CN103073696A - Preparation method of light-resistant waterborne polyurethane - Google Patents
Preparation method of light-resistant waterborne polyurethane Download PDFInfo
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- CN103073696A CN103073696A CN2013100343312A CN201310034331A CN103073696A CN 103073696 A CN103073696 A CN 103073696A CN 2013100343312 A CN2013100343312 A CN 2013100343312A CN 201310034331 A CN201310034331 A CN 201310034331A CN 103073696 A CN103073696 A CN 103073696A
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- CN
- China
- Prior art keywords
- photostabilization
- preparation
- aqueous polyurethane
- polyurethane
- stirring reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229920002635 polyurethane Polymers 0.000 title claims abstract description 44
- 239000004814 polyurethane Substances 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 46
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims abstract description 21
- 238000006243 chemical reaction Methods 0.000 claims abstract description 21
- 238000004945 emulsification Methods 0.000 claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000007908 nanoemulsion Substances 0.000 claims abstract description 13
- 229920001730 Moisture cure polyurethane Polymers 0.000 claims abstract description 12
- 239000004970 Chain extender Substances 0.000 claims abstract description 9
- 239000003054 catalyst Substances 0.000 claims abstract description 9
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims abstract description 7
- 239000012975 dibutyltin dilaurate Substances 0.000 claims abstract description 7
- 230000000176 photostabilization Effects 0.000 claims description 24
- 230000035484 reaction time Effects 0.000 claims description 12
- BJZYYSAMLOBSDY-QMMMGPOBSA-N (2s)-2-butoxybutan-1-ol Chemical compound CCCCO[C@@H](CC)CO BJZYYSAMLOBSDY-QMMMGPOBSA-N 0.000 claims description 10
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 claims description 10
- ZQBAKBUEJOMQEX-UHFFFAOYSA-N phenyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OC1=CC=CC=C1 ZQBAKBUEJOMQEX-UHFFFAOYSA-N 0.000 claims description 10
- PTBDIHRZYDMNKB-UHFFFAOYSA-N 2,2-Bis(hydroxymethyl)propionic acid Chemical compound OCC(C)(CO)C(O)=O PTBDIHRZYDMNKB-UHFFFAOYSA-N 0.000 claims description 8
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 8
- 239000002086 nanomaterial Substances 0.000 claims description 7
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000006096 absorbing agent Substances 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 6
- 239000004255 Butylated hydroxyanisole Substances 0.000 claims description 5
- 239000004322 Butylated hydroxytoluene Substances 0.000 claims description 5
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims description 5
- 239000003963 antioxidant agent Substances 0.000 claims description 5
- 230000003078 antioxidant effect Effects 0.000 claims description 5
- 235000019282 butylated hydroxyanisole Nutrition 0.000 claims description 5
- CZBZUDVBLSSABA-UHFFFAOYSA-N butylated hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 claims description 5
- 229940043253 butylated hydroxyanisole Drugs 0.000 claims description 5
- 235000010354 butylated hydroxytoluene Nutrition 0.000 claims description 5
- 229940095259 butylated hydroxytoluene Drugs 0.000 claims description 5
- 239000003995 emulsifying agent Substances 0.000 claims description 5
- 229920005862 polyol Polymers 0.000 claims description 5
- 150000003077 polyols Chemical class 0.000 claims description 5
- 239000005057 Hexamethylene diisocyanate Substances 0.000 claims description 4
- 239000005058 Isophorone diisocyanate Substances 0.000 claims description 4
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims description 4
