CN103052317A - Noxious arthropod control composition and noxious arthropod control method - Google Patents
Noxious arthropod control composition and noxious arthropod control method Download PDFInfo
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- CN103052317A CN103052317A CN2011800378683A CN201180037868A CN103052317A CN 103052317 A CN103052317 A CN 103052317A CN 2011800378683 A CN2011800378683 A CN 2011800378683A CN 201180037868 A CN201180037868 A CN 201180037868A CN 103052317 A CN103052317 A CN 103052317A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom
- A01N47/06—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having no bond to a nitrogen atom containing —O—CO—O— groups; Thio analogues thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
- A01N43/38—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
- A01N37/22—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
- A01N37/24—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides containing at least one oxygen or sulfur atom being directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/56—1,2-Diazoles; Hydrogenated 1,2-diazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/32—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing >N—CO—N< or >N—CS—N< groups directly attached to a cycloaliphatic ring
Abstract
A noxious arthropod control composition comprising spirotetramat and at least one sheath blight disease control compound selected from the group (A). Group (A): consisting of flutolanil, pencycuron, furametpyr and validamycin A.
Description
Technical field
The present invention relates to prevent and kill off pest with composition and the method for preventing and kill off pest.
Background technology
In the past, as the active ingredient of the composition of preventing and kill off harmful arthropod, known had a large amount of compounds (for example with reference to The Pesticide Manual-15th edition (BCPC periodical); ISBN978-1-901396-18-8).
Summary of the invention
Problem of the present invention is to provide has the effectiveness of the composition of preventing and kill off harmful arthropod prevent and kill off to(for) the excellence of harmful arthropod.
That is, the present invention relates to following [1]～[6].
[1] a kind of composition of preventing and kill off harmful arthropod, the compound of preventing and kill off banded sclerotial blight more than a kind that it contains spiral shell worm ethyl ester and is selected from group (A).
The group that group (A) is comprised of flutolanil (flutolanil), Pencycuron (pencycuron), good fortune Lapie and Validacin (Takeda).
[2] according to [1] described composition of preventing and kill off harmful arthropod, wherein, the compound of preventing and kill off banded sclerotial blight is flutolanil or good fortune Lapie.
[3] according to [1] or [2] described composition of preventing and kill off harmful arthropod, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of banded sclerotial blight.
[4] a kind of method of preventing and kill off harmful arthropod, it comprises the operation that spiral shell worm ethyl ester and the compound of preventing and kill off banded sclerotial blight more than a kind that is selected from group (A) is applied to the cultivation ground of plant or plant with effective dose.
The group that group (A) is comprised of flutolanil, Pencycuron, good fortune Lapie and Validacin (Takeda).
[5] according to [4] described the method for control, wherein, the compound of preventing and kill off banded sclerotial blight is flutolanil or good fortune Lapie.
[6] according to [4] or [5] described the method for control, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of banded sclerotial blight.
[7] according to each described the method for control in [4]～[6], wherein, harmful arthropod is the insect that belongs to the Delphacidae class.
[8] according to each described the method for control in [4]～[6], wherein, harmful arthropod is brown planthopper, white-backed planthopper or small brown rice planthopper.
Embodiment
The composition that the composition of preventing and kill off harmful arthropod of the present invention refers to contain spiral shell worm ethyl ester and is selected from the compound of preventing and kill off banded sclerotial blight more than a kind (the following compound of originally preventing and kill off banded sclerotial blight that sometimes is designated as) of following group (A).
Group (A): formed by flutolanil, Pencycuron, good fortune Lapie and Validacin (Takeda).
As above-mentioned typical case of preventing and kill off the compound of banded sclerotial blight, can enumerate flutolanil and good fortune Lapie.
Spiral shell worm ethyl ester is known compound, and the method that for example can utilize Japanese Unexamined Patent Application Publication 2000-516918 communique to put down in writing is made.
Flutolanil, Pencycuron, good fortune Lapie and valida are known compound, for example are recorded in " The Pesticide Manual-15
ThEdition (BCPC periodical); ISBN978-1-901396-18-8 " 559,871,580 and 1187 pages etc. in.These compounds can be obtained by commercially available preparation, perhaps obtain by known method manufacturing.
