CN103058532B - Antiultraviolet composite fireproof glass - Google Patents
Antiultraviolet composite fireproof glass Download PDFInfo
- Publication number
- CN103058532B CN103058532B CN201110321264.3A CN201110321264A CN103058532B CN 103058532 B CN103058532 B CN 103058532B CN 201110321264 A CN201110321264 A CN 201110321264A CN 103058532 B CN103058532 B CN 103058532B
- Authority
- CN
- China
- Prior art keywords
- fireproofing
- glass
- composite fireproof
- fireproof glass
- glass substrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000011521 glass Substances 0.000 title claims abstract description 30
- 239000002131 composite material Substances 0.000 title claims abstract description 11
- 238000004079 fireproofing Methods 0.000 claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 claims abstract description 12
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000000758 substrate Substances 0.000 claims abstract description 8
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims abstract description 6
- 239000000347 magnesium hydroxide Substances 0.000 claims abstract description 6
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims abstract description 6
- DXGLGDHPHMLXJC-UHFFFAOYSA-N oxybenzone Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1 DXGLGDHPHMLXJC-UHFFFAOYSA-N 0.000 claims abstract description 6
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims abstract description 6
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims abstract description 4
- 230000002265 prevention Effects 0.000 claims abstract 2
- 230000000694 effects Effects 0.000 claims description 9
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims description 5
- 150000004702 methyl esters Chemical class 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims 1
- 230000005540 biological transmission Effects 0.000 abstract description 6
- 238000005187 foaming Methods 0.000 abstract description 4
- 239000003292 glue Substances 0.000 description 13
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 2
- 239000013543 active substance Substances 0.000 description 2
- 230000002528 anti-freeze Effects 0.000 description 2
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 description 2
- 239000012965 benzophenone Substances 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 235000011089 carbon dioxide Nutrition 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000005202 decontamination Methods 0.000 description 2
- 230000003588 decontaminative effect Effects 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 239000000314 lubricant Substances 0.000 description 2
- 230000010412 perfusion Effects 0.000 description 2
- 230000000176 photostabilization Effects 0.000 description 2
- 230000002829 reductive effect Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- 239000011787 zinc oxide Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241000237502 Ostreidae Species 0.000 description 1
- 239000002390 adhesive tape Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005238 degreasing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 239000005357 flat glass Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000005816 glass manufacturing process Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000005340 laminated glass Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000003032 molecular docking Methods 0.000 description 1
- 235000020636 oyster Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000004904 shortening Methods 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
- 239000005341 toughened glass Substances 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
Landscapes
- Joining Of Glass To Other Materials (AREA)
Abstract
The invention discloses one and effectively can intercept ultraviolet fire prevention composite structure glass, comprise two panels glass substrate, be filled with fireproofing in two panels glass substrate, fireproofing comprises first first junket 50%, dibutylester 15%, S-WAT 20%, zinc oxide (ZNO) 1.3%, magnesium hydroxide 3%, phthalic acid fourth Bian fat 0.2%, acrylamide 10%, ethanol 0.1%, ESCALOL 567 0.4% by weight percentage.The present invention adopts the fireproofing of this kind of formula, and effectively can intercept ultraviolet, fire performance is good, and under long-time using state, fireproofing is not easy foaming, and therefore light transmission is good.
Description
[technical field]
The invention belongs to flame resistant glass Material Field, especially there is the composite fireproof glass of antiultraviolet effect.
[background technology]
Antiultraviolet composite fireproof glass is the structure at two sheet glass central filler fireproofings, and when by uviolizing, fireproofing specific proportions batching can effective ultraviolet-cutoff and light transmission is good; When fire occurs, fireproofing specific proportions batching will absorb the heat of flame transmission in large quantities by foaming and intumescing, and the heat stoping burning to produce is from counter-fire towards the transmission in the fiery face of the back of the body.In actual use, it is more weak that common composite fireproof glass penetrates obstructing capacity to ultraviolet, and under ultraviolet long-term irradiation, fire-resistant fluid can become oyster white and produce steam bubble, loses the transparent functional of glass, thus limits its range of application.And common pad pasting or coating against UV-radiation glass are also because of the restriction of working life, the occasion that particularly sunlight equitemperature is slightly high, its aging speed is constantly accelerated, and rete, coating go bad gradually, and effect weakens in time.
