CN103018141B - High alloy low-carbon martensitic steels original grain developer and display packing - Google Patents
High alloy low-carbon martensitic steels original grain developer and display packing Download PDFInfo
- Publication number
- CN103018141B CN103018141B CN201210497718.7A CN201210497718A CN103018141B CN 103018141 B CN103018141 B CN 103018141B CN 201210497718 A CN201210497718 A CN 201210497718A CN 103018141 B CN103018141 B CN 103018141B
- Authority
- CN
- China
- Prior art keywords
- sample
- developer
- high alloy
- gram
- mass concentration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 229910000831 Steel Inorganic materials 0.000 title claims abstract description 23
- 239000010959 steel Substances 0.000 title claims abstract description 23
- 229910000734 martensite Inorganic materials 0.000 title claims abstract description 21
- 229910045601 alloy Inorganic materials 0.000 title claims abstract description 19
- 239000000956 alloy Substances 0.000 title claims abstract description 19
- 229910052799 carbon Inorganic materials 0.000 title claims abstract description 17
- 238000012856 packing Methods 0.000 title claims abstract description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 18
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- OXNIZHLAWKMVMX-UHFFFAOYSA-N picric acid Chemical compound OC1=C([N+]([O-])=O)C=C([N+]([O-])=O)C=C1[N+]([O-])=O OXNIZHLAWKMVMX-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000002360 preparation method Methods 0.000 claims abstract description 4
- 239000002904 solvent Substances 0.000 claims abstract description 3
- 238000005260 corrosion Methods 0.000 claims description 15
- 230000007797 corrosion Effects 0.000 claims description 14
- 229920000742 Cotton Polymers 0.000 claims description 10
- 238000001704 evaporation Methods 0.000 claims description 8
- 238000005498 polishing Methods 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 239000013078 crystal Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 230000003628 erosive effect Effects 0.000 claims description 4
- 239000011521 glass Substances 0.000 claims description 4
- 230000000007 visual effect Effects 0.000 claims description 4
- 238000004458 analytical method Methods 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 3
- 238000011156 evaluation Methods 0.000 claims description 3
- 230000003287 optical effect Effects 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 4
- 238000009472 formulation Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000005259 measurement Methods 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000005457 optimization Methods 0.000 abstract description 3
- 239000000243 solution Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 5
- 239000003518 caustics Substances 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 238000005530 etching Methods 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 244000137852 Petrea volubilis Species 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 229910001566 austenite Inorganic materials 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005070 sampling Methods 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 229910000677 High-carbon steel Inorganic materials 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- 229910000954 Medium-carbon steel Inorganic materials 0.000 description 1
- 238000005275 alloying Methods 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 238000005282 brightening Methods 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000005242 forging Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
Landscapes
- Investigating And Analyzing Materials By Characteristic Methods (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210497718.7A CN103018141B (en) | 2012-11-29 | 2012-11-29 | High alloy low-carbon martensitic steels original grain developer and display packing |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201210497718.7A CN103018141B (en) | 2012-11-29 | 2012-11-29 | High alloy low-carbon martensitic steels original grain developer and display packing |
Publications (2)
Publication Number | Publication Date |
---|---|
CN103018141A CN103018141A (en) | 2013-04-03 |
CN103018141B true CN103018141B (en) | 2015-11-18 |