In the composition of preventing and kill off harmful arthropod of the present invention, proportional being not particularly limited that contain of spiral shell worm ethyl ester and the compound of originally preventing and kill off banded sclerotial blight, with respect to spiral shell worm ethyl ester 1000 weight portions, the compound of originally preventing and kill off banded sclerotial blight is generally 10～1000000 weight portions (being spiral shell worm ethyl ester: prevent and kill off the compound (weight ratio) of banded sclerotial blight=100: 1～1: 1000), be preferably 100～100000 weight portions (spiral shell worm ethyl ester: prevent and kill off the compound (weight ratio) of banded sclerotial blight=10: 1～1: 100), 100～10000 weight portions (spiral shell worm ethyl ester: prevent and kill off the compound (weight ratio) of banded sclerotial blight=10: 1～1: 10 more preferably.
The composition of preventing and kill off harmful arthropod of the present invention can be for only mixing spiral shell worm ethyl ester and the composition of originally preventing and kill off the compound of banded sclerotial blight; Also spiral shell worm ethyl ester and the compound of originally preventing and kill off banded sclerotial blight can be mixed with non-active carrier, and add as required surfactant, other preparation auxiliary material, thereby make finish, emulsion, suspension, hydrating agents, particle hydrating agents, pulvis, granula etc.
In addition, the above-mentioned composition of preventing and kill off harmful arthropod through preparation can directly use, and perhaps adds other non-active ingredient (water, sand, plant wet goods) and uses as the harmful arthropod agent for preventing and eliminating.
In the composition of preventing and kill off harmful arthropod of the present invention, spiral shell worm ethyl ester and the total amount of originally preventing and kill off the compound of banded sclerotial blight be generally 0.01～99 % by weight, be preferably the scope of 0.1～90 % by weight, the scope of 0.5～70 % by weight more preferably.
As above-mentioned non-active carrier, can enumerate solid carrier, liquid-carrier etc.
As solid carrier, can enumerate mineral such as comprising kaolin, attapulgite clay, bentonite, montmorillonite, Emathlite, pyrophyllite, talcum, diatomite, calcite; The natural organic matters such as corncob powder, walnut parting; The synthesis of organic substance such as urea; The salt such as calcium carbonate, ammonium sulfate; The synthesizing inorganic things such as synthetic oxidizing aqueous silicon; Deng micro mist or shot-like particle etc.
As liquid-carrier, dimethylbenzene, alkylbenzene, methyl naphthalene etc. are aromatic hydrocarbon based such as enumerating; The alcohols such as 2-propyl alcohol, ethylene glycol, propane diols, ethylene glycol monoethyl ether; The ketones such as acetone, cyclohexanone, isophorone; Soybean oil, cottonseed wet goods vegetable oil; The petroleum aliphatic hydrocarbon; The ester class; Dimethyl sulfoxide (DMSO); Acetonitrile; And water.
As surfactant, such as enumerating the anion surfactants such as alkyl sulfate salt, alkylaryl sulfonates, dialkyl sulfosuccinates, polyoxyethylene alkylaryl ether phosphate ester salt, lignosulphonates, napsylate formaldehyde condensation products; The non-ionic surface active agents such as polyoxyethylene alkylaryl ether, polyxyethylated polyoxypropylene block copolymers, fatty acid esters of sorbitan; Reach the cationic surfactants such as alkyl trimethyl ammonium salt.
As other preparation auxiliary material, can enumerate the water soluble polymers such as polyvinyl alcohol, polyvinylpyrrolidone; Gum Arabic, alginic acid and salt thereof; The polysaccharoses such as carboxymethyl cellulose (CMC), xanthans; The inorganic matter such as Magnesiumaluminumsilicate, alumina gel; Preservative; Colouring agent; Reach the stabilizing agents such as acid phosphatase isopropyl ester (PAP), BHT.
The composition of preventing and kill off harmful arthropod of the present invention can be used for protective plant and avoids the persecution undertaken by the harmful arthropod of plant being ingested, inhales the persecution such as juice (for example harmful insect and harmful tick).
As the harmful arthropod that the composition of preventing and kill off harmful arthropod of the present invention has the effectiveness of preventing and kill off, for example can enumerate following arthropods.
