CN103007561A - Concentration production technology for glucose liquid - Google Patents

Concentration production technology for glucose liquid Download PDF

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Publication number
CN103007561A
CN103007561A CN2012105473695A CN201210547369A CN103007561A CN 103007561 A CN103007561 A CN 103007561A CN 2012105473695 A CN2012105473695 A CN 2012105473695A CN 201210547369 A CN201210547369 A CN 201210547369A CN 103007561 A CN103007561 A CN 103007561A
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concentration
glucose feed
effect evaporator
glucose
mvr
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CN103007561B (en
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王棣
张健
李伟
王岩
唐海静
张全刚
杨如玉
马森
王茜
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XIWANG PHARMACEUTICAL CO Ltd
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XIWANG PHARMACEUTICAL CO Ltd
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Abstract

A concentration production technology for glucose liquid comprises the following steps: heating glucose liquid in a plate heat exchanger; evaporating the heated liquid in an MVR (mechanical vapor recompression) evaporating unit; and evaporating the liquid in a triple-effect evaporator to obtain 70-75 % of liquid. Heat required by the triple-effect evaporator used in the technology is compression heat of flash evaporation waste gas. According to the technology, one-step glucose liquid concentration treatment in the prior art is changed into staged evaporation treatment; the MVR evaporating unit and the triple-effect evaporator are respectively used in two stages of treatment; and the heat source of the triple-effect evaporator is flash evaporation waste gas produced in other procedures, so as to realize zero consumption of live steam in the stage. Through implementation of the technology, the quality of crystallized glucose products is improved, the technology has the advantages of high efficiency, low consumption, energy conservation and environmental friendliness, and a zinc gluconate product produced through the technology has high concentration and meets the current national requirements on energy conservation and environmental protection of enterprises.

