CN103059641B - Colorful PVB (Polyvinyl Butyral) intermediate film and preparation method thereof - Google Patents
Colorful PVB (Polyvinyl Butyral) intermediate film and preparation method thereof Download PDFInfo
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- CN103059641B CN103059641B CN201110323044.4A CN201110323044A CN103059641B CN 103059641 B CN103059641 B CN 103059641B CN 201110323044 A CN201110323044 A CN 201110323044A CN 103059641 B CN103059641 B CN 103059641B
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- pvb
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- intermediate film
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- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 title abstract description 42
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000975 dye Substances 0.000 claims abstract description 9
- 150000002148 esters Chemical class 0.000 claims abstract description 8
- 238000004519 manufacturing process Methods 0.000 claims abstract description 7
- 238000005096 rolling process Methods 0.000 claims abstract description 5
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 10
- 239000004902 Softening Agent Substances 0.000 claims description 7
- QPQKUYVSJWQSDY-UHFFFAOYSA-N 4-phenyldiazenylaniline Chemical compound C1=CC(N)=CC=C1N=NC1=CC=CC=C1 QPQKUYVSJWQSDY-UHFFFAOYSA-N 0.000 claims description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical class CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 6
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 claims description 5
- TVBNRFCUTVWHQB-UHFFFAOYSA-N 1-anilino-4-(methylamino)anthracene-9,10-dione Chemical compound C1=2C(=O)C3=CC=CC=C3C(=O)C=2C(NC)=CC=C1NC1=CC=CC=C1 TVBNRFCUTVWHQB-UHFFFAOYSA-N 0.000 claims description 3
- NMZURKQNORVXSV-UHFFFAOYSA-N 6-methyl-2-phenylquinoline Chemical compound C1=CC2=CC(C)=CC=C2N=C1C1=CC=CC=C1 NMZURKQNORVXSV-UHFFFAOYSA-N 0.000 claims description 3
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 claims description 3
- MRQIXHXHHPWVIL-UHFFFAOYSA-N chembl1397023 Chemical compound OC1=CC=C2C=CC=CC2=C1N=NC1=CC=CC=C1 MRQIXHXHHPWVIL-UHFFFAOYSA-N 0.000 claims description 3
- MIMDHDXOBDPUQW-UHFFFAOYSA-N dioctyl decanedioate Chemical compound CCCCCCCCOC(=O)CCCCCCCCC(=O)OCCCCCCCC MIMDHDXOBDPUQW-UHFFFAOYSA-N 0.000 claims description 3
- OJXOOFXUHZAXLO-UHFFFAOYSA-M magnesium;1-bromo-3-methanidylbenzene;bromide Chemical compound [Mg+2].[Br-].[CH2-]C1=CC=CC(Br)=C1 OJXOOFXUHZAXLO-UHFFFAOYSA-M 0.000 claims description 3
- TVRGPOFMYCMNRB-UHFFFAOYSA-N quinizarine green ss Chemical compound C1=CC(C)=CC=C1NC(C=1C(=O)C2=CC=CC=C2C(=O)C=11)=CC=C1NC1=CC=C(C)C=C1 TVRGPOFMYCMNRB-UHFFFAOYSA-N 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 claims description 2
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims description 2
- PYGXAGIECVVIOZ-UHFFFAOYSA-N Dibutyl decanedioate Chemical compound CCCCOC(=O)CCCCCCCCC(=O)OCCCC PYGXAGIECVVIOZ-UHFFFAOYSA-N 0.000 claims description 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 claims description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 claims description 2
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 125000001931 aliphatic group Chemical group 0.000 claims description 2
- MYONAGGJKCJOBT-UHFFFAOYSA-N benzimidazol-2-one Chemical compound C1=CC=CC2=NC(=O)N=C21 MYONAGGJKCJOBT-UHFFFAOYSA-N 0.000 claims description 2
- 235000019445 benzyl alcohol Nutrition 0.000 claims description 2
- 229960004217 benzyl alcohol Drugs 0.000 claims description 2
- 229940043232 butyl acetate Drugs 0.000 claims description 2
- SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 claims description 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims description 2
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 2
- 229920005989 resin Polymers 0.000 abstract description 5
- 239000011347 resin Substances 0.000 abstract description 5
- 238000000034 method Methods 0.000 abstract description 4
- 239000005340 laminated glass Substances 0.000 abstract description 2