- HGRNRWNRNVPVMM-UHFFFAOYSA-N benzene-1,3-diol;benzoic acid Chemical compound OC1=CC=CC(O)=C1.OC(=O)C1=CC=CC=C1 HGRNRWNRNVPVMM-UHFFFAOYSA-N 0.000 claims description 4
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 4
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims description 4
- NIMLQBUJDJZYEJ-UHFFFAOYSA-N isophorone diisocyanate Chemical compound CC1(C)CC(N=C=O)CC(C)(CN=C=O)C1 NIMLQBUJDJZYEJ-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 239000005543 nano-size silicon particle Substances 0.000 claims description 4
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 claims description 4
- RDBMUARQWLPMNW-UHFFFAOYSA-N phosphanylmethanol Chemical compound OCP RDBMUARQWLPMNW-UHFFFAOYSA-N 0.000 claims description 4
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 4
- 239000002105 nanoparticle Substances 0.000 claims description 3
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 3
- 235000019982 sodium hexametaphosphate Nutrition 0.000 claims description 3
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 3
- ZXDDPOHVAMWLBH-UHFFFAOYSA-N 2,4-Dihydroxybenzophenone Chemical compound OC1=CC(O)=CC=C1C(=O)C1=CC=CC=C1 ZXDDPOHVAMWLBH-UHFFFAOYSA-N 0.000 claims description 2
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 2
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 2
- 238000013019 agitation Methods 0.000 claims description 2
- 125000000896 monocarboxylic acid group Chemical group 0.000 claims description 2
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 abstract 1
- 125000005442 diisocyanate group Chemical group 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 229920000909 polytetrahydrofuran Polymers 0.000 abstract 1
- 238000010008 shearing Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 description 5
- 238000009835 boiling Methods 0.000 description 4
- -1 Urethane aromatic isocyanate Chemical class 0.000 description 3
- 239000012948 isocyanate Substances 0.000 description 3
- 229920006264 polyurethane film Polymers 0.000 description 3
- 238000000576 coating method Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000001782 photodegradation Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000009281 ultraviolet germicidal irradiation Methods 0.000 description 1
- 239000002966 varnish Substances 0.000 description 1
- 238000004383 yellowing Methods 0.000 description 1
Landscapes
- Polyurethanes Or Polyureas (AREA)
Abstract
Description
Time/min | PODESENG ?513MS | D | F | G | H |
90 | 0.7 | 0.2 | 0.5 | 0.3 | 0.1 |
150 | 0.9 | 0.6 | 0.7 | 0.3 | 0.1 |
270 | 1.0 | 0.7 | 0.8 | 0.4 | 0.3 |
330 | 1.1 | 0.7 | 0.8 | 0.5 | 0.4 |
390 | 1.3 | 0.8 | 0.9 | 0.6 | 0.6 |
450 | 1.5 | 0.9 | 0.9 | 0.7 | 0.7 |
510 | 1.8 | 1.0 | 1.0 | 0.8 | 0.9 |
540 | 2.1 | 1.1 | 1.2 | 0.8 | 0.9 |
600 | 2.3 | 1.2 | 1.2 | 1.1 | 1.0 |
Classification | PODESENG 513MS | D | F | G | H |
Elongation at break/% | 187.06 | 237.67 | 262.52 | 271.80 | 253.54 |
Claims (9)
Priority Applications (1)
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CN201310034331.2A CN103073696B (en) | 2013-01-30 | 2013-01-30 | Preparation method of light-resistant waterborne polyurethane |
Applications Claiming Priority (1)
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CN201310034331.2A CN103073696B (en) | 2013-01-30 | 2013-01-30 | Preparation method of light-resistant waterborne polyurethane |
Publications (2)
Publication Number | Publication Date |
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CN103073696A true CN103073696A (en) | 2013-05-01 |
CN103073696B CN103073696B (en) | 2014-08-13 |
Family
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Family Applications (1)