Family
ID=47966995
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201210497718.7A Active CN103018141B (en) | 2012-11-29 | 2012-11-29 | High alloy low-carbon martensitic steels original grain developer and display packing |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN103018141B (en) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103454187B (en) * | 2013-08-27 | 2016-02-10 | 宁夏共享集团有限责任公司 | A kind of method of room temperature display tempering bainite tissue's original austenite grains border |
CN104374627A (en) * | 2014-11-19 | 2015-02-25 | 苏州华碧微科检测技术有限公司 | Corrosion liquid and corrosion method for ultralow steel original austenite crystal boundary |
CN104729963B (en) * | 2015-03-31 | 2017-08-08 | 常州天山重工机械有限公司 | A kind of detection display methods of the austenite crystal of room temperature lower gear quenched and tempered steel |
CN105136629B (en) * | 2015-08-24 | 2017-11-17 | 首钢总公司 | A kind of display methods of zinc-plated plate surface zinc crystal grain |
CN105352779A (en) * | 2015-10-21 | 2016-02-24 | 中国船舶重工集团公司第七二五研究所 | Metallographic erosion method of nickel-aluminum bronze crystal boundary |
CN105486567A (en) * | 2015-11-24 | 2016-04-13 | 太原理工大学 | Chemical erosion agent for displaying macrostructure of expansion alloy, and erosion method thereof |
CN105908186A (en) * | 2016-05-06 | 2016-08-31 | 江西昌河航空工业有限公司 | Stainless steel corrosive agent and stainless steel grain size display method |
CN106086906B (en) * | 2016-06-08 | 2019-02-12 | 中国船舶重工集团公司第七二五研究所 | It is a kind of for clearing up the cleaning agent of steel macrostructure hot acid corrosion product |
CN109001200A (en) * | 2018-06-15 | 2018-12-14 | 济南大学 | A kind of corrosive liquid and caustic solution of medium carbon steel original austenite crystal boundary |
CN109490302A (en) * | 2018-11-11 | 2019-03-19 | 上海电气上重铸锻有限公司 | A kind of test method of the austenite grain of midium-carbon steel martensitic structure |
CN112082912A (en) * | 2020-09-10 | 2020-12-15 | 中车戚墅堰机车车辆工艺研究所有限公司 | Steel grain size etching agent and application thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0613756B2 (en) * | 1988-11-24 | 1994-02-23 | 住友金属工業株式会社 | Ferrite grain boundary developing solution and etching method |
CN1401012A (en) * | 2000-02-28 | 2003-03-05 | 新日本制铁株式会社 | Steel pipe having excellent formability and method for production thereof |
CN101831653A (en) * | 2010-06-23 | 2010-09-15 | 天津市电力公司 | Martensite high-alloy heat resistant steel metallography detection polishing agent and application thereof |
CN102103051A (en) * | 2011-01-13 | 2011-06-22 | 马鞍山钢铁股份有限公司 | Medium-high carbon steel actual grain size developer and developing method |
CN102191431A (en) * | 2010-03-09 | 2011-09-21 | 株式会社神户制钢所 | Steel bar with excellent brittle crack spreading stopping performance and manufacturing method thereof |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2010141113A2 (en) * | 2009-02-13 | 2010-12-09 | Babcock & Wilcox Technical Services Y-12, Llc | Nano-material and method of fabrication |
-
2012
- 2012-11-29 CN CN201210497718.7A patent/CN103018141B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0613756B2 (en) * | 1988-11-24 | 1994-02-23 | 住友金属工業株式会社 | Ferrite grain boundary developing solution and etching method |
CN1401012A (en) * | 2000-02-28 | 2003-03-05 | 新日本制铁株式会社 | Steel pipe having excellent formability and method for production thereof |
CN102191431A (en) * | 2010-03-09 | 2011-09-21 | 株式会社神户制钢所 | Steel bar with excellent brittle crack spreading stopping performance and manufacturing method thereof |
CN101831653A (en) * | 2010-06-23 | 2010-09-15 | 天津市电力公司 | Martensite high-alloy heat resistant steel metallography detection polishing agent and application thereof |
CN102103051A (en) * | 2011-01-13 | 2011-06-22 | 马鞍山钢铁股份有限公司 | Medium-high carbon steel actual grain size developer and developing method |
Non-Patent Citations (2)
Title |
---|
《A Comparison of Etchants for Quantitative Metallography of Bainite and Martensite Microstructures in Fe-C-Mo Alloys》;C. K. SHUI et al.;《METALLOGRAPHY》;19881231;第21卷;第91-102页 * |
低合金钢奥氏体晶粒度显示方法的研究;郭泽尧;《金属材料与冶金工程》;20081031;全文 * |
Also Published As
Publication number | Publication date |
---|---|
