CN103074226B - Composite flora for biological preparation of textile fibers, and applications thereof - Google Patents
Composite flora for biological preparation of textile fibers, and applications thereof Download PDFInfo
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- CN103074226B CN103074226B CN201210344042.8A CN201210344042A CN103074226B CN 103074226 B CN103074226 B CN 103074226B CN 201210344042 A CN201210344042 A CN 201210344042A CN 103074226 B CN103074226 B CN 103074226B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
Abstract
The present invention relates to a composite flora for biological preparation of textile fibers, and applications thereof. The composite flora comprises bacillus sp. with a preservation number of CGMCC No.5971, rheinheimera tangshanensis with a preservation number of CGMCC No.5972, and Wickerhamomyces anomalus with a preservation number of CGMCC No.5975. The method comprises the following steps: preparing a bacterial liquid; treating raw materials; and preparing fibers, wherein fiber preparation comprises biodegradation, steam sterilization, fiber obtaining, drying, and combing. According to the present invention, the method does not pollute the environment, a waste liquid is directly converted into an organic fertilizer so as to achieve zero emission and zero pollution, the biological treatment process provides a protection effect for fibers, advantages of low production cost and high economic benefits are provided compared with the traditional chemical method, and characteristics of energy source saving and environmental protection are provided.
Description
Technical field
The present invention relates to a kind of textile fiber, relate in particular to a kind of composite flora and application thereof of preparing textile fibres for biology.
Background technology
In recent years, day by day exhausted along with petrochemical industry resource, bast-fibre enjoys doting on of human consumer because having the good characteristic such as ecology, environmental protection, and its demand is at increase year after year, the annual speedup 8% of global natural fiber.The maximum feature of bast-fibre raw material is that fibre content is high, and elongated being conducive to of fiber interweaves, and intensity is good; Fiber cell is little, cell wall is thick, wall chamber ratio is large; Because bast-fibre lumen is thin, fiber trivial matter opaqueness is high.But its shortcoming is fiber is not easy wire-dividing broom purification, make the fabric air-permeability degree made low.
In prior art, from numb raw material, prepare fiber, how by chemical process, the waste liquor contamination sublimity that chemical process produces in producing, damage to land, polluted air, and also it is high to consume energy, and power consumption and water consumption are large.Do not meet national energy-saving and reduce discharging policy.Material can not reach Efficient Cycle recycling.Chemicals cannot separate from waste liquid, and organism and chemicals mix, and organism also cannot be reused, and causes a large amount of losses.
Therefore, be necessary to develop biological fibre technology processed, fundamentally solve an above-mentioned pollution difficult problem, energy-saving and emission-reduction, water-saving, reduces production costs and improves the rate of utilization of material.
Summary of the invention
The object of the invention is the above-mentioned defect of the chemical legal system fiber that overcomes prior art, a kind of new fiber biological bacteria of preparing is provided.Contriver, by long screening operation, has obtained the biological bacteria that can realize foregoing invention object that is suitable for preparing fiber.
Particularly, the invention provides a kind of composite flora, its comprise the silent Salmonella (Rheinheimera tangshanensis) of Tangshan Lay mattress that the genus bacillus that preserving number is CGMCC No.5971 (Bacillus sp.), preserving number are CGMCC No.5972, this Wickerhamomyces anomalus bacterium of Wickerhamomyces anomalus(that preserving number is CGMCC No.5975 in malt juice liquid medium 25 ℃ cultivate three days, cell is spherical, avette, sausage shape, size is (4.8-14.4) × (3.6-7.2) μ m, has precipitation to form.25 ℃, wort agar inclined-plane cultivation one month, bacterium colony cheese shape, oyster white, surface smoothing, not reflective, edge root shape.Corn Meal Agar Dalmau is dull and stereotyped to be cultivated, and produces pseudohypha).
Described composite flora can be used in prepares textile fiber.