- 238000007646 gravure printing Methods 0.000 abstract 5
- 239000003086 colorant Substances 0.000 abstract 1
- 238000007791 dehumidification Methods 0.000 abstract 1
- 239000004014 plasticizer Substances 0.000 abstract 1
- 239000011521 glass Substances 0.000 description 12
- 239000000976 ink Substances 0.000 description 7
- 238000001125 extrusion Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 206010041662 Splinter Diseases 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- KLQVCADYSBUVAV-UHFFFAOYSA-N 4-[(2,4-dimethylphenyl)diazenyl]-5-methyl-2-phenyl-4h-pyrazol-3-one Chemical compound CC1=NN(C=2C=CC=CC=2)C(=O)C1N=NC1=CC=C(C)C=C1C KLQVCADYSBUVAV-UHFFFAOYSA-N 0.000 description 1
- ZTQSAGDEMFDKMZ-UHFFFAOYSA-N Butyraldehyde Chemical compound CCCC=O ZTQSAGDEMFDKMZ-UHFFFAOYSA-N 0.000 description 1
- GURPRKDCWIMUIF-UHFFFAOYSA-N CCOC(C)=O.CCOC(C)=O.CCOC(C)=O.CCOC(C)=O Chemical compound CCOC(C)=O.CCOC(C)=O.CCOC(C)=O.CCOC(C)=O GURPRKDCWIMUIF-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- DHKHKXVYLBGOIT-UHFFFAOYSA-N acetaldehyde Diethyl Acetal Natural products CCOC(C)OCC DHKHKXVYLBGOIT-UHFFFAOYSA-N 0.000 description 1
- 125000002777 acetyl group Chemical class [H]C([H])([H])C(*)=O 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- HRCGVBPHFJNVNN-UHFFFAOYSA-N butyl acetate Chemical compound C(C)(=O)OCCCC.C(C)(=O)OCCCC.C(C)(=O)OCCCC HRCGVBPHFJNVNN-UHFFFAOYSA-N 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- -1 polyethylene Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
Landscapes
- Joining Of Glass To Other Materials (AREA)
Abstract
The invention provides a preparation method of a colorful PVB (Polyvinyl Butyral) intermediate film. The method comprises the following steps of: (a) additionally arranging a multicolour rotogravure press unit at the rear of a dehumidification section of a PVB diaphragm production line and in front of a rolling section, wherein the multicolour rotogravure press unit comprises at least two gravure printing units; and (b) carrying out gravure printing on fed PVB diaphragms by using each gravure printing unit of the rotogravure press unit to obtain the colorful PVB intermediate film, wherein oil ink used by each gravure printing unit comprises the following components in parts by weight: 6-12 parts of dye, 5-10 parts of PVB resin oatmeal, 3-6 parts of plasticizer, 30-70 parts of alcohol and 30-70 parts of ester, and colors of dyes in oil ink used by all the gravure printing units are different. The invention also provides a PVB intermediate film prepared by using the preparation method. The colorful PVB intermediate film produced by using the method is simple and feasible; and laminated glass made of the colorful PVB intermediate film emits radiant sparkles and is excellent in decorative effect.
Description
Technical field
The present invention relates to a kind of colorful PVB intermediate coat and preparation method thereof.
Background technology
Polyvinyl butyral acetal (PVB) intermediate coat is by a kind of macromolecular material of polyvinyl butyral resin through softening agent plasticating extrusion.The characteristics such as it has good cohesiveness to unorganic glass, has transparent, heat-resisting, cold-resistant, moisture-proof, and physical strength is high.PVB film is the specialty products for the preparation of shatter proof glass, splinter-proof glass.Shatter proof glass is the special glass sandwiching layer of polyethylene butyral (PVB) diaphragm and make between two-layer simple glass, when being subject to extraneous intense impact, pvb film can apparatus with shock absorbing, this glass is made fragmentation not to occur and produce fragment and hurt sb.'s feelings, and the shatter proof glass adding polyvinyl butyral film sheet has high, water-fast, the ageing-resistant characteristic of transparency, and can use in the environment of-60 DEG C, synthetic glass can be replaced in addition to make the products such as transparent material, and namely MULTILAYER COMPOSITE can be made into military splinter-proof glass.