[summary of the invention]
The object of the invention is to the deficiency overcoming above-mentioned existence, provide a kind of stability high and can effectively intercept ultraviolet composite fireproof glass.
The object of the invention is to have come by following technical solution, antiultraviolet composite fireproof glass, comprises two panels glass substrate, is filled with fireproofing in two panels glass substrate, and fireproofing comprises following components by weight percentage:
First methyl esters 50%; Dibutylester 15%; S-WAT 20%;
Zinc oxide (ZnO) 1.3%; Magnesium hydroxide 3%; Phthalic acid fourth benzyl fat 0.2%;
Acrylamide 10%; Ethanol 0.1%; ESCALOL 567 0.4%.
Each component function illustrates:
1, ESCALOL 567
It contains the benzophenone of two vicinal hydroxyl groups, absorbs ultraviolet ability the strongest, has strong absorption effect to the UV-light that wavelength is 330-370nm.
2, phthalic acid fourth benzyl fat
Strengthen goods thermotolerance, photostabilization and winter hardiness.
3, zinc oxide
Absorb ultraviolet.
4, first methyl esters
Methyl methacrylate, molecular formula is C5H8O2, specific refractory power 1.4142.
5, dibutylester
Lubricant and tenderizer.
6, S-WAT
Bleaching reductive agent, sanitas, antichlor etc.
7, magnesium hydroxide
Carbonic acid gas in easy absorption air.
8, ethanol
Reduce freezing point of solution, play antifreeze effect; Due to the existence of tensio-active agent, by wetting infiltration, the effect of reach clean decontamination, enhancing the transparency.
The present invention adopts the fireproofing of this kind of formula, and effectively can intercept ultraviolet, fire performance is good, and under long-time using state, fireproofing is not easy foaming, and therefore light transmission is good.
[embodiment]
Detailed introduction is done to fireproofing component of the present invention and compound glass manufacturing process below:
Antiultraviolet composite fireproof glass, comprises two panels glass substrate, is filled with fireproofing in two panels glass substrate, and glass substrate can adopt toughened glass, and fireproofing comprises following components by weight percentage:
First methyl esters 50%; Dibutylester 15%; S-WAT 20%;
Zinc oxide (ZnO) 1.3%; Magnesium hydroxide 3%; Phthalic acid fourth benzyl fat 0.2%;
Acrylamide 10%; Ethanol 0.1%; ESCALOL 567 0.4%.
Each component function illustrates:
1, ESCALOL 567
It contains the benzophenone of two vicinal hydroxyl groups, absorbs ultraviolet ability the strongest, has strong absorption effect to the UV-light that wavelength is 330-370nm.
2, phthalic acid fourth benzyl fat
Strengthen goods thermotolerance, photostabilization and winter hardiness.
3, zinc oxide
Absorb ultraviolet.
4, first methyl esters
Methyl methacrylate, molecular formula is C5H8O2, specific refractory power 1.4142.
5, dibutylester
Lubricant and tenderizer.
6, S-WAT
Bleaching reductive agent, sanitas, antichlor etc.
7, magnesium hydroxide
Carbonic acid gas in easy absorption air.
8, ethanol
Reduce freezing point of solution, play antifreeze effect; Due to the existence of tensio-active agent, by wetting infiltration, the effect of reach clean decontamination, enhancing the transparency.
The present invention adopts the fireproofing of this kind of formula, and effectively can intercept ultraviolet, fire performance is good, and under long-time using state, fireproofing is not easy foaming, and therefore light transmission is good.
Below introduce the manufacturing operation code of compound glass:
1) size cutting glass plate on demand, scale error < 0.2mm.
2) glass fine-grinding four limit, and send into temperature tempering in the annealing furnace of 650-750 DEG C
3) wash away with softening water after coming out of the stove; Good perfusion face, first with dry cloth wiping, ensures clean clean.
4) use cloth to wipe with wipe dry after, then be stained with acetone wiping degreasing with clean cotton, can not there be greasy dirt or dirt settling in surface, for subsequent use.