Semiptera insect: small brown rice planthopper (Laodelphax striatellus), brown planthopper (Nilaparvata lugens), the plant hoppers such as white-backed planthopper (Sogatella furcifera), caudal lobe cicada (Nephotettix cincticeps), the leafhopper classes such as nephotettix bipunctatus (Nephotettix virescens), cotten aphid (Aphis gossypii), black peach aphid (Myzus persicae), cabbage aphid (Brevicoryne brassicae), potato aphid (Macrosiphum euphorbiae), the eggplant ditch is without net aphid (Aulacorthum solani), rhopalosiphum padi (Rhopalosiphum padi), the aphid classes such as citrus aphid (Toxoptera citricidus), trialeurodes vaporariorum (Trialeurodes vaporariorum), Bemisia tabaci (Bemisia tabaci), the aleyrodid classes such as Bemisia argentifolii (Bemisia argentifolii), California red scale (Aonidiella aurantii), san jose scale (Comstockaspis perniciosa), arrowhead scales (Unaspis citri), ceroplastes rubens (Ceroplastes rubens), the a red-spotted lizard classes such as cottonycushion scale (Icerya purchasi) etc.;
Acarina pest: the mite classes such as Tetranychus urticae (Tetranychus urticae), tangerine Panonychus citri (Panonychus citri), Oligonychus etc.;
In above-mentioned harmful arthropod, as preference, can enumerate the plant hoppers such as small brown rice planthopper (Laodelphax striatellus), brown planthopper (Nilaparvata lugens), white-backed planthopper (Sogatella furcifera).
The composition of preventing and kill off harmful arthropod of the present invention can be used as purpose to prevent and kill off plant disease, such as the banded sclerotial blight that can prevent and kill off rice (Rhizoctonia solani) etc.
The composition of preventing and kill off harmful arthropod of the present invention for example can be used to prevent and kill off harmful arthropod by the cultivation ground that is applied to plant or plant.At this, as the place of using of plant, can enumerate the cauline leaf of plant, the flower of plant, the fruit of plant, the seed of plant etc.
Method of preventing and kill off harmful arthropod of the present invention comprises spiral shell worm ethyl ester and is selected from the compound of preventing and kill off banded sclerotial blight more than a kind in above-mentioned group (A) is applied to the cultivation ground of plant or plant with effective dose operation.In this method of control, the typical case of the above-mentioned compound of preventing and kill off banded sclerotial blight is identical with the composition of preventing and kill off harmful arthropod of the present invention.
The method of harmful arthropod of preventing and kill off of the present invention is such as being undertaken by the composition of preventing and kill off harmful arthropod of the present invention being applied to plant etc.
As the example of using of the composition of preventing and kill off harmful arthropod of the present invention, spiral shell worm ethyl ester and the above-mentioned compound of preventing and kill off banded sclerotial blight, can enumerate cauline leaf distribution etc. to the processing of the cauline leaf of plant, soil treatment etc. to the processing on the cultivation ground of plant etc.
When harmful arthropod composition of the present invention being applied to the cultivation ground of plant or plant, its amount of application is that effective dose gets final product, can be according to the kind of the plant of using, changed as the kind of preventing and kill off the harmful arthropod of object, occurrence degree, preparation form, toeatment period, meteorological condition etc., but as spiral shell worm ethyl ester and the total amount of originally preventing and kill off the compound of banded sclerotial blight, the every 10000m in place that cultivates this plant
2Be generally 1～5000g, be preferably 10～500g.In this manual, effective dose refers to spiral shell worm ethyl ester and above-mentioned total amount of application of preventing and kill off the compound of banded sclerotial blight, refers to the amount of application be used to the necessity of preventing and kill off harmful arthropod.
Composition, spiral shell worm ethyl ester and the above-mentioned compound of preventing and kill off banded sclerotial blight of preventing and kill off harmful arthropod of the present invention usually scatters by dilute with water and used in the situation for emulsion, hydrating agents, suspension etc.In this case, spiral shell worm ethyl ester and total concentration of originally preventing and kill off the compound of banded sclerotial blight are generally 0.0001～3 % by weight, are preferably the scope of 0.0005～1 % by weight.Composition, spiral shell worm ethyl ester and the above-mentioned compound of preventing and kill off banded sclerotial blight of preventing and kill off harmful arthropod of the present invention is in the situation of pulvis, granula etc., usually need not the dilution and directly use.