Colour sandwich glass is as a kind of safe finishing material, at present accept by increasing people, be mainly used on mall, hotel, the curtain wall of restaurant's contour level building, skylight, ceiling, partition, safe antitheft door and window, commodity display show window.The way of current color safe glass adds pigment particles when the extrusion moulding of PVB intermediate coat, becomes transparent colored film.But this film color is single, if realize multicolour on a slice film, need multiple stage forcing machine co-extrusion, this method is with high costs and not easily realize.
Summary of the invention
The invention provides a kind of colorful PVB intermediate coat and preparation method thereof, can make to produce this colorful PVB intermediate coat simple, the laminated glass using this colorful PVB intermediate coat to be made into is bright and glittering, and decorative effect is splendid.
A preparation method for colorful PVB intermediate coat, comprises step:
A (), after the dehumidifying section of pvb film production line, before rolling section, installs a multicolour rotogravure press group additional, described multicolour rotogravure press group comprises at least two gravure unit;
B each gravure unit of () described gravure unit carries out gravure to the pvb film sent into can obtain described colorful PVB intermediate coat, and the component of ink that wherein each gravure unit uses according to weight is:
Dyestuff: 6 ~ 12 parts
PVB resin powder: 5 ~ 10 parts
Softening agent: 3 ~ 6 parts
Alcohol: 30 ~ 70 parts
Ester: 30 ~ 70 parts
Wherein in the ink that uses of each gravure unit, the color of dyestuff is different.
Wherein, described dyestuff is one or more in Red-1 200 5, solvent yellow 14, solvent yellow 17, solvent yellow 18, solvent yellow 40, solvent yellow 46, solvent blue 19 02, solvent blue 36, solvent green 3, solvent violet 17.
Wherein, described softening agent is one or more in DHA (dihexyl adipate), 3GO (triglycol two 2-ethylhexoate), 4GO (benzimidazolone yellow), 5G8 (dibasic alcohol special-shaped polyhydric aliphatic acid complex ester), DOS (dioctyl sebacate), DOP (dioctyl phthalate (DOP)) or DBS (Uniflex DBS), is wherein preferably softening agent used when pvb film is extruded.
Wherein, described alcohol is one or more in methyl alcohol, ethanol, n-propyl alcohol, Pentyl alcohol, phenylcarbinol, butanols, Pyranton.
Wherein, described ester is one or more in methyl acetate, ethyl acetate, butylacetate.
A kind of PVB intermediate coat prepared according to above-mentioned preparation method.
The invention has the advantages that: on pvb film production line, install a gravure unit additional can realize continuous prodution, production efficiency is high and simple and easy to do; The PVB intermediate coat of the special-effect such as colorful can be realized by the close specialty inks of telling requirement of intaglio printing press assembly, reach splendid decorative effect.
Accompanying drawing explanation
Fig. 1 is the effect schematic diagram of the colorful PVB intermediate coat using the method for one of them embodiment of the present invention to prepare.
Embodiment
Below in conjunction with specific embodiment, the technical scheme in the present invention is clearly and completely described.
Embodiment 1
A preparation method for colorful PVB intermediate coat, comprises step:
A (), after the dehumidifying section of pvb film production line, before rolling section, installs a multicolour rotogravure press group additional, described multicolour rotogravure press group comprises four gravure unit;
B described pvb film is sent into described gravure unit by (), each gravure unit of described gravure unit carries out gravure to the pvb film sent into can obtain described colorful PVB intermediate coat, and wherein the component of ink that uses of each gravure unit is as shown in table 1 according to weight:
Table 1 gravure ink formula
| Gravure unit 1 | Gravure unit 2 | Gravure unit 3 | Gravure unit 4 | |
| Dyestuff (10 parts) | Solvent blue 19 02 | Solvent green 3 | Red-1 200 5 | Solvent yellow 14 |
| PVB resin powder (8 parts) | PVB | PVB | PVB | PVB |
| Softening agent (3 parts) | 3G8 | 3G8 | 3G8 | 3G8 |
| Alcohol (30 parts) | Butanols | Butanols | Butanols | Butanols |
| Ester (70 parts) | Ethyl acetate | Ethyl acetate | Ethyl acetate | Ethyl acetate |
Embodiment 2
A preparation method for colorful PVB intermediate coat, comprises step:
A (), after the dehumidifying section of pvb film production line, before rolling section, installs a multicolour rotogravure press group additional, described multicolour rotogravure press group comprises four gravure unit;
B described pvb film is sent into described gravure unit by (), each gravure unit of described gravure unit carries out gravure to the pvb film sent into can obtain described colorful PVB intermediate coat, and wherein the component of ink that uses of each gravure unit is as shown in table 2 according to weight:
Table 2 gravure ink formula
| Gravure unit 1 | Gravure unit 2 | Gravure unit 3 | |
| Dyestuff (12 parts) | Solvent blue 36 | Solvent yellow 40 | Solvent violet 17 |
| PVB resin powder (10 parts) | PVB | PVB | PVB |
| Softening agent (6 parts) | 3G8 | 3G8 | 3G8 |
| Alcohol (30 parts) | N-propyl alcohol | N-propyl alcohol | N-propyl alcohol |
| Ester (70 parts) | Butylacetate | Butylacetate | Butylacetate |
The above; be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, anyly belongs to those skilled in the art in the technical scope that the present invention discloses; the change that can expect easily or replacement, all should be encompassed within protection scope of the present invention.