5), on the glass after one piece wiping, joint strip is sticked along limit.After real, by angle injecting glue entrance being stayed the one end on the long limit of glass.
6) sealed strip is in stitching portion, is cut into 45 degree of docking, during joint close, adhesive tape is coated with some glue preventing from cementing leakages.
7) joint strip will develop, compacting.Do not allow artificial elongation or shortening, prevent shrink, wrinkling.
8) after glazing tape posts, with " dovetail clip ", glass surrounding is clipped, aligns, reserve injecting glue entrance and venting hole.The glue injection frame being placed in inclination gets final product injecting glue.The tank glue device made with pop can is inserted tank Jiao Kou, inserts tank glue device with screwdriver, slightly glass is strutted some gaps, facilitate the quick person who lives in exile of glue.
9) thick with every square of rice glue: the 1. ratio metering glue consumption of 0.38mm/0.45Kg, 2. 0.76mm/0.86Kg, 3. 1mm/1.14Kg, calculates the perfusion of glue consumption by physical size, extract tank glue device, checked whether bubble after injection.As found that there is bubble, using to knock or put in syringe derives bubble.
10) slowly universal stage is rotated to level attitude, glue is refluxed, be full of whole glass chamber completely, close gum-injecting port.
11), after laminated glass work in-process rationally put into still car, fixing situation is checked;
12) connect the rail joints of rotating disk and kettle, at the uniform velocity will enter still car and advance still internal fixtion;
13) autoclave operation work removes rail joints link, and translation interface platform closes still door;
14) turn on the power switch, setting Heating temperature 132 DEG C, preheating temperature 55 DEG C, exhaust temperature 55 DEG C, setting soaking time 30-60min, check whether vent valve is opened.
15) start swing to close the door, be rocked to travel switch place, start rotation and close the door, be threaded to travel switch place.
16) bat-handle switch on closed still door limit, starts autoclave.Open little intake valve, open little water pump, open air compressor machine, open intake valve.
17) air pressure reaches set(ting)value ± 12MPA, closes air compressor machine, closes master air suction valve.Temperature reaches 132 DEG C, and after carrying out heat-insulation pressure keeping, open cooling-water pump and make temperature in the kettle be down to 55 DEG C, autoclave out of service, vent valve opens exhaust automatically, turns off cooling-water pump.
18) when still internal gas pressure is drained, display with no pressure in operation cabinet still, opens bat-handle switch, swings and open the door, turn to open.
19) finished product shelves warehouse-in through inspection.
Claims (2)
1. an antiultraviolet composite fireproof glass, is characterized in that: the fireproofing being filled with special proportioning in two panels glass substrate, and fireproofing comprises following composition by weight percentage:
First methyl esters 50%; Dibutylester 15%; S-WAT 20%;
Zinc oxide (ZnO) 1.3%; Magnesium hydroxide 3%; Phthalic acid fourth benzyl fat 0.2%;
Acrylamide 10%; Ethanol 0.1%; ESCALOL 567 0.4%.