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CN201310034331.2A Expired - Fee Related CN103073696B (en) | 2013-01-30 | 2013-01-30 | Preparation method of light-resistant waterborne polyurethane |
Country Status (1)
Country | Link |
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CN (1) | CN103073696B (en) |
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103436155A (en) * | 2013-09-09 | 2013-12-11 | 段宝荣 | Preparation method of light-resistant water-based polyurethane coating |
CN103936959A (en) * | 2014-05-14 | 2014-07-23 | 张家港康得新光电材料有限公司 | Preparation method of water-based self-extinction spray resin |
CN104073149A (en) * | 2014-07-21 | 2014-10-01 | 朱蕾 | Preparation method for lightproof and waterproof polyurethane coating |
CN104073145A (en) * | 2014-07-21 | 2014-10-01 | 段小宁 | Preparation method for lightproof and waterproof polyurethane coating |
CN104087149A (en) * | 2014-07-21 | 2014-10-08 | 段宝荣 | Method for preparing light-fast waterborne polyurethane coating material |
CN104194607A (en) * | 2014-08-15 | 2014-12-10 | 段小宁 | Preparation method of light-resistant and waterproof water-based flame retardant polyurethane coating and adhesive |
CN106221550A (en) * | 2016-08-30 | 2016-12-14 | 段宝荣 | The polyurethane coating preparation method of fire-retardant, light resistance and low VOC |
CN106221551A (en) * | 2016-08-30 | 2016-12-14 | 段宝荣 | Polyurethane coating preparation method with low VOC fire-retardant, waterproof |
CN106590394A (en) * | 2016-11-25 | 2017-04-26 | 清远市美佳乐环保新材股份有限公司 | Process of preparing waterborne polyurethane optical coating through continuous method |
CN107417881A (en) * | 2017-08-04 | 2017-12-01 | 合肥思敬齐化工材料有限责任公司 | A kind of preparation method of the aqueous polyurethane of ultraviolet radiation preventing |
CN108822713A (en) * | 2018-07-15 | 2018-11-16 | 段宝荣 | The preparation method of light-resistant waterborne polyurethane coating and adhesive |
CN109721704A (en) * | 2019-01-11 | 2019-05-07 | 北京理工大学 | A kind of light shield extinguishing waterborn polyurethane and preparation method thereof |
CN111303374A (en) * | 2020-04-02 | 2020-06-19 | 上海应用技术大学 | Brominated soybean oil modified pure water-based polyurethane nano-emulsion and preparation method thereof |
CN113999360A (en) * | 2021-12-02 | 2022-02-01 | 太原理工大学 | Method for preparing flame-retardant waterborne polyurethane from waste polyester textile fabrics |
CN114025959A (en) * | 2019-07-12 | 2022-02-08 | 陶氏环球技术有限责任公司 | Water-based composition |
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JP2002302524A (en) * | 2001-04-06 | 2002-10-18 | Arakawa Chem Ind Co Ltd | Method for producing polyurethane resin aqueous dispersion |
KR20030040821A (en) * | 2001-11-16 | 2003-05-23 | 신원상사주식회사 | Composition of water polyurethane and method for processing the same |
CN101845217A (en) * | 2010-05-11 | 2010-09-29 | 陕西科技大学 | Preparation method of water-based polyurethane/nano-silicon dioxide composite emulsion |
CN102344699A (en) * | 2011-07-05 | 2012-02-08 | 天津大学 | Nano-grade silica modified montmorillonite particle preparation method, and method for applying nano-grade silica modified montmorillonite particles in producing modified aqueous polyurethane resin with in-situ method |
CN102558488A (en) * | 2012-03-02 | 2012-07-11 | 上海嘉宝莉涂料有限公司 | Preparation method for nano white carbon black modified polyether type aqueous polyurethane for coating |
CN102604039A (en) * | 2012-03-20 | 2012-07-25 | 王全杰 | Preparation method of waterborne polyurethane material with resistance to yellowing |
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2013
- 2013-01-30 CN CN201310034331.2A patent/CN103073696B/en not_active Expired - Fee Related
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JP2002302524A (en) * | 2001-04-06 | 2002-10-18 | Arakawa Chem Ind Co Ltd | Method for producing polyurethane resin aqueous dispersion |
