CN103011529A - Industrial wastewater treatment technology - Google Patents
Industrial wastewater treatment technology Download PDFInfo
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- CN103011529A CN103011529A CN2012105954553A CN201210595455A CN103011529A CN 103011529 A CN103011529 A CN 103011529A CN 2012105954553 A CN2012105954553 A CN 2012105954553A CN 201210595455 A CN201210595455 A CN 201210595455A CN 103011529 A CN103011529 A CN 103011529A
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- waste water
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- water
- anoxic
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- 238000004065 wastewater treatment Methods 0.000 title claims abstract description 7
- 239000010842 industrial wastewater Substances 0.000 title abstract description 4
- 239000002351 wastewater Substances 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 238000000034 method Methods 0.000 claims abstract description 13
- 239000000126 substance Substances 0.000 claims abstract description 12
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 6
- 230000003647 oxidation Effects 0.000 claims abstract description 5
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 5
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 10
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical group CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 claims description 7
- BNBLBRISEAQIHU-UHFFFAOYSA-N disodium dioxido(dioxo)manganese Chemical compound [Na+].[Na+].[O-][Mn]([O-])(=O)=O BNBLBRISEAQIHU-UHFFFAOYSA-N 0.000 claims description 7
- 239000004743 Polypropylene Substances 0.000 claims description 5
- 125000000266 alpha-aminoacyl group Chemical group 0.000 claims description 5
- 238000003889 chemical engineering Methods 0.000 claims description 5
- 150000001875 compounds Chemical class 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 230000003311 flocculating effect Effects 0.000 claims description 5
- 230000007062 hydrolysis Effects 0.000 claims description 5
- 230000020477 pH reduction Effects 0.000 claims description 5
- -1 polypropylene Polymers 0.000 claims description 5
- 229920001155 polypropylene Polymers 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 4
- 239000003054 catalyst Substances 0.000 claims description 2
- 229910052759 nickel Inorganic materials 0.000 claims description 2
- 239000007800 oxidant agent Substances 0.000 claims description 2
- 239000010802 sludge Substances 0.000 claims description 2
- 238000009280 upflow anaerobic sludge blanket technology Methods 0.000 claims description 2
- 230000008901 benefit Effects 0.000 abstract description 3
- 239000007788 liquid Substances 0.000 abstract description 3
- 239000002699 waste material Substances 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 238000012423 maintenance Methods 0.000 abstract description 2
- 238000001728 nano-filtration Methods 0.000 abstract description 2
- 238000000108 ultra-filtration Methods 0.000 abstract description 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 230000015556 catabolic process Effects 0.000 abstract 1
- 238000006731 degradation reaction Methods 0.000 abstract 1
- 238000005189 flocculation Methods 0.000 abstract 1
- 230000016615 flocculation Effects 0.000 abstract 1
- 238000006479 redox reaction Methods 0.000 abstract 1
- 238000004062 sedimentation Methods 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 7
- 229910052698 phosphorus Inorganic materials 0.000 description 7
- 239000011574 phosphorus Substances 0.000 description 7
- XKMRRTOUMJRJIA-UHFFFAOYSA-N ammonia nh3 Chemical compound N.N XKMRRTOUMJRJIA-UHFFFAOYSA-N 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000010865 sewage Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 230000000050 nutritive effect Effects 0.000 description 2
- 239000002957 persistent organic pollutant Substances 0.000 description 2
- 238000007639 printing Methods 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 208000031320 Teratogenesis Diseases 0.000 description 1
- 150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000004630 mental health Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000002703 mutagenesis Methods 0.000 description 1
- 231100000350 mutagenesis Toxicity 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
Landscapes
- Separation Using Semi-Permeable Membranes (AREA)
- Purification Treatments By Anaerobic Or Anaerobic And Aerobic Bacteria Or Animals (AREA)
Abstract
本发明公开了一种化工工业废水处理工艺，包括氧化还原反应、缺氧水解反应、厌氧反应、好氧生物反应、超滤、纳滤、吸附。本发明是通过在废水中加入无机强氧化物进行预氧化处理，再生物处理，使废水依次经过厌氧、缺氧、好氧生物处理，再絮凝沉降，最后深度处理。本发明具有设备结构简单，便于操作和维修的特点，而且对处理后的水质可以反复循环利用，在彻底降解情况下，没有废液产生，同时使处理后的工业废水的COD值降到最低，具有良好的经济和环境效益。The invention discloses a chemical industry wastewater treatment process, which includes redox reaction, anoxic hydrolysis reaction, anaerobic reaction, aerobic biological reaction, ultrafiltration, nanofiltration and adsorption. In the present invention, pre-oxidation treatment and rebiological treatment are carried out by adding inorganic strong oxides into the waste water, so that the waste water undergoes anaerobic, anoxic and aerobic biological treatment in sequence, then flocculation and sedimentation, and finally advanced treatment. The invention has the characteristics of simple equipment structure, easy operation and maintenance, and the treated water can be recycled repeatedly. In the case of complete degradation, no waste liquid is produced, and the COD value of the treated industrial wastewater is reduced to the minimum. It has good economic and environmental benefits.