The present invention also provides a kind of method of preparing textile fiber, and it mainly comprises step:
1) configuration of bacterium liquid: above-mentioned composite flora is configured to the composite bacteria aqueous solution according to following mass ratio, is bacterium liquid:
Genus bacillus: the Tangshan Lay mattress Salmonella of writing from memory: Wickerhamomyces anomalus is 2-3:1-2:2-3;
2) raw material processing: crudefiber crop raw material is cut into chunks, and raw material is put into fermentation vat swollen;
3) preparation of fiber, it comprises step:
Biological degradation: by the raw material soaking after discongesting in the bacterium liquid configuring;
Wet sterilization: by the raw material after above-mentioned biological degradation from bacterium liquid, pull out, draining, pass into water vapor sterilizing;
Obtaining of fiber: the raw material after sterilizing is carried out to one section of corase grind, become fibrous bundle; Above-mentioned one section of corase grind is carried out to two sections of fine grindings, make fibrous bundle disperse into single fiber; Fibrous bundle in screening, the slurries of filtration after one section of corase grind and two sections of fine grindings, defibrination makes it make single fiber again;
Dry, combing: the above-mentioned fiber making is soaked in warm water, and then oven dry, combing, for the preparation of textile fiber.
The density of the bacterium liquid wherein, forming in step 1) be 6,000 ten thousand/more than ml bacterium.
Wherein, step 2) in, described crudefiber crop raw material is flax, ramie, yellow bluish dogbane or sisal hemp.The described swollen time is 10-12h.
Wherein, the biological degradation temperature described in step 3) remains on 35-40 ℃, time 32-36 hour.The mass ratio of the raw material after discongesting and bacterium liquid is 1:7-9.Described steam sterilizing is water at atmospheric pressure steam sterilizing 10-30 minute.
Further, step 2) in soak soak solution after raw material through flocculation, precipitation, supernatant liquor recycling, the fermentation of throw out input methane-generating pit produces biogas.
The advantage that biological method provided by the invention is prepared fiber is: 1) free from environmental pollution: waste liquid directly changes into organic fertilizer, reaches zero release, and zero pollutes.2) biological method can play a protective role to fiber, and compared with traditional chemical process, present method can all reclaim full fiber and half fiber, has therefore improved yield.3) biological method is degraded under normal pressure, energy-conservation, reduction of discharging, low-carbon (LC).4) production cost is low, and economic benefit is high.
Byproduct of the present invention is transported to settling tank flocculation, precipitation, and supernatant liquor returns to second stage employ, remakes presoak and uses.In throw out, contain the nutrient for plants such as abundant gas chromatography and N, P, K, throw out mixes with old bacterium liquid (the raw material thickness bacterium liquid of repeatedly degrading, also contains N, P, K, Fe and trace element) again, acidifying, then together enter in marsh gas fermentation pool, produce biogas.By the Boiler Ash mixing granulation of natural pond slag, natural pond liquid and pulverizing, granulation fertilizer, finally dispatches from the factory, and realizes zero release.
The present invention is by the biological bacteria that provides above-mentioned contriver to obtain through long creation work, the further perfect cellulosic technology of existing preparation, reduce the reaction times, improved the purity and the yield that make fiber, this technology can be applied on a large scale in actual production.Applying biological bacterium of the present invention at short notice degrading plant obtains fiber, and byproduct twice transformation becomes biogas, and biogas coal supply, gas boiler for dual purpose combustion heating are saved coal consumption.Finally, natural pond slag is made organic fertilizer, has formed the economic circulation new model of " material organic transformation ", reaches no waste discharge, namely zero release.Fundamentally solve a pollution difficult problem for chemical preparation fiber of the prior art.Energy-saving and emission-reduction, water-saving, has reduced production cost, has improved the rate of utilization of material.
For above and other objects of the present invention, feature and advantage can be become apparent, preferred embodiment cited below particularly, and coordinate accompanying drawing, be described in detail below.
Accompanying drawing explanation
Fig. 1 is the schema of preparing textile fiber according to one embodiment of the invention.
Embodiment
The configuration of embodiment 1 bacterium liquid
The biological bacteria adopting in the present invention on April 6th, 2012 at China Committee for Culture Collection of Microorganisms's common micro-organisms center (CGMCC, No. 3, Yard 1, BeiChen xi Road, Chaoyang District, Beijing City) preservation, it comprises the genus bacillus that preserving number is CGMCC No.5971 (Bacillus sp.), preserving number is that the silent Salmonella (Rheinheimera tangshanensis) of Tangshan Lay mattress, the preserving number of CGMCC No.5972 is the Wickerhamomyces anomalus of CGMCC No.5975.
Above-mentioned composite flora is configured to the composite bacteria aqueous solution according to following mass ratio, is bacterium liquid:
Genus bacillus: the Tangshan Lay mattress Salmonella of writing from memory: Wickerhamomyces anomalus is 2-3:1-2:2-3; The density of bacterium liquid forming be 6,000 ten thousand/more than ml bacterium, for subsequent use.