Method of preventing and kill off harmful arthropod of the present invention can should be used for carrying out in the crop land in dry land, paddy field, lawn, fruit tree garden etc. or non-agricultural cultivated land.
In addition, the present invention can be used for preventing and kill off the harmful arthropod of this crop land in crop land of following cited cultivation " plant " etc. etc. and uses.
Crops: corn, rice, wheat, barley, rye, oat, Chinese sorghum, cotton, soybean, peanut, pea, French beans, buckwheat, beet, rape seed, sunflower, sugarcane, tobacco etc.,
Vegetables: solanaceous vegetable (eggplant, tomato, green pepper, capsicum, potato etc.), cucurbitaceae vegetable (cucumber, custard squash (pumpkin), zucchini, watermelon, muskmelon, pumpkin (squash) etc.), rape section vegetables (radish, turnip, horseradish, root-mustard, Chinese cabbage, cabbage, leaf mustard, brocoli, cauliflower etc.), composite vegetable (burdock, crowndaisy chrysanthemum, artichoke, lettuce etc.), liliaceous vegetable (green onion, onion, garlic, asparagus etc.), umbrella flower section vegetables (carrot, caraway, celery, parsnip etc.), goosefoot vegetable (spinach, Swiss chard etc.), lip vegetables (purple perilla, peppermint, sweet basil etc.), strawberry, sweet potato, sweet potato, taro etc.
Flowers (rose, chrysanthemum etc.),
Ornamental foliage plant,
Lawn (lawn grasses),
Fruit tree: pomaceous fruit (apple, European pear, Japanese pear, pawpaw Quinces Quince fruit etc.), drupe class (peach, plum, nectarine, plum, Huang Tao, apricot, prune etc.), citrus (satsuma mandarin, orange, lemon, bitter orange, grapefruit etc.), nut fruits (chestnut, English walnut, fibert, almond, the pistachio fruit, cashew nut, macadamia nut etc.), soft fruits (blueberry berry, red certain kind of berries tongue, blackberry, blueberry, raspberry etc.), grape, persimmon, olive, loquat, banana, coffee, date palm, coconut palm etc.
Tree beyond the fruit tree: tea tree, mulberry tree, flowering tree class, street tree (such as ash tree, birch, dogwood, eucalyptus, ginkgo, cloves, maple, filigree, white poplar, cercis, Chinese sweet gum, plane tree, Zelkova, arbor-vitae, fir, siebold hemlock, needle juniper, pine tree, juniper, yew etc.)
In above-mentioned plant, can enumerate corn, wheat, rice as preference, as more preferably the example and can enumerate rice.
Above-mentioned " plant " can be by give the plant of patience based on the method for breeding of genetic recombination, hybridization.
Embodiment
Below, by formulation example and test example the present invention further being described in detail, the present invention not only is defined as following example.It should be noted that in following example, part is not having to represent weight portion in the situation about specifying.
Formulation example 1
10 parts of 10 parts of spiral shell worm ethyl esters and flutolanils are joined in the mixture that is mixed with 54 parts in 4 parts of NaLSs, 2 parts of Lignosites, 20 parts at synthetic oxidizing aqueous silicon powder end and diatomite, mix fully and obtain hydrating agents.
Formulation example 2
10 parts of 10 parts of spiral shell worm ethyl esters and Pencycurons are joined in the mixture that is mixed with 54 parts in 4 parts of NaLSs, 2 parts of Lignosites, 20 parts at synthetic oxidizing aqueous silicon powder end and diatomite, mix fully and obtain hydrating agents.
Formulation example 3
10 parts of 10 parts of spiral shell worm ethyl esters and good fortune Lapies are joined in the mixture that is mixed with 54 parts in 4 parts of NaLSs, 2 parts of Lignosites, 20 parts at synthetic oxidizing aqueous silicon powder end and diatomite, mix fully and obtain hydrating agents.
Formulation example 4
10 parts of 10 parts of spiral shell worm ethyl esters and Validacin (Takeda)s are joined in the mixture that is mixed with 54 parts in 4 parts of NaLSs, 2 parts of Lignosites, 20 parts at synthetic oxidizing aqueous silicon powder end and diatomite, mix fully and obtain hydrating agents.
Formulation example 5
By being pulverized and mixed fully, 10 parts in 2 parts of spiral shell worm ethyl esters, 1 part of flutolanil, 87 parts of kaolin and talcum obtain pulvis.