KR20030040821A (en) * | 2001-11-16 | 2003-05-23 | 신원상사주식회사 | Composition of water polyurethane and method for processing the same |
CN101845217A (en) * | 2010-05-11 | 2010-09-29 | 陕西科技大学 | Preparation method of water-based polyurethane/nano-silicon dioxide composite emulsion |
CN102344699A (en) * | 2011-07-05 | 2012-02-08 | 天津大学 | Nano-grade silica modified montmorillonite particle preparation method, and method for applying nano-grade silica modified montmorillonite particles in producing modified aqueous polyurethane resin with in-situ method |
CN102558488A (en) * | 2012-03-02 | 2012-07-11 | 上海嘉宝莉涂料有限公司 | Preparation method for nano white carbon black modified polyether type aqueous polyurethane for coating |
CN102604039A (en) * | 2012-03-20 | 2012-07-25 | 王全杰 | Preparation method of waterborne polyurethane material with resistance to yellowing |
Non-Patent Citations (1)
Title |
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刘益军: "《聚氨酯原料及助剂手册》", 30 April 2005, 化学工业出版社 * |
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103436155A (en) * | 2013-09-09 | 2013-12-11 | 段宝荣 | Preparation method of light-resistant water-based polyurethane coating |
CN103436155B (en) * | 2013-09-09 | 2015-12-23 | 段宝荣 | A kind of preparation method of light-resistant waterborne polyurethane coating |
CN103936959A (en) * | 2014-05-14 | 2014-07-23 | 张家港康得新光电材料有限公司 | Preparation method of water-based self-extinction spray resin |
CN104073149A (en) * | 2014-07-21 | 2014-10-01 | 朱蕾 | Preparation method for lightproof and waterproof polyurethane coating |
CN104073145A (en) * | 2014-07-21 | 2014-10-01 | 段小宁 | Preparation method for lightproof and waterproof polyurethane coating |
CN104087149A (en) * | 2014-07-21 | 2014-10-08 | 段宝荣 | Method for preparing light-fast waterborne polyurethane coating material |
CN104073145B (en) * | 2014-07-21 | 2016-08-24 | 常州市天安特种涂料有限公司 | A kind of preparation method of light-resistant waterborne polyurethane coating |
CN104194607A (en) * | 2014-08-15 | 2014-12-10 | 段小宁 | Preparation method of light-resistant and waterproof water-based flame retardant polyurethane coating and adhesive |
CN106221550A (en) * | 2016-08-30 | 2016-12-14 | 段宝荣 | The polyurethane coating preparation method of fire-retardant, light resistance and low VOC |
CN106221551A (en) * | 2016-08-30 | 2016-12-14 | 段宝荣 | Polyurethane coating preparation method with low VOC fire-retardant, waterproof |
CN106221551B (en) * | 2016-08-30 | 2018-03-13 | 河北晨阳工贸集团有限公司 | Fire-retardant, waterproof and low VOC polyurethane coating preparation method |
CN106590394A (en) * | 2016-11-25 | 2017-04-26 | 清远市美佳乐环保新材股份有限公司 | Process of preparing waterborne polyurethane optical coating through continuous method |
CN107417881A (en) * | 2017-08-04 | 2017-12-01 | 合肥思敬齐化工材料有限责任公司 | A kind of preparation method of the aqueous polyurethane of ultraviolet radiation preventing |
CN108822713A (en) * | 2018-07-15 | 2018-11-16 | 段宝荣 | The preparation method of light-resistant waterborne polyurethane coating and adhesive |
CN109721704A (en) * | 2019-01-11 | 2019-05-07 | 北京理工大学 | A kind of light shield extinguishing waterborn polyurethane and preparation method thereof |
CN114025959A (en) * | 2019-07-12 | 2022-02-08 | 陶氏环球技术有限责任公司 | Water-based composition |
CN114025959B (en) * | 2019-07-12 | 2024-05-14 | 陶氏环球技术有限责任公司 | Water-based composition |
CN111303374A (en) * | 2020-04-02 | 2020-06-19 | 上海应用技术大学 | Brominated soybean oil modified pure water-based polyurethane nano-emulsion and preparation method thereof |
CN113999360A (en) * | 2021-12-02 | 2022-02-01 | 太原理工大学 | Method for preparing flame-retardant waterborne polyurethane from waste polyester textile fabrics |
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