Embodiment 2 prepares fiber from flax
Take flax as raw material, illustrate the preparation method of fiber.Composite flora is configured according to following mass ratio: genus bacillus: the Tangshan Lay mattress Salmonella of writing from memory: Wickerhamomyces anomalus is 3:1:3.
Specifically please refer to Fig. 1, the preparation method's of fiber flow process is divided into three phases: preparatory stage, fiber workshop section and byproduct workshop section.
(1) preparatory stage: 1,4
Flax that harvesting is returned immerse soak in storehouse or fermentation vat wash, cold soaking, first the foreign material such as raw material appearance earth are washed away, soak simultaneously, water temperature is natural temperature, the time soaking into, swollen is as the criterion, 10-12 hour.After liquid muddiness after repeatedly soaking, after flocculating, precipitating, supernatant liquor can also reuse.The fermentation of throw out input methane-generating pit, produces biogas.
(2) fiber workshop section: 6-12
6) biological degradation: by the raw material input biological bacteria degraded storehouse after discongesting or tank, be immersed in bacterium liquid prepared by embodiment 1, the mass ratio of the raw material after discongesting and bacterium liquid is 1:8, and temperature remains on 35-40 ℃, time 32-36 hour.Under the condition of biological bacteria, there is DeR, bring into play its single-minded effect.
7) wet sterilization: after raw materials pretreatment completes, by raw material from bacterium liquid, pull out, draining, be input in steam storehouse, pass into the sterilizing in 10-30 minute of water at atmospheric pressure steam.Paste roller mill inputted by raw material by lower end.
8) obtaining of fiber: the raw material after sterilizing is carried out to one section of corase grind, become fibrous bundle.
9) above-mentioned one section of corase grind is carried out to two sections of fine grindings, make fibrous bundle disperse into single fiber.
10) multiple sieve: the fibrous bundle in screening, the slurries of filtration after one section of corase grind and two sections of fine grindings, defibrination makes it make single fiber again.
11) dry, combing: the above-mentioned fiber making is soaked in warm water, then dry, combing, drawing-off, further stretches fiber parallel.
12) prepare textile fiber: adopt further Technology to prepare textile fiber the fiber of above-mentioned acquisition.
(3) byproduct stage: A-C
In A, 3, isolated raw material residuum contains abundant nutritive ingredient, and fermentation changes into ox, sheep feed.
After liquid muddiness through repeatedly soaking, washing in B, 4, through flocculation, precipitation, supernatant liquor recycling, the fermentation of throw out input methane-generating pit produces biogas, passes into coal gas boiler for dual purpose and does fuel, can play effect of energy.
C, biological organic fertilizer: natural pond slag, natural pond liquid after methane-generating pit fermentation are abundant biological organic fertilizers, liquid topdresses as farm crop and flower nutrient solution uses, and solid granulation is made base manure and is used, and is all green fertilizers.
The physical performance index measurement result of the fiber obtaining please refer to table 1.
Embodiment 3 prepares Mierocrystalline cellulose from ramie
Concrete preparation technology is with embodiment 2.Difference is, composite flora is configured according to following mass ratio: genus bacillus: the Tangshan Lay mattress Salmonella of writing from memory: Wickerhamomyces anomalus is 3:1:2; When biological degradation, the mass ratio of the raw material after discongesting and bacterium liquid is 1:7.
The physical performance index measurement result of the fiber obtaining please refer to table 1.
Embodiment 4 prepares Mierocrystalline cellulose from yellow bluish dogbane
Concrete preparation technology is with embodiment 2.Difference is, composite flora is configured according to following mass ratio: genus bacillus: the Tangshan Lay mattress Salmonella of writing from memory: Wickerhamomyces anomalus is 3:2:2; When biological degradation, the mass ratio of the raw material after discongesting and bacterium liquid is 1:8.5.
The physical performance index measurement result of the fiber obtaining please refer to table 1.
Embodiment 5 prepares Mierocrystalline cellulose from sisal hemp
Concrete preparation technology is with embodiment 2.Difference is, composite flora is configured according to following mass ratio: genus bacillus: the Tangshan Lay mattress Salmonella of writing from memory: Wickerhamomyces anomalus is 2:1:3; When biological degradation, the mass ratio of the raw material after discongesting and bacterium liquid is 1:9.
The physical performance index measurement result of the fiber obtaining please refer to table 1.