Formulation example 6
By being pulverized and mixed fully, 10 parts in 2 parts of spiral shell worm ethyl esters, 1 part of Pencycuron, 87 parts of kaolin and talcum obtain pulvis.
Formulation example 7
By being pulverized and mixed fully, 10 parts in 2 parts of spiral shell worm ethyl esters, 1 part of good fortune Lapie, 87 parts of kaolin and talcum obtain pulvis.
Formulation example 8
By being pulverized and mixed fully, 10 parts in 4 parts of spiral shell worm ethyl esters, 1 part of Validacin (Takeda), 85 parts of kaolin and talcum obtain pulvis.
Formulation example 9
With 5 parts of spiral shell worm ethyl esters, 10 parts of flutolanils, contain 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts white carbon (=white carbon: the mixture of polyoxyethylene alkyl ether sulfuric ester ammonium salt=1: 1 (weight ratio)) 30 parts, and 55 parts of mixing of water, utilize the case of wet attrition method to carry out Crushing of Ultrafine and obtain suspension.
Production Example 10
With 5 parts of spiral shell worm ethyl esters, 10 parts of Pencycurons, contain 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts white carbon (=white carbon: the mixture of polyoxyethylene alkyl ether sulfuric ester ammonium salt=1: 1 (weight ratio)) 30 parts, and 55 parts of mixing of water, utilize the case of wet attrition method to carry out Crushing of Ultrafine and obtain suspension.
Production Example 11
With 5 parts of spiral shell worm ethyl esters, 10 parts of good fortune Lapies, contain 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts white carbon (=white carbon: the mixture of polyoxyethylene alkyl ether sulfuric ester ammonium salt=1: 1 (weight ratio)) 30 parts, and 55 parts of mixing of water, utilize the case of wet attrition method to carry out Crushing of Ultrafine and obtain suspension.
Production Example 12
With 5 parts of spiral shell worm ethyl esters, 10 parts of Validacin (Takeda)s, contain 50 parts of polyoxyethylene alkyl ether sulfuric ester ammonium salts white carbon (=white carbon: the mixture of polyoxyethylene alkyl ether sulfuric ester ammonium salt=1: 1 (weight ratio)) 30 parts, and 55 parts of mixing of water, utilize the case of wet attrition method to carry out Crushing of Ultrafine and obtain suspension.
Next, utilize test example that effect of the present invention is shown.
Test example 1 (to the insecticidal activity test of brown planthopper)
Spiral shell worm ethyl ester substance with the method manufacturing that utilizes Japanese Unexamined Patent Application Publication 2000-516918 communique to put down in writing, flutolanil substance (with the pure medicine of light company system), Pencycuron substance (with the pure medicine of light company system) and each 10mg of good fortune Lapie substance (with the pure medicine of light company system) are dissolved in respectively among acetone (pure pharmaceutical worker already makes with the light) 1ml that contains SOLGEN TW-20 (the first industrial pharmacy system), then mode spreader (trade name: the DAIN (registration mark) that contains 0.02 capacity % to reach normal concentration, live chemical weapons rural area skill system) water diluted.The water diluent of spiral shell worm ethyl ester is mixed preparation test liquid with the water diluent of flutolanil, the water diluent of Pencycuron or good fortune Lapie's water diluent.
The paper pot of 2.5 leaf phases is planted rice, and (Oryza sativa, kind: the dream of star) above-mentioned test liquid 20ml is scattered in per 2 strains of seedling.After this rice seedling is air-dry, it is inserted in the glass developmental tube processed (diameter 30mm, high 200mm) of the water that is added with 4.8ml.In each this developmental tube, put 10 of 3 instar larvaes of brown planthopper in a suitable place to breed, place indoor (25 ℃, humidity 60%).The life and death of observing afterwards for the larva of examination in 6 days from putting beginning day beginning in a suitable place to breed.By this observed result, utilize formula 1) calculate dead worm rate, utilize formula 2) calculate the dead worm rate of proofreading and correct.It should be noted that test is carried out 2 times repeatedly.Its mean value is shown in table 1.