CN103018141A (en) | 2013-04-03 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103018141B (en) | High alloy low-carbon martensitic steels original grain developer and display packing | |
CN102890027B (en) | Metallographic structure display method of interstitial free (IF) steel cold-rolled sheet containing titanium (Ti) | |
CN103792128B (en) | A kind of method of the biphase crystal boundary showing two phase stainless steel | |
CN107574439B (en) | Etching agent for displaying original austenite grain boundary of FB2 steel, preparation method and application | |
CN104562012A (en) | Iron-base high-temperature alloy sample metallographic etching solution and etching method | |
CN105018931A (en) | GH3030 high-temperature alloy as-cast metallographic etchant and preparing method and using method thereof | |
CN109187152B (en) | Corrosive agent for displaying heat-resistant steel original austenite grain boundary and display method | |
CN102383130B (en) | Observation method for metallographic structures of amorphous alloys | |
CN104513985A (en) | Nickel-chromium alloy metallographic corrosion solution and corrosion method | |
CN102590050B (en) | Method for displaying P91 and P92 steel original austenite grain boundaries | |
CN104878389A (en) | Pure-nickel metallographic etchant and corroding method using same | |
CN105002498A (en) | GH625 high-temperature alloy metallographic etchant and preparation and application method thereof | |
CN101825574B (en) | Solution and method for detecting ferrite pollution on surface of austenitic stainless steel | |
CN102103051A (en) | Medium-high carbon steel actual grain size developer and developing method | |
CN103993319A (en) | Corrosive agent and display method for macrostructure of aluminum and aluminum copper alloys | |
CN104977299B (en) | A kind of method for showing P91, P92 ferritic heat-resistant steel original austenite crystal prevention | |
CN101880881A (en) | High aluminum zinc alloy etching agent and use method thereof | |
CN105177577A (en) | Corrosion method for small-specification red copper rod | |
CN111979547A (en) | Metallographic corrosive agent for nickel-based alloy and use method thereof | |
CN110389129B (en) | Corrosive agent for displaying 690 nickel-based alloy deposited metal grain boundary and etching method thereof | |
CN107779941A (en) | Electrolytic polishing liquid, its preparation method and alloy electrolytic polishing method | |
CN109142010A (en) | A kind of method of retained austenite distribution and content in detection low-alloy structural steel | |
CN105738184B (en) | The application method for the etchant that manganese steel austenite grain boundary is shown | |
CN110749718A (en) | Dendritic crystal corrosive agent and corrosion method for maraging stainless steel | |
CN107643204B (en) | Cobalt-chromium alloy etching agent and method for obtaining metallographic structure by using same |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20201009 Address after: 244000 No.8 Chang'an Avenue, Zongyang Economic Development Zone, Tongling City, Anhui Province Patentee after: Anhui Huachi kinetic energy technology Co.,Ltd. Address before: Hebei Street West Harbor area, 066004 Hebei city of Qinhuangdao province No. 438 Patentee before: Yanshan University |
|
TR01 | Transfer of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Original grain display agent and display method of high alloy low carbon martensitic steel Effective date of registration: 20211229 Granted publication date: 20151118 Pledgee: Zongyang Financing Guarantee Co.,Ltd. Pledgor: Anhui Huachi kinetic energy technology Co.,Ltd. Registration number: Y2021980016707 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220607 Granted publication date: 20151118 Pledgee: Zongyang Financing Guarantee Co.,Ltd. Pledgor: Anhui Huachi kinetic energy technology Co.,Ltd. Registration number: Y2021980016707 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: High alloy low carbon martensitic steel original grain display agent and display method Effective date of registration: 20220914 Granted publication date: 20151118 Pledgee: Tongling Comprehensive Transportation Investment Group Co.,Ltd. Pledgor: Anhui Huachi kinetic energy technology Co.,Ltd. Registration number: Y2022980015111 |