Claims (2)
1. a preparation method for colorful PVB intermediate coat, is characterized in that: comprise
A (), after the dehumidifying section of pvb film production line, before rolling section, installs a multicolour rotogravure press group additional, described multicolour rotogravure press group comprises at least two gravure unit;
B each gravure unit of () described gravure unit carries out gravure to the pvb film sent into can obtain described colorful PVB intermediate coat, and the component of ink that wherein each gravure unit uses according to weight is:
Wherein in the ink that uses of each gravure unit, the color of dyestuff is different;
Described dyestuff is one or more in Red-1 200 5, solvent yellow 14, solvent yellow 17, solvent yellow 40, solvent blue 19 02, solvent blue 36, solvent green 3, solvent violet 17;
Described softening agent is one or more in dihexyl adipate, triglycol two 2-ethylhexoate, benzimidazolone yellow, dibasic alcohol special-shaped polyhydric aliphatic acid complex ester, dioctyl sebacate, dioctyl phthalate (DOP), Uniflex DBS;
Described alcohol is one or more in methyl alcohol, ethanol, n-propyl alcohol, Pentyl alcohol, phenylcarbinol, butanols, Pyranton;
Described ester is one or more in methyl acetate, ethyl acetate, butylacetate.
2. the PVB intermediate coat prepared according to preparation method described in claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110323044.4A CN103059641B (en) | 2011-10-21 | 2011-10-21 | Colorful PVB (Polyvinyl Butyral) intermediate film and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110323044.4A CN103059641B (en) | 2011-10-21 | 2011-10-21 | Colorful PVB (Polyvinyl Butyral) intermediate film and preparation method thereof |
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| Publication Number | Publication Date |
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| CN103059641A CN103059641A (en) | 2013-04-24 |
| CN103059641B true CN103059641B (en) | 2014-12-24 |
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| CN201110323044.4A Active CN103059641B (en) | 2011-10-21 | 2011-10-21 | Colorful PVB (Polyvinyl Butyral) intermediate film and preparation method thereof |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103740014B (en) * | 2013-12-27 | 2016-04-13 | 齐鲁工业大学 | A kind of color safe glass interlayer plastics film and production method thereof |
| CN105860645B (en) * | 2016-04-14 | 2018-05-29 | 镇江恒昌彩艺科技有限公司 | One kind is used for PVC intaglio plate environment-friendly ink compositions |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5470316A (en) * | 1977-11-16 | 1979-06-06 | Sekisui Chemical Co Ltd | Method of making intermediate layer for laminated glass |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070087137A9 (en) * | 2003-06-26 | 2007-04-19 | Elwakil Hamdy A | Decorative laminated safety glass |
| JP4852031B2 (en) * | 2004-03-02 | 2012-01-11 | イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー | Decorative laminated safety glass |
| CN101258027A (en) * | 2005-08-31 | 2008-09-03 | 纳幕尔杜邦公司 | Solar control laminate |
| WO2009008857A1 (en) * | 2007-07-09 | 2009-01-15 | E. I. Du Pont De Nemours And Company | Decorative polyvinyl butyral solar control laminates |
| CN101722749A (en) * | 2009-12-10 | 2010-06-09 | 上海烟草（集团）公司 | Multicolour photogravure method |
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- 2011-10-21 CN CN201110323044.4A patent/CN103059641B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5470316A (en) * | 1977-11-16 | 1979-06-06 | Sekisui Chemical Co Ltd | Method of making intermediate layer for laminated glass |
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