Description

A kind of glucose feed liquid concentrates production technology
Technical field
The present invention relates to the glucose production technical field, especially relate to a kind of for realizing the production technology that the glucose feed liquid is concentrated by evaporimeter.
Background technology
In engineering of producing crystalline dextrose, need to be that to be evaporated to concentration be to carry out crystallization with evaporimeter again behind the 70%-75% for the liquid glucose of 30-35% with concentration, in production process in the past, generally use general evaporimeter it is carried out evaporation and concentration, one ton of water of the every evaporation of this kind technology need consume the steam of 0.25-0.35 ton, and the waste gas that produces directly is cooled to the solidifying water of vapour, can not reasonably utilize its waste heat, when having increased single ton of sugared production cost, also cause resource waste extremely, do not met very much current national to the requirement of industry energy conservation environmental protection.
Summary of the invention
The object of the invention is to overcome the defective that exists in the prior art, provide a kind of glucose feed liquid to concentrate production technology, this production technology by evaporation mode stage by stage with the thermal balance of the whole production line of rational allocation, realized that zero gives birth to steam consumption, reached energy-saving and cost-reducing purpose, the technical scheme that adopts is: a kind of glucose feed liquid concentrates production technology, and it is characterized in that: described production technology may further comprise the steps:
1) when reaching 50%, the liquid level of glucose feed liquid in the storage tank before the evaporation opens feed pump, by feed pump the glucose feed pump being delivered to plate type heat exchanger heats, the glucose feed pump is delivered in the material balance tank after the heating, and the plate type heat exchanger drop temperature is 75 ℃;
2) open feed pump when above when material in the material balance tank reaches 30%, glucose feed pump in the material balance tank is delivered to the vaporization chamber of MVR evaporation unit and started simultaneously MVR evaporation unit carry out evaporation process;
3) the glucose feed liquid after MVR evaporation unit is processed enters into MVR and processes rear storage tank, open feed pump when storage tank reaches 50% after MVR processes, the glucose feed liquid is pumped into triple effect evaporator, open simultaneously the feed back valve, close discharge valve, make the rear glucose feed liquid of processing at first be back to MVR and process rear storage tank;
4) observe the growth of triple effect evaporator DC density, slowly adjust triple effect evaporator FC output concentration, after exporting concentration and reaching requirement concentration, discharge valve is opened simultaneously closing volume valve, make the glucose feed liquid after the processing enter next workshop section;
5) be in stable state and output concentration when having reached requirement concentration when the glucose feed liquid, each triple effect evaporation circulating pump FC series connection of triple effect evaporator PC, it is auto state that triple effect evaporator DC is set.
Technical scheme of the present invention also has: the flash distillation waste gas compression that the liquefaction operation produces in will producing heats up, and regenerates thermal source, and this thermal source is passed in the triple effect evaporator.
Technical scheme of the present invention also has: the concentration of glucose feed liquid is 30-35% in the front storage tank of the described evaporation of step 1), and the glucose feed concentration after the described MVR evaporation of step 3) unit is processed is 55-60%, and the concentration of output described in the step 5) is 70-75%.
Beneficial effect of the present invention is: this process modification the concentrated production technology of grape sugar feed liquid, one step completed glucose feed liquid concentration in the prior art has been become stage by stage evaporation treatment process, MVR evaporation unit and triple effect evaporator have been used respectively in two phase process, and the thermal source that uses in triple effect evaporator derives from the flash distillation waste gas that produces in other operation, thereby has realized and should the stage zero give birth to steam consumption.The enforcement of this technique has not only improved the quality of crystallization glucose product, and has the advantage of efficient, low consumption, energy-conservation and environmental protection, and the zinc gluconate product design by this explained hereafter is high and meet the current requirement to the industry energy conservation environmental protection of country.
Description of drawings
Accompanying drawing 1 is process chart of the present invention.
The specific embodiment
Below in conjunction with accompanying drawing, the present invention is specifically described.The invention discloses the concentrated production technology of a kind of glucose feed liquid, this production technology may further comprise the steps:
1) when reaching 50%, the liquid level of glucose feed liquid in the storage tank before the evaporation opens feed pump, the concentration of glucose feed liquid is 30-35% in the front storage tank of evaporation, by feed pump the glucose feed pump being delivered to plate type heat exchanger heats, the glucose feed pump is delivered in the material balance tank after the heating, and the plate type heat exchanger drop temperature is 75 ℃;
2) when reaching 30%, material in the material balance tank opens feed pump when above, glucose feed pump in the material balance tank delivered to the vaporization chamber of MVR evaporation unit and start simultaneously MVR evaporation unit carry out evaporation process, the glucose feed concentration after MVR evaporation unit is processed is 55-60%;
3) the glucose feed liquid after MVR evaporation unit is processed enters into MVR and processes rear storage tank, open feed pump when storage tank reaches 50% after MVR processes, the glucose feed liquid is pumped into triple effect evaporator, open simultaneously the feed back valve, close discharge valve, make the rear glucose feed liquid of processing at first be back to MVR and process rear storage tank;
4) growth of observation triple effect evaporator DC density, slowly adjust triple effect evaporator FC output concentration, after exporting concentration and reaching requirement concentration, discharge valve is opened simultaneously closing volume valve, make the glucose feed liquid after the processing enter next workshop section, this glucose feed liquid output concentration is 70-75%;
5) be in stable state and output concentration when having reached requirement concentration when the glucose feed liquid, each triple effect evaporation circulating pump FC series connection of triple effect evaporator PC, it is auto state that triple effect evaporator DC is set.
Wherein, the MVR evaporimeter is different from common single-action falling liquid film or multiple-effect falling film evaporimeter, MVR is the monomer evaporimeter, integrate the multiple-effect falling film evaporimeter, take the segmented evaporation according to required product concentration difference, when to be product can not reach desired concn after for the first time through the effect body, product vavuum pump by effect body bottom after leaving the effect body was extracted into effect body top again by the effect body with product by effect external body pipeline, then by this repeatedly by the effect body to reach desired concn.
In the MVR evaporator system, under certain pressure, utilize fixed gas (during the beginning preheating) and water vapour (during start vaporizer) in the vapour compression machine heat exchanger to compress, thereby produce steam, discharge simultaneously heat energy.The indirect steam that produces is after mechanical type heat energy compressor (being similar to air blast) effect, and in evaporator system the heat of the indirect steam that produces of recycling repeatedly, make 5~20 ℃ of intrasystem temperature increase, heat can continuous several times be utilized, live steam only is used for the supplemental heat loss and replenishes the input and output material heat content, significantly lowers evaporimeter to the consumption of external live steam.Improve the thermal efficiency, reduced energy consumption, avoided using external steam (main operating expenses of this steam recompression formula energy-saving evaporator only is the electric energy of drive compression machine).Because electric energy is clean energy resource, therefore, the MVR evaporimeter has really reached the discharging of " zero " pollution, has not namely had the requirement of CO2 emission fully.
Required thermal source comes from the flash distillation waste gas that the liquefaction operation produces in the glucose production in the triple effect evaporator, will change the compression of flash distillation waste gas and heat up, and regenerates thermal source, and this thermal source is passed in the triple effect evaporator.
Certainly, above-mentioned explanation is not limitation of the present invention, and the present invention also is not limited only to above-mentioned giving an example, and the variation that those skilled in the art make in essential scope of the present invention, remodeling, interpolation or replacement also belong to protection scope of the present invention.

