CN103121782B - Mud low pressure hot water solution treatment process and application thereof - Google Patents
Mud low pressure hot water solution treatment process and application thereof Download PDFInfo
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- CN103121782B CN103121782B CN201210212079.5A CN201210212079A CN103121782B CN 103121782 B CN103121782 B CN 103121782B CN 201210212079 A CN201210212079 A CN 201210212079A CN 103121782 B CN103121782 B CN 103121782B
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Abstract
The invention belongs to technical field of sludge treatment, and disclose a kind of mud low pressure hot water solution treatment process and application thereof, the method comprises: be that the mud of 70-97% injects in reactor by water ratio; In reactor, inject the saturation steam of 1.0-1.59MPa, when the temperature of mud reaches 150 ~ 180 DEG C, stop injecting saturation steam and mud after obtaining thermal hydrolysis after keeping 0 ~ 30 minute.Thermal hydrolysis treatment process of the present invention can be used for processing organic solid castoff.Thermal hydrolysis treatment process of the present invention is applicable to the mud of multiple water ratio, and without the need to carrying out any pre-treatment to mud before the reaction; Because the present invention adopts the saturation steam of below 1.6MPa to heat mud, the thermal hydrolysis reaction unit of low pressure configurations therefore can be adopted as reactor, effectively reduce equipment investment cost, corresponding maintenance cost and operator's cost also decline; Thermal hydrolysis treatment temp is lower, thus significantly can reduce the time be heated to by mud required for certain treatment temp, and then reduces energy consumption and running cost.
Description
Technical field
The invention belongs to technical field of sludge treatment, and relate to a kind for the treatment of process of mud.More specifically, the present invention relates to a kind of mud low pressure hot water solution treatment process and application thereof.
Background technology
Dewatered sludge is the Main By product produced in sewage treatment process, it is not only containing abundant moisture, organism and microorganism, and containing multiple objectionable impuritiess causing environmental pollution such as heavy metals, therefore the improper process of mud probably causes secondary environmental pollution.For avoiding the generation of the problems referred to above, developing some method for sludge treatment and device successively at present, to expect to reduce the harmful substance contents in mud, and by sludge treatment, secondary recovery utilization being carried out to it.Wherein, carrying out thermal hydrolysis process to mud is a kind of effective sludge treatment means.Existing sludge hot hydrolysis treatment all adopts high-pressure saturated steam to heat mud, and usually under higher than the hot conditions of 190 DEG C, is incubated hydrolysis reaction for a long time.Owing to being high pressure high thermal environment for a long time in reactor in treating processes, this treatment process requires the high-tension apparatus that use cost is higher, and energy consumption is high.On the other hand, heating mud, isothermal holding and high-tension apparatus pressure release all consume the long period, cause the length consuming time of whole sludge hot hydrolysis treatment, efficiency lower, and cause the running cost of whole treating processes higher.
Summary of the invention
The technical problem to be solved in the present invention is, energy consumption for sludge hot hydrolysis process for treating of the prior art is large, equipment requirements is strict and processing efficiency is low and cause running cost and the high defect of cost of investment, provides that a kind of energy consumption is little, processing efficiency is high and adopts the low-voltage equipment and attainable mud low pressure hot water solution treatment process that cost is low.
The technical problem to be solved in the present invention is achieved by the following technical programs: provide a kind of mud low pressure hot water solution treatment process, described method comprises:
S1: be that the mud of 70-97% injects in reactor by water ratio;
S2: the saturation steam injecting 1.0-1.59MPa in reactor, when the temperature of mud reaches 150 ~ 180 DEG C, stops injecting saturation steam and mud after obtaining thermal hydrolysis after keeping 0 ~ 30 minute.
Under the effect of heating power and pressure, in mud, the water holding of the solid matter such as organic polymer structure, colloid is destructurized, makes mud by the solid state transformed mud extremely strong for mobility of initial thickness.In addition, high-temperature hot hydrolysis treatment thoroughly can kill bacterium in mud and pathogenic agent, realizes the innoxious of mud.After thermal hydrolysis process, the water holding of mud is destructurized, and the Bound moisture in mud is released, and dewatering is greatly improved, for follow-up processed creates favorable conditions; Simultaneously, microorganism contained by mud is disintegrated, the organic matter of microorganism cells fully discharges an one-step hydrolysis of going forward side by side, and in mud, the dissolving of solid organic matters and hydrolysis make the anaerobic digestion performance of mud be greatly improved, for follow-up Anaerobic Digestion creates favorable conditions.
In above-mentioned mud low pressure hot water solution treatment process, the water ratio injecting mud in described step S1 in reactor is 70 ~ 89%.
In above-mentioned mud low pressure hot water solution treatment process, the water ratio injecting mud in described step S1 in reactor is 80 ~ 85%.
