchi Chemical Industry Co., Ltd. Process of continuous suspension polymerization
CN102086240A (en) * 2010-12-22 2011-06-08 天津大学 Equipment and method for producing uniform particle ion exchange resin beads
CN102502646A (en) * 2011-10-10 2012-06-20 中国科学院过程工程研究所 Equipment and method for preparing polysilicon by fast circulating fluidized bed-based chemical vapor deposition
CN202527137U (en) * 2012-03-09 2012-11-14 中国石油天然气股份有限公司 Preparation device for spherical particles
CN203174013U (en) * 2013-03-12 2013-09-04 蚌埠市天星树脂有限责任公司 Uniform ion exchange resin particle production equipment

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