Formula 1): the dead borer population of dead worm rate (%)=treatment region/confession examination borer population * 100
Formula 2): the dead worm rate of revisal (%)={ (the dead worm rate of the treatment region-dead worm rate in non-processor district)/(the dead worm rate in 100-non-processor district) } * 100
Table 1
| Test compound | Concentration (notes)(ppm) | Proofread and correct dead worm rate (%) |
| Spiral shell worm ethyl ester | 0.4 | 60 |
| Spiral shell worm ethyl ester+flutolanil | 0.4+0.04 | 80 |
| Spiral shell worm ethyl ester+flutolanil | 0.4+0.4 | 90 |
| Spiral shell worm ethyl ester+flutolanil | 0.4+4 | 90 |
| Spiral shell worm ethyl ester+Pencycuron | 0.4+0.04 | 85 |
| Spiral shell worm ethyl ester+Pencycuron | 0.4+0.4 | 90 |
| Spiral shell worm ethyl ester+Pencycuron | 0.4+4 | 85 |
| Spiral shell worm ethyl ester+good fortune Lapie | 0.4+0.04 | 85 |
| Spiral shell worm ethyl ester+good fortune Lapie | 0.4+0.4 | 85 |
| Spiral shell worm ethyl ester+good fortune Lapie | 0.4+4 | 90 |
Concentration when (notes) test compound is 2 kinds is sequentially put down in writing according to the record of compound.
Industrial utilizability
But utilize composition efficient of preventing and kill off harmful arthropod of the present invention to prevent and kill off well harmful arthropod.
Claims (8)
1. composition of preventing and kill off harmful arthropod, it contains spiral shell worm ethyl ester and is selected from the compound of preventing and kill off banded sclerotial blight more than a kind of group A, wherein,
The group that group A is comprised of flutolanil, Pencycuron, good fortune Lapie and Validacin (Takeda).
2. the composition of preventing and kill off harmful arthropod according to claim 1, wherein, the compound of preventing and kill off banded sclerotial blight is flutolanil or good fortune Lapie.
3. the composition of preventing and kill off harmful arthropod according to claim 1 and 2, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of banded sclerotial blight.
4. method of preventing and kill off harmful arthropod, it comprises spiral shell worm ethyl ester and the compound of preventing and kill off banded sclerotial blight more than a kind that is selected from group A is applied to the operation on the cultivation ground of plant or plant with effective dose, wherein,
The group that group A is comprised of flutolanil, Pencycuron, good fortune Lapie and Validacin (Takeda).
5. the method for control according to claim 4, wherein, the compound of preventing and kill off banded sclerotial blight is flutolanil or good fortune Lapie.
6. according to claim 4 or 5 described the method for control, wherein, spiral shell worm ethyl ester is 10: 1～1: 100 with the weight ratio of preventing and kill off the compound of banded sclerotial blight.
7. according to claim 4 or 5 described the method for control, wherein, harmful arthropod is the insect that belongs to Delphacidae.
8. according to claim 4 or 5 described the method for control, harmful arthropod is brown planthopper, white-backed planthopper or small brown rice planthopper.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
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| JP2010-175201 | 2010-08-04 | ||
| JP2010175201A JP5720137B2 (en) | 2010-08-04 | 2010-08-04 | Harmful arthropod control composition and harmful arthropod control method |
| PCT/JP2011/067817 WO2012018060A1 (en) | 2010-08-04 | 2011-07-28 | Noxious arthropod control composition and noxious arthropod control method |
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| JP (1) | JP5720137B2 (en) |
| KR (1) | KR20130132764A (en) |
| CN (2) | CN104430437A (en) |
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| CN107484767A (en) * | 2017-08-14 | 2017-12-19 | 江苏龙灯化学有限公司 | A kind of oil-based suspension and its production and use |
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- 2011-07-28 CN CN201410612833.3A patent/CN104430437A/en active Pending
- 2011-07-28 KR KR1020137004962A patent/KR20130132764A/en not_active Application Discontinuation
- 2011-07-28 CN CN201180037868.3A patent/CN103052317B/en not_active Expired - Fee Related
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| KR20130132764A (en) | 2013-12-05 |
| CN103052317B (en) | 2014-12-03 |
| JP5720137B2 (en) | 2015-05-20 |
| WO2012018060A1 (en) | 2012-02-09 |
| CN104430437A (en) | 2015-03-25 |
| JP2012036105A (en) | 2012-02-23 |
| TW201210479A (en) | 2012-03-16 |
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