In above-mentioned mud low pressure hot water solution treatment process, in described step S2, in reactor, inject the saturation steam of 1.2 ~ 1.4Mpa.
In above-mentioned mud low pressure hot water solution treatment process, in described step S2, when the temperature of described mud reaches 155 ~ 175 DEG C, stop injecting saturation steam and keeping 5 ~ 25 minutes.
In above-mentioned mud low pressure hot water solution treatment process, in described step S2, when the temperature of described mud reaches 160 ~ 170 DEG C, stop injecting saturation steam and keeping 10 ~ 20 minutes.
In above-mentioned mud low pressure hot water solution treatment process, in described step S2, the temperature of described mud is the temperature of cold zone in described reactor.
In above-mentioned mud low pressure hot water solution treatment process, whipping appts is equipped with in described reactor inside, and described method starts described whipping appts after being also included in and injecting described mud and stirs mud.Stirring operation can promote fully contacting of mud and saturation steam, such that hot mass transfer in treating processes is faster, the thermal hydrolysis reaction of mud is more complete.Illustrate in addition, although all start whipping appts after injection mud herein and in subsequent embodiment, the use of whipping appts controls to be not limited to this mode.In other words, also can inject the process of mud or starting whipping appts after start to inject saturation steam.
In above-mentioned mud low pressure hot water solution treatment process, described method also comprises steam discharge pressure release and discharges described mud.
According to a further aspect in the invention, the application of a kind of above-mentioned mud low pressure hot water solution treatment process in process organic solid castoff is provided.The organic solid castoff of this type includes but not limited to changing food waste, animal excrement and/or food-processing factory waste residue etc.
Implement the present invention and can obtain following beneficial effect: thermal hydrolysis treatment process of the present invention is applicable to the mud of multiple water ratio, and without the need to carrying out any pre-treatment to mud before thermal hydrolysis reaction; Because the present invention adopts the saturation steam of below 1.6MPa to heat mud, the thermal hydrolysis reaction unit of low pressure configurations therefore can be adopted as reactor, effectively reduce equipment investment cost, corresponding maintenance cost and operator's cost also decline; Thermal hydrolysis treatment temp is lower, thus significantly can reduce the time be heated to by mud required for certain treatment temp, and then reduces energy consumption and running cost; Meanwhile, stop the also comparatively prior art shortening of the hold-time after injecting saturation steam, therefore, overall treatment time shortens greatly, and processing efficiency improves greatly, and facility investment significantly reduces, and corresponding maintenance cost also declines.
Accompanying drawing explanation
Fig. 1 is the schema according to mud low pressure hot water solution treatment process of the present invention.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with the drawings and specific embodiments, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
As shown in Figure 1, the invention provides a kind of mud low pressure hot water solution treatment process, the method adopts the saturation steam of 1.0-1.59MPa to carry out thermal hydrolysis process to the mud that water ratio is 70-97%, after mud temperature reaches 150-180 DEG C, the mud stopping keeping can making for 0-30 minute initial thick mud to be converted into when injecting saturation steam mobility is strong, be convenient to processed.
Above-mentioned lignin-sludge for the treatment of carries out in the process heated, and the present invention is contacted by mud and saturation steam (can be described as heating source) direct and heat exchange between mud realizes heating.It is understood to one skilled in the art that the reactor being used as sludge hot hydrolysis treatment at present mainly injects saturation steam from its top, minority reactor injects saturation steam from its top and bottom simultaneously.Because thermal hydrolysis mud before treatment is that thick, heat exchanging process is slow, and in reactor not etc., in heat-processed, in reactor, the mud temperature of different positions is not identical in the position of the mud distance heating source of different zones.
When using thermal hydrolysis treatment process provided by the present invention, first longitudinally getting a little at inside reactor, reactor is divided into upper, middle, and lower part by longitudinally third-class, is namely top near 1/3 of top, 1/3 of close bottom is bottom, and middle 1/3 is middle part.When saturation steam injects from top, bottom is cold zone; When injecting saturation steam from upper and lower simultaneously, middle part is cold zone.In other words, expression used herein " cold zone " means the comparatively far away and therefore region at the mud place that temperature is relatively low in heat-processed of in reactor distance heating source.
In a preferred embodiment of the invention, measure the temperature of mud in cold zone, and with this temperature value for standard judges whether to need to continue to inject saturation steam.The advantage measuring mud temperature in cold zone is: can guarantee that all pending mud of reactor all reaches the required temperature of carrying out net heat hydrolysis treatment, contribute to the abundant hydrolysis of mud in follow-up keep-process; Shorten the treatment time simultaneously, reduce energy consumption and raise the efficiency.