Description
Technical field
The present invention relates to a kind of chemical engineering industry waste water treatment process, specifically a kind of process for treating industrial waste water.
Background technology
In the factory of enterprise, mainly be distributed in the industries such as electronics, plastic cement, plating, five metals, printing, food, printing and dyeing.Though yet most of sewage that these factories produce are through just being discharged into after certain processing in the cultivation waters such as lake, reservoir, rivers, pond.But, still there are a lot of impurity to be difficult to process in the sewage after processing, for example: organic chloride comprises the chlorine-containing organic compounds such as chlorinated aliphatic hydrocarbon, chlorination aromatic hydrocarbon.The chemical property of organic chloride is relatively stable, easily accumulates in the organic matter of organism, soils and sediments, and in the occurring in nature degraded slowly, the environmental hazard cycle is long.Many organic chlorides are considered to have " carcinogenic, teratogenesis shape, mutagenesis " effect; The color of industrial sewage can not get weakening in addition, so not only can not reach the standard of national requirements, but also can produce secondary pollution to environment.They have a strong impact on existence, the growth of cultured fishes, affect output, the quality of fishery products, cause biological processing unit efficient obviously to descend, and also jeopardize people's physical and mental health
Summary of the invention
The purpose of this invention is to provide a kind of technique for treating industrial wastewater, for cooled trade effluent being reclaimed and utilizing saving water resource.The method carries out effectively removing synchronously to nutritive elements such as carbon containing organic pollutant and nitrogen, phosphorus, and the final outflow water chemical oxygen demand COD can reach below the 10mg/L, and ammonia nitrogen maintains below the 5mg/L, and total phosphorus maintains below the 0.5mg/L can be back to industrial production.
Technical scheme of the present invention:
A kind of chemical engineering industry waste water treatment process is characterized in that:
(1) pre-oxidation treatment: add inorganic strong oxide compound and carry out oxide treatment in waste water, the amount of adding is waste water 30～40kg per ton;
(2) acidication: the wastewater from chemical industry after the oxide treatment is placed the hydrolysis acidification pool acidifying that is hydrolyzed, and hydraulic detention time is 2.5～3.0 hours;
(3) biological treatment: waste water is processed through anaerobism, anoxic, aerobe successively;
(4) flocculating settling: add polymerize aluminum chloride and polypropylene aminoacyl and carry out mud-water separation;
(5) advanced treatment: the second pond water outlet is processed through entering the RO film after coarse filtration, the essence filter successively.
Described inorganic strong oxidizer is sodium chlorate, sodium manganate, Na2Fe04 and catalyst oxidation nickel, and the mass ratio of three kinds of strong oxidizers is: sodium chlorate 20～50%, sodium manganate 20～50%, Na2Fe04 20～50%.
Described anaerobic pond is UASB anaerobic sludge expansion pond.
Described Aerobic Pond is the value aerobic biofilter.
Effect of the present invention:
Can carry out effectively removing synchronously to nutritive elements such as carbon containing organic pollutant and nitrogen, phosphorus, the final outflow water chemical oxygen demand COD can reach below the 10mg/L, ammonia nitrogen maintains below the 5mg/L, total phosphorus maintains below the 0.5mg/L, can be back to industrial production, ultrafiltration, nanofiltration concentrated solution are cycled to repeat processing, and thoroughly degraded does not have waste liquid to produce.
