CN103143189A - Process improvement system for preparing alanyl-glutamine - Google Patents

Process improvement system for preparing alanyl-glutamine Download PDF

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Publication number
CN103143189A
CN103143189A CN2013100768863A CN201310076886A CN103143189A CN 103143189 A CN103143189 A CN 103143189A CN 2013100768863 A CN2013100768863 A CN 2013100768863A CN 201310076886 A CN201310076886 A CN 201310076886A CN 103143189 A CN103143189 A CN 103143189A
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CN
China
Prior art keywords
pipe
tank
crystallizing tank
shower nozzle
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2013100768863A
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Chinese (zh)
Inventor
邢将军
许刘华
王洪芳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NANTONG CHENGXIN AMINO ACID CO Ltd
Original Assignee
NANTONG CHENGXIN AMINO ACID CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NANTONG CHENGXIN AMINO ACID CO Ltd filed Critical NANTONG CHENGXIN AMINO ACID CO Ltd
Priority to CN2013100768863A priority Critical patent/CN103143189A/en
Publication of CN103143189A publication Critical patent/CN103143189A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a process improvement system for preparing alanyl-glutamine, which comprises a feeding pipe, a pre-crystallizing tank, a material pipe, a crystallizing tank, a discharging pipe, an air pressure device, a water supply device, an air pipeline and a spray head, wherein the feeding pipe is connected with the pre-crystallizing tank; the crystallizing tank is connected with the pre-crystallizing tank through the material pipe; the discharging pipe is connected with the crystallizing tank; the water supply device comprises a water pump, a water tank and a water pipe; the air pipeline is connected with the air pressure device; the interior of the spray head is an aerial fog extension cavity; and the air pipeline is communicated with the water pipe and the aerial fog extension cavity of the spray head. By adopting the process improvement system for preparing alanyl-glutamine disclosed by the invention in the process production process, the production yield can be increased.

Description

A kind of process modification system for preparing alanyl glutamine
Technical field
The technology of the present invention relates to chemical field, particularly the technique preparation field of alanyl glutamine.
Background technology
In the industrial production of preparation alanyl glutamine, crystallization apparatus is the key equipment of commonly using.In the process of alanyl glutamine crystallization, the crystallization of generation easily is attached to and forms harder brilliant scar on the wall of crystallisation chamber, on especially cold wall, is difficult to peace and quietly, and needing regularly stops carries out thoroughly peace and quietly, and the production maintenance difficulty is large.Say in a certain sense, the cycle of operation of crystallization apparatus has affected the process cycle of whole alanyl glutamine.
Existing crystallization apparatus is equipped with condenser system and water system, and water pipe rinses the crystallization apparatus inwall, and is often bad but water directly washes away the effect of crystallization apparatus inwall, expend a large amount of water, do not reach the purpose of the brilliant scar of cleaning, the crystalline solid through washing away is affected crystallization yield by excess dilution.
Summary of the invention
Goal of the invention: for overcoming defects, the invention provides a kind of simple in structure, cost is low, improve the process system of crystallization yield.
Technical scheme: a kind of process modification system for preparing alanyl glutamine, comprise feed pipe, pre-crystallized tank, material pipe, crystallizing tank, discharge nozzle, air compressing device, water supply installation, air duct, shower nozzle, described feed pipe is connected with pre-crystallized tank, described crystallizing tank is connected with described pre-crystallized tank by described material pipe, described discharge nozzle is connected with this crystallizing tank, and described water supply installation comprises water pump, tank, water pipe; Described air duct is connected with described air compressing device, is the aerosol extended cavity in described shower nozzle, and described air duct is connected with the aerosol extended cavity of this shower nozzle with described water pipe.
As preferably, described aerosol extended cavity is vortex structure, is snakelike arrangement by the multiple layer metal dividing plate.
As preferably, a plurality of spray orifices are arranged on described shower nozzle, be regular annular array.
As preferably, be divided into a plurality of confined chambers in described crystallizing tank, described confined chamber is connected with described material pipe; Described shower nozzle has a plurality of, is connected with described each confined chamber respectively.
As preferably, described material pipe is the hydrocone type pipe.
Useful effect: because water pipe, air compressing device are connected with the aerosol extended cavity of shower nozzle respectively, compressed air and water under high pressure enter after the aerosol extended cavity at snakelike vortex structure high speed rotary-atomizing, then spray through jet rose, form simultaneously powerful underbalance effect, greatly strengthened scouring force, reduce water consumption, improved crystallization yield.
Description of drawings
Fig. 1 is structural representation of the present invention;
Fig. 2 is shower nozzle schematic internal view of the present invention;
Fig. 3 is shower nozzle schematic diagram of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing and instantiation, type technology of the present invention is described further, but protection scope of the present invention is not limited to following example.For those skilled in the art; under enlightenment of the present invention; can directly derive the identical basic deformation of some principles of association from this patent disclosure; or the substituting of known technology commonly used in prior art; and the identical mutual various combination of feature, the technical characterictic of same or similar technique effect simply change, and all belongs to the protection domain of the technology of the present invention.
As Fig. 1, Fig. 2, shown in Figure 3, a kind of process modification system for preparing alanyl glutamine, comprise feed pipe 1, pre-crystallized tank 2, material pipe 3, crystallizing tank 4, discharge nozzle 5, air compressing device 6, water supply installation, air duct 8, shower nozzle 9, described feed pipe 1 is connected with pre-crystallized tank 2, described crystallizing tank 4 is connected with described pre-crystallized tank 2 by described material pipe 3, described discharge nozzle 5 is connected with this crystallizing tank 4, and described water supply installation comprises water pump 11, tank 10, water pipe 7; Described air duct 8 is connected with described air compressing device 6, is the aerosol extended cavity in described shower nozzle 9, and described air duct 8 is connected with the aerosol extended cavity of this shower nozzle 9 with described water pipe 7.Be divided into a plurality of confined chambers in described crystallizing tank 4, described confined chamber is connected with described material pipe 3; Described shower nozzle 9 has a plurality of, is connected with described each confined chamber respectively.
Described material pipe 3 is the hydrocone type pipe, both can to convey materials in crystallizing tank, the material in crystallizing tank can be sucked back again.
Described aerosol extended cavity is vortex structure, is snakelike arrangement by multiple layer metal dividing plate 12; A plurality of spray orifices 13 are arranged on described shower nozzle 9, be regular annular array.Because water pipe 7, air compressing device 6 are connected with the aerosol extended cavity of shower nozzle 9 respectively, compressed air and water under high pressure enter after the aerosol extended cavity at snakelike vortex structure high speed rotary-atomizing, then spray through jet rose, form simultaneously powerful underbalance effect, greatly strengthened scouring force, reduce water consumption, improved simultaneously crystallization yield.