The present invention preferably uses the reactor of prone configuration and low pressure configurations.The equipment cost of the reactor that the present invention is used is low, and with the reactor of the type with the use of other devices (such as boiler, feed valve, discharge valve and corresponding pipeline etc.) all can adopt low-pressure type device.On the other hand, compare the reactor adopting vertical structure, the reactor heating surface area of prone configuration is larger, conduct heat more even, when using the saturation steam of same equipressure hot mass transfer speed faster and evenly, the time thus making whole pending mud be heated to needed for certain treatment temp can shorten dramatically.Following specific embodiment also all launches to describe in detail in conjunction with horizontal reacting still (in an embodiment referred to as reactor).But the present invention is not limited to the reaction unit using this structure, the distortion of the reactor of other structures of any employing and equivalent replacement are all within protection scope of the present invention.
Mud low pressure hot water solution treatment process of the present invention is further described below with reference to specific embodiment.
Embodiment 1:
Be the mud injection reactor of 90-97% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; From reactor top to the saturation steam injecting 1.1-1.2MPa in it, the mud in reactor is heated; The real time temperature of detection reaction still bottom mud, when mud temperature reaches 180 DEG C, stops injecting saturation steam and keeping 25-30 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 90-97%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 55-60%.
Embodiment 2:
Be the mud injection reactor of 85-89% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; Simultaneously from reactor upper and lower to the saturation steam injecting 1.2-1.3MPa in it, the mud in reactor is heated; The real time temperature of mud in the middle part of detection reaction still, when mud temperature reaches 175 DEG C, stops injecting saturation steam and keeping 20-25 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 85-89%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 45-55%.
Embodiment 3:
Be the mud injection reactor of 80-84% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; From reactor top to the saturation steam injecting 1.3-1.4MPa in it, the mud in reactor is heated; The real time temperature of detection reaction still bottom mud, when mud temperature reaches 170 DEG C, stops injecting saturation steam and keeping 15-20 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 80-84%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 35-45%.
Embodiment 4:
Be the mud injection reactor of 75-80% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; From reactor top to the saturation steam injecting 1.4-1.5MPa in it, the mud in reactor is heated; The real time temperature of detection reaction still bottom mud, when mud temperature reaches 165 DEG C, stops injecting saturation steam and keeping 10-15 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 75-80%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 40-45%.
Embodiment 5:
Be the mud injection reactor of 70-75% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; Simultaneously from reactor upper and lower to the saturation steam injecting 1.5-1.59MPa in it, the mud in reactor is heated; The real time temperature of mud in the middle part of detection reaction still, when mud temperature reaches 160 DEG C, stops injecting saturation steam and keeping 15-20 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 70-75%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 50-55%.
Embodiment 6:
Be the mud injection reactor of 80-85% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; From reactor top to the saturation steam injecting 1.15-1.25MPa in it, the mud in reactor is heated; The real time temperature of detection reaction still bottom mud, when mud temperature reaches 155 DEG C, stops injecting saturation steam and keeping 10-15 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 80-85%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 40-50%.
Embodiment 7:
Be the mud injection reactor of 80-85% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; Simultaneously from reactor upper and lower to the saturation steam injecting 1.35-1.45MPa in it, the mud in reactor is heated; The real time temperature of mud in the middle part of detection reaction still, when mud temperature reaches 150 DEG C, stops injecting saturation steam and keeping 10-20 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 80-85%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 45-50%.
Embodiment 8:
Be the mud injection reactor of 80-85% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the mud injected in it; Simultaneously from reactor upper and lower to the saturation steam injecting 1.45-1.59MPa in it, the mud in reactor is heated; The real time temperature of mud in the middle part of detection reaction still, when mud temperature reaches 180C, stops injecting saturation steam and keeping 0-5 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the mud that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the mud of 80-85%.
After the mud cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dehydrated sludge cake of 45-50%.
From above embodiment 1-8, mud low pressure hot water solution treatment process of the present invention is applicable to the mud of multiple water ratio, has wide range of applications.Adopt the saturation steam of 1.1-1.59MPa under lower pressure, carry out thermal hydrolysis process and not only reduce requirement (adopting the reactor of low pressure configurations) to equipment, and effectively save the time reaching required condition of high voltage and processed rear pressure release, overall treatment time is shortened dramatically, overall thermal hydrolysis processing efficiency improves, more mud can be processed under equal energy consumption and time conditions.Thick mud can be made to be converted into the extremely strong mud of mobility by method of the present invention; Be convenient to follow-uply to be further processed mud in conjunction with the treatment facility such as mechanical dewatering equipment or anaerobic digestion facility and to fully utilize.