Advantage of the present invention is:
(1) device structure is simple, the characteristics of convenient operation and maintenance;
(2) can reclaim and utilize trade effluent, the trade effluent after the processing can use as boiler feed water again;
(3) saving water resource in thorough degraded situation, does not have waste liquid to produce, and makes simultaneously the COD value of the trade effluent after the processing drop to minimum;
(4) has good economy and environment benefit.
Embodiment
Example 1
In waste water, add inorganic strong oxide compound (sodium chlorate 30%, sodium manganate 30%, Na2Fe04 20%) carries out oxide treatment, the amount that adds is waste water 30kg per ton, acidication: the wastewater from chemical industry after the oxide treatment is placed the hydrolysis acidification pool acidifying that is hydrolyzed, hydraulic detention time is 2.5 hours, biological treatment: make waste water pass through successively anaerobism, anoxic, aerobe is processed, flocculating settling: add polymerize aluminum chloride and polypropylene aminoacyl and carry out mud-water separation, advanced treatment: coarse filtration is passed through in the second pond water outlet successively, entering the RO film after the essence filter processes, the water outlet chemical oxygen demand COD can reach 8mg/L, and ammonia nitrogen maintains 3mg/L, and total phosphorus maintains 0.3mg/L.
Example 2
In waste water, add inorganic strong oxide compound (sodium chlorate 30%, sodium manganate 20%, Na2Fe04 50%) carries out oxide treatment, the amount that adds is waste water 35kg per ton, acidication: the wastewater from chemical industry after the oxide treatment is placed the hydrolysis acidification pool acidifying that is hydrolyzed, hydraulic detention time is 3.0 hours, biological treatment: make waste water pass through successively anaerobism, anoxic, aerobe is processed, flocculating settling: add polymerize aluminum chloride and polypropylene aminoacyl and carry out mud-water separation, advanced treatment: coarse filtration is passed through in the second pond water outlet successively, entering the RO film after the essence filter processes, the water outlet chemical oxygen demand COD can reach below the 5mg/L, ammonia nitrogen maintains 2mg/L, and total phosphorus maintains 0.1mg/L.
Example 3
In waste water, add inorganic strong oxide compound (sodium chlorate 40%, sodium manganate 40%, Na2Fe04 20%) carries out oxide treatment, the amount that adds is waste water 40kg per ton, acidication: the wastewater from chemical industry after the oxide treatment is placed the hydrolysis acidification pool acidifying that is hydrolyzed, hydraulic detention time is 3.0 hours, biological treatment: make waste water pass through successively anaerobism, anoxic, aerobe is processed, flocculating settling: add polymerize aluminum chloride and polypropylene aminoacyl and carry out mud-water separation, advanced treatment: coarse filtration is passed through in the second pond water outlet successively, entering the RO film after the essence filter processes, the water outlet chemical oxygen demand COD can reach 5mg/L, and ammonia nitrogen maintains 1mg/L, and total phosphorus maintains 0.2mg/L.
Claims (2)
1. chemical engineering industry waste water treatment process is characterized in that:
(1) pre-oxidation treatment: add inorganic strong oxide compound and carry out oxide treatment in waste water, the amount of adding is waste water 30～40kg per ton;
(2) acidication: the wastewater from chemical industry after the oxide treatment is placed the hydrolysis acidification pool acidifying that is hydrolyzed, and hydraulic detention time is 2.5～3.0 hours;
(3) biological treatment: waste water is processed through anaerobism, anoxic, aerobe successively;
(4) flocculating settling: add polymerize aluminum chloride and polypropylene aminoacyl and carry out mud-water separation;
(5) advanced treatment: the second pond water outlet is processed through entering the RO film after coarse filtration, the essence filter successively.