Claims (5)

1. process modification system for preparing alanyl glutamine, comprise feed pipe (1), pre-crystallized tank (2), material pipe (3), crystallizing tank (4), discharge nozzle (5), air compressing device (6), water supply installation, air duct (8), shower nozzle (9), described feed pipe (1) is connected with pre-crystallized tank (2), described crystallizing tank (4) is connected with described pre-crystallized tank (2) by described material pipe (3), described discharge nozzle (5) is connected with this crystallizing tank (4), described water supply installation comprises water pump (11), tank (10), water pipe (7), described air duct (8) is connected with described air compressing device (6), it is characterized in that: be the aerosol extended cavity in described shower nozzle (9), described air duct (8) is connected with the aerosol extended cavity of described water pipe (7) with this shower nozzle (9).
2. the process modification system of preparation alanyl glutamine according to claim 1, it is characterized in that: described aerosol extended cavity is vortex structure, is snakelike arrangement by multiple layer metal dividing plate (12).
3. the process modification system of preparation alanyl glutamine according to claim 1, is characterized in that: a plurality of spray orifices (13) are arranged on described shower nozzle (9), be regular annular array.
4. the process modification system of preparation alanyl glutamine according to claim 1, it is characterized in that: described crystallizing tank is divided into a plurality of confined chambers in (4), and described confined chamber is connected with described material pipe (3); Described shower nozzle (9) has a plurality of, is connected with described each confined chamber respectively.
5. the process modification system of described preparation alanyl glutamine one of according to claim 1-4, it is characterized in that: described material pipe (3) is the hydrocone type pipe.
CN2013100768863A 2013-03-12 2013-03-12 Process improvement system for preparing alanyl-glutamine Pending CN103143189A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2013100768863A CN103143189A (en) 2013-03-12 2013-03-12 Process improvement system for preparing alanyl-glutamine

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Application Number Priority Date Filing Date Title
CN2013100768863A CN103143189A (en) 2013-03-12 2013-03-12 Process improvement system for preparing alanyl-glutamine

Publications (1)

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CN103143189A true CN103143189A (en) 2013-06-12

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104561202A (en) * 2015-02-06 2015-04-29 江苏诚信药业有限公司 Preparation method and technological system for enzymatically synthesizing N(2)-L-alanyl-L-glutamine

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2555903Y (en) * 2002-06-28 2003-06-18 云南亚太环境工程设计研究有限公司 Negative pressure ammonium sulfate concentration crystallizing tank
CN102190677A (en) * 2010-03-03 2011-09-21 中国石油天然气股份有限公司 Atomization synthesizer and application thereof in synthesis of alkylaluminoxane
CN203108257U (en) * 2013-03-12 2013-08-07 南通诚信氨基酸有限公司 Process improvement system for preparing alanyl-glutamine

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2555903Y (en) * 2002-06-28 2003-06-18 云南亚太环境工程设计研究有限公司 Negative pressure ammonium sulfate concentration crystallizing tank
CN102190677A (en) * 2010-03-03 2011-09-21 中国石油天然气股份有限公司 Atomization synthesizer and application thereof in synthesis of alkylaluminoxane
CN203108257U (en) * 2013-03-12 2013-08-07 南通诚信氨基酸有限公司 Process improvement system for preparing alanyl-glutamine

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104561202A (en) * 2015-02-06 2015-04-29 江苏诚信药业有限公司 Preparation method and technological system for enzymatically synthesizing N(2)-L-alanyl-L-glutamine

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Application publication date: 20130612