Table 1
Although the present invention discloses as above with preferred embodiment; so it is not in order to limit the present invention; any person of ordinary skill in the field; without departing from the spirit and scope of the present invention; when doing a little change and improvement, therefore protection scope of the present invention is when being as the criterion depending on the claim person of defining.
Claims (4)
1. a method of preparing textile fibres, is characterized in that, comprises step:
1) configuration of bacterium liquid: be that the silent Salmonella (Rheinheimera tangshanensis) of the genus bacillus (Bacillus sp.) of CGMCC No.5971, Tangshan Lay mattress that preserving number is CGMCC No.5972, preserving number are that the abnormal Brunswick Durham yeast (Wickerhamomyces anomalus) of CGMCC No.5975 is configured to the composite bacteria aqueous solution according to following mass ratio by preserving number, be bacterium liquid:
Genus bacillus: the Tangshan Lay mattress Salmonella of writing from memory: abnormal Brunswick Durham yeast is 2-3:1-2:2-3, the density of bacterium liquid be 6,000 ten thousand/more than ml bacterium;
2) raw material processing: crudefiber crop raw material is cut into chunks, and raw material is put into fermentation vat swollen, crudefiber crop raw material is flax, ramie, yellow bluish dogbane or sisal hemp;
3) preparation of fiber, it comprises step:
Biological degradation: in the bacterium liquid configuring, the mass ratio of the raw material after discongesting and bacterium liquid is 1:7-9 by the raw material soaking after discongesting, and degradation temperature is 35-40 ℃, and degradation time is 32-36 hour;
Wet sterilization: by the raw material after above-mentioned biological degradation from bacterium liquid, pull out, draining, pass into water vapor sterilizing;
Obtaining of fiber: the raw material after sterilizing is carried out to one section of corase grind, become fibrous bundle; Above-mentioned one section of corase grind is carried out to two sections of fine grindings, make fibrous bundle disperse into single fiber; Fibrous bundle in screening, the slurries of filtration after one section of corase grind and two sections of fine grindings, defibrination makes it make single fiber again;
Dry, combing: the above-mentioned fiber making is soaked in warm water, and then oven dry, combing, for the preparation of textile fibres.
2. method according to claim 1, is characterized in that step 2) the described swollen time is 10-12h.
3. method according to claim 1, is characterized in that, the steam sterilizing described in step 3) is water at atmospheric pressure steam sterilizing 10-30 minute.
4. method according to claim 1, is characterized in that step 2) in soak soak solution after raw material through flocculation, precipitation, supernatant liquor recycling, the fermentation of throw out input methane-generating pit produces biogas.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210344042.8A CN103074226B (en) | 2012-09-17 | 2012-09-17 | Composite flora for biological preparation of textile fibers, and applications thereof |
| PCT/CN2013/001091 WO2014040390A1 (en) | 2012-09-17 | 2013-09-16 | Complex microbial flora and application thereof |
| CA2885486A CA2885486A1 (en) | 2012-09-17 | 2013-09-16 | Complex microbial flora and application thereof |
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| CN201210344042.8A CN103074226B (en) | 2012-09-17 | 2012-09-17 | Composite flora for biological preparation of textile fibers, and applications thereof |
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| CA2885486A1 (en) * | 2012-09-17 | 2014-03-20 | Beijing Tian'an Bioscience & Technology Co., Ltd. | Complex microbial flora and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101838613A (en) * | 2009-09-30 | 2010-09-22 | 河南省恒隆态生物工程股份有限公司 | Agricultural straw fast-degradation decomposition agent strain composition |
| CN102174399A (en) * | 2010-12-31 | 2011-09-07 | 广西赛尔纸业有限公司 | Method for preparing herbal biological fiber and biological paper pulp |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101838613A (en) * | 2009-09-30 | 2010-09-22 | 河南省恒隆态生物工程股份有限公司 | Agricultural straw fast-degradation decomposition agent strain composition |
| CN102174399A (en) * | 2010-12-31 | 2011-09-07 | 广西赛尔纸业有限公司 | Method for preparing herbal biological fiber and biological paper pulp |
Non-Patent Citations (2)
| Title |
|---|
| Rheinheimera tangshanensis sp. Nov., a rice root associated bacterium;Xiaoxia Zhang et al.;《International journal of systematic and evolutionary microbiology》;20081031;第58卷(第10期);2420-2424 * |
| XiaoxiaZhangetal..Rheinheimeratangshanensissp.Nov. a rice root associated bacterium.《International journal of systematic and evolutionary microbiology》.2008 |
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