2. a kind of chemical engineering industry method of wastewater treatment according to claim 1, it is characterized in that: described inorganic strong oxidizer is sodium chlorate, sodium manganate, Na2Fe04 and catalyst oxidation nickel, the mass ratio of three kinds of strong oxidizers is: sodium chlorate 20～50%, sodium manganate 20～50%, Na2Fe04 20～50%; Described anaerobic pond is UASB anaerobic sludge expansion pond; Described Aerobic Pond is the value aerobic biofilter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105954553A CN103011529A (en) | 2012-12-07 | 2012-12-07 | Industrial wastewater treatment technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012105954553A CN103011529A (en) | 2012-12-07 | 2012-12-07 | Industrial wastewater treatment technology |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103011529A true CN103011529A (en) | 2013-04-03 |
Family
ID=47960707
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012105954553A Pending CN103011529A (en) | 2012-12-07 | 2012-12-07 | Industrial wastewater treatment technology |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103011529A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103395934A (en) * | 2013-08-02 | 2013-11-20 | 江苏和顺环保股份有限公司 | Processing apparatus for machine solvent wastewater and wastewater containing organic solvent |
| CN104291522A (en) * | 2014-09-16 | 2015-01-21 | 天津千鑫有色金属制品有限公司 | Method for treating industrial wastewater |
| CN104944709A (en) * | 2015-07-01 | 2015-09-30 | 郭景奎 | Electroplating wastewater zero-discharge treatment method and system |
| CN105366876A (en) * | 2015-09-25 | 2016-03-02 | 张荣斌 | Urban industrial sewage treatment system |
| CN117720226A (en) * | 2023-12-18 | 2024-03-19 | 山西大学 | A new low-carbon and near-zero emission process for industrial wastewater |
Citations (6)
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|---|---|---|---|---|
| WO2003093178A1 (en) * | 2002-04-30 | 2003-11-13 | International Waste Management Systems Plc | Organic slurry treatment process |
| CN1762843A (en) * | 2004-10-20 | 2006-04-26 | 哈尔滨工业大学 | Pollution removing composite medicament for water disposal |
| CN201990576U (en) * | 2011-01-27 | 2011-09-28 | 上海彰华膜净化有限公司 | A printing and dyeing wastewater treatment system |
| CN102464401A (en) * | 2011-10-20 | 2012-05-23 | 常州亚环环保科技有限公司 | COD (chemical oxygen demand) degradation agent for removing formaldehyde in industrial wastewater |
| CN102583879A (en) * | 2012-01-16 | 2012-07-18 | 宁波工程学院 | High-concentration integrated chemical organic wastewater treatment process |
| CN102659280A (en) * | 2012-04-20 | 2012-09-12 | 南京理工大学常熟研究院有限公司 | Effective printing and dyeing sewage treatment method |
-
2012
- 2012-12-07 CN CN2012105954553A patent/CN103011529A/en active Pending
Patent Citations (6)
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| WO2003093178A1 (en) * | 2002-04-30 | 2003-11-13 | International Waste Management Systems Plc | Organic slurry treatment process |
| CN1762843A (en) * | 2004-10-20 | 2006-04-26 | 哈尔滨工业大学 | Pollution removing composite medicament for water disposal |
| CN201990576U (en) * | 2011-01-27 | 2011-09-28 | 上海彰华膜净化有限公司 | A printing and dyeing wastewater treatment system |
| CN102464401A (en) * | 2011-10-20 | 2012-05-23 | 常州亚环环保科技有限公司 | COD (chemical oxygen demand) degradation agent for removing formaldehyde in industrial wastewater |
| CN102583879A (en) * | 2012-01-16 | 2012-07-18 | 宁波工程学院 | High-concentration integrated chemical organic wastewater treatment process |
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Non-Patent Citations (2)
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| 王申等: "水解酸化+A2O工艺处理混合化工废水运行中的问题与对策", 《水处理技术》 * |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103395934A (en) * | 2013-08-02 | 2013-11-20 | 江苏和顺环保股份有限公司 | Processing apparatus for machine solvent wastewater and wastewater containing organic solvent |
| CN104291522A (en) * | 2014-09-16 | 2015-01-21 | 天津千鑫有色金属制品有限公司 | Method for treating industrial wastewater |
| CN104944709A (en) * | 2015-07-01 | 2015-09-30 | 郭景奎 | Electroplating wastewater zero-discharge treatment method and system |
| CN105366876A (en) * | 2015-09-25 | 2016-03-02 | 张荣斌 | Urban industrial sewage treatment system |
| CN105366876B (en) * | 2015-09-25 | 2017-12-01 | 东营国安化工有限公司 | Urban industry sewage disposal system |
| CN117720226A (en) * | 2023-12-18 | 2024-03-19 | 山西大学 | A new low-carbon and near-zero emission process for industrial wastewater |
| US12358823B2 (en) | 2023-12-18 | 2025-07-15 | Shanxi University | Low-carbon near zero emission process of industrial waste water |
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Application publication date: 20130403 |