2. antiultraviolet composite fireproof glass according to claim 1 is characterized in that: based on fire prevention effect outer to have ultraviolet penetrate obstructing capacity, and not exposure time limitation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110321264.3A CN103058532B (en) | 2011-10-18 | 2011-10-18 | Antiultraviolet composite fireproof glass |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110321264.3A CN103058532B (en) | 2011-10-18 | 2011-10-18 | Antiultraviolet composite fireproof glass |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103058532A CN103058532A (en) | 2013-04-24 |
| CN103058532B true CN103058532B (en) | 2015-09-09 |
Family
ID=48101468
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110321264.3A Expired - Fee Related CN103058532B (en) | 2011-10-18 | 2011-10-18 | Antiultraviolet composite fireproof glass |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103058532B (en) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103232159A (en) * | 2013-05-10 | 2013-08-07 | 苏州工业园区方圆金属制品有限公司 | Multifunctional plate glass |
| CN106183243A (en) * | 2016-07-27 | 2016-12-07 | 泉州市科茂利通智能科技有限公司 | A kind of windshield |
| CN107640914A (en) * | 2017-10-10 | 2018-01-30 | 浙江树人学院 | The fire prevention perfusion and encapsulating method of a kind of filling type flame resistant glass |
| CN107915416A (en) * | 2017-11-27 | 2018-04-17 | 信利光电股份有限公司 | A kind of liquid filling method and its system |
| CN108490998A (en) * | 2018-02-02 | 2018-09-04 | 信义玻璃工程（东莞）有限公司 | A kind of control method of autoclave, system and terminal device |
| CN108483905A (en) * | 2018-05-14 | 2018-09-04 | 江苏铁锚玻璃股份有限公司 | A kind of vehicle glass and its manufacturing method |
| CN108585526A (en) * | 2018-05-15 | 2018-09-28 | 江苏铁锚玻璃股份有限公司 | A kind of aircraft glass and its manufacturing method |
| CN111635148B (en) * | 2020-07-08 | 2024-07-23 | 广东平治防火材料有限公司 | Fireproof laminated glass and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN88100180A (en) * | 1988-01-20 | 1988-08-03 | 北京市有机玻璃制品厂 | X-ray-preventing ultraviolet ray synthetic glass and method for making |
| CN1394741A (en) * | 2002-07-10 | 2003-02-05 | 黄志清 | Photochromic sandwich glass |
| CN1898175A (en) * | 2003-12-26 | 2007-01-17 | 积水化学工业株式会社 | Interlayer film for laminated glass, and laminated glass |
| CN201419535Y (en) * | 2009-05-25 | 2010-03-10 | 席德水 | Fireproof compound glass |
| JP2011168477A (en) * | 2010-01-22 | 2011-09-01 | Nippon Electric Glass Co Ltd | Fireproof protective plate glass with antireflection film, fireproof protective laminated glass with the antireflection film, and specific fire prevention apparatus |
-
2011
- 2011-10-18 CN CN201110321264.3A patent/CN103058532B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN88100180A (en) * | 1988-01-20 | 1988-08-03 | 北京市有机玻璃制品厂 | X-ray-preventing ultraviolet ray synthetic glass and method for making |
| CN1394741A (en) * | 2002-07-10 | 2003-02-05 | 黄志清 | Photochromic sandwich glass |
| CN1898175A (en) * | 2003-12-26 | 2007-01-17 | 积水化学工业株式会社 | Interlayer film for laminated glass, and laminated glass |
| CN201419535Y (en) * | 2009-05-25 | 2010-03-10 | 席德水 | Fireproof compound glass |
| JP2011168477A (en) * | 2010-01-22 | 2011-09-01 | Nippon Electric Glass Co Ltd | Fireproof protective plate glass with antireflection film, fireproof protective laminated glass with the antireflection film, and specific fire prevention apparatus |
Non-Patent Citations (2)
| Title |
|---|
| 温变英.添加剂概论.《高分子材料与加工》.中国轻工业出版社,2011, * |
| 王国建等.复合型防火玻璃防火层的类型和特点.《建筑防火材料》.中国石化出版社,2006, * |
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| Publication number | Publication date |
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| CN103058532A (en) | 2013-04-24 |
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Addressee: Wang Zheng Document name: Notification of Publication and of Entering the Substantive Examination Stage of the Application for Invention |
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| ASS | Succession or assignment of patent right |
Owner name: HANGZHOU FULONGDING DOOR WINDOW AND CURTAIN WALL C Free format text: FORMER OWNER: ZHEJIANG FULONGDING GLASS TECHNOLOGY CO., LTD. Effective date: 20141128 |
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Effective date of registration: 20141128 Address after: 311228, 555 Jinsha Road, No. 26 Haida South Road, Hangzhou economic and Technological Development Zone, Zhejiang Province, room 10, floor 3 Applicant after: Zhejiang Fulongding Glass Technology Co., Ltd. Address before: Go Green Road Industrial Park, No. 199 Zhejiang fulongding Glass Technology Co., Ltd. Hangzhou City, Zhejiang province 310018 Hangzhou economic and Technological Development Zone Applicant before: Zhejiang Fulongding Glass Technology Co., Ltd. |
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