Mud low pressure hot water solution treatment process of the present invention can be applicable to process organic solid castoff, the organic solid castoff of preferably treatment high-moisture percentage, and more preferably processing water ratio is the organic solid castoff of 70-97%.The organic solid castoff of this type includes but not limited to changing food waste, animal excrement and/or food-processing factory waste residue etc.To be described in detail the application of this treatment process by concrete example below, but it should be understood that following concrete example is only for explaining the present invention, and any restriction is not formed to scope of the present invention.
Example 1:
Be the changing food waste injection reactor of 90-97% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the changing food waste injected in it; From reactor top to the saturation steam injecting 1.3-1.4MPa in it, the changing food waste in reactor is heated; The real time temperature of detection reaction still bottom changing food waste, when the temperature of changing food waste reaches 170 DEG C, stops injecting saturation steam and keeping 15-20 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the pulpous state changing food waste that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the changing food waste of 90-97%.
After the soup compound cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dewatered product of 50-55%.
Example 2:
Be the animal excrement injection reactor of 75-84% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the animal excrement of injecting in it; From reactor top to the saturation steam injecting 1.4-1.5MPa in it, the animal excrement in reactor are heated; The real time temperature of detection reaction still bottom animal excrement, when the temperature of animal excrement reaches 165 DEG C, stops injecting saturation steam and keeping 10-15 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the pulpous state animal excrement that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the animal excrement of 75-84%.
After the soup compound cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dewatered product of 40-45%.
Example 3:
Be the food-processing factory waste residue injection reactor of 70-75% by water ratio, off-response still opening for feed, and start the whipping appts in reactor, at the uniform velocity stir the food-processing factory waste residue injected in it; Simultaneously from reactor upper and lower to the saturation steam injecting 1.5-1.59MPa in it, the food-processing factory waste residue in reactor is heated; The real time temperature of food-processing factory waste residue in the middle part of detection reaction still, when the temperature of food-processing factory waste residue reaches 160 DEG C, stops injecting saturation steam and keeping 15-20 minute; Open pressure release valve subsequently and start exhaust pressure relief, when the Pressure Drop in reactor opens blow-off valve to during below 0.05MPa, discharge the pasty food source mill waste residue that thermal hydrolysis process obtains; Now completing water ratio is the low pressure hot water solution process of the food-processing factory waste residue of 70-75%.
After the soup compound cooling of discharging, processed is carried out to it, obtain removing liquid and water ratio is the dewatered product of 50-55%.
The foregoing is only the preferred embodiments of the present invention, not in order to limit the present invention, all do in the spirit and principles in the present invention any amendment, equivalent to replace or improvement etc., all should be included in protection scope of the present invention.
Claims (4)
1. a mud low pressure hot water solution treatment process, is characterized in that, be made up of following steps:
S1: be that the mud of 70-89% injects in reactor by water ratio;
S2: the saturation steam injecting 1.0-1.59MPa in reactor, when the temperature of mud reaches 160 ~ 170 DEG C, stops injecting saturation steam and mud after obtaining thermal hydrolysis after keeping 10 ~ 20 minutes: steam discharge pressure release also discharges described mud;
S3: after the mud cooling of discharging, processed is carried out to it, obtain removing liquid and dehydrated sludge cake;
Wherein, after the described mud of injection, start whipping appts to stir mud, injecting sludge process or start whipping appts after starting to inject saturation steam.
2. mud low pressure hot water solution treatment process according to claim 1, is characterized in that, the water ratio injecting mud in described step S1 in reactor is 80 ~ 85%.
3. mud low pressure hot water solution treatment process according to claim 1, is characterized in that, in described step S2, injects the saturation steam of 1.2 ~ 1.4Mpa in reactor.
4. in claim 1-3, the mud low pressure hot water solution treatment process of arbitrary claim is processing the application in organic solid castoff.
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Citations (3)
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CN101880118A (en) * | 2010-02-03 | 2010-11-10 | 王鹤立 | Energy reclaiming sludge reduction method |
CN101987772A (en) * | 2010-11-23 | 2011-03-23 | 北京机电院高技术股份有限公司 | Method for improving sludge dewatering performance through thermal conditioning of sludge |
CN102417285A (en) * | 2011-10-20 | 2012-04-18 | 同济大学 | Continuous pyrohydrolysis device and method for high-solid-content biological sludge |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN101880118A (en) * | 2010-02-03 | 2010-11-10 | 王鹤立 | Energy reclaiming sludge reduction method |
CN101987772A (en) * | 2010-11-23 | 2011-03-23 | 北京机电院高技术股份有限公司 | Method for improving sludge dewatering performance through thermal conditioning of sludge |
CN102417285A (en) * | 2011-10-20 | 2012-04-18 | 同济大学 | Continuous pyrohydrolysis device and method for high-solid-content biological sludge |
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