Claims (3)

1. a glucose feed liquid concentrates production technology, and it is characterized in that: described production technology may further comprise the steps:
1) when reaching 50%, the liquid level of glucose feed liquid in the storage tank before the evaporation opens feed pump, by feed pump the glucose feed pump being delivered to plate type heat exchanger heats, the glucose feed pump is delivered in the material balance tank after the heating, and the plate type heat exchanger drop temperature is 75 ℃;
2) open feed pump when above when material in the material balance tank reaches 30%, glucose feed pump in the material balance tank is delivered to the vaporization chamber of MVR evaporation unit and started simultaneously MVR evaporation unit carry out evaporation process;
3) the glucose feed liquid after MVR evaporation unit is processed enters into MVR and processes rear storage tank, open feed pump when storage tank reaches 50% after MVR processes, the glucose feed liquid is pumped into triple effect evaporator, open simultaneously the feed back valve, close discharge valve, make the rear glucose feed liquid of processing at first be back to MVR and process rear storage tank;
4) observe the growth of triple effect evaporator DC density, slowly adjust triple effect evaporator FC output concentration, after exporting concentration and reaching requirement concentration, discharge valve is opened simultaneously closing volume valve, make the glucose feed liquid after the processing enter next workshop section;
5) be in stable state and output concentration when having reached requirement concentration when the glucose feed liquid, each triple effect evaporation circulating pump FC series connection of triple effect evaporator PC, it is auto state that triple effect evaporator DC is set.
2. according to the concentrated production technology of glucose feed liquid claimed in claim 1, it is characterized in that: the flash distillation waste gas compression that the liquefaction operation produces in will producing heats up, and regenerates thermal source, and this thermal source is passed in the triple effect evaporator.
3. according to claim 1 or the concentrated production technology of 2 described glucose feed liquids, it is characterized in that: the concentration of glucose feed liquid is 30-35% in the front storage tank of the described evaporation of step 1), glucose feed concentration after the described MVR evaporation of step 3) unit is processed is 55-60%, and the concentration of output described in the step 5) is 70-75%.
CN201210547369.5A 2012-12-17 2012-12-17 Concentration production technology for glucose liquid Active CN103007561B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103537104A (en) * 2013-10-25 2014-01-29 昆山市盛兴设备安装有限公司 Fructose-glucose syrup evaporating system
CN109022625A (en) * 2018-09-18 2018-12-18 上海立足生物科技有限公司 A method of producing the D-Psicose of concentration
CN112843761A (en) * 2021-03-10 2021-05-28 郑州博大浓缩干燥设备有限公司 Lees protein production fodder is with lees filter liquor evaporation concentration system

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103537104A (en) * 2013-10-25 2014-01-29 昆山市盛兴设备安装有限公司 Fructose-glucose syrup evaporating system
CN109022625A (en) * 2018-09-18 2018-12-18 上海立足生物科技有限公司 A method of producing the D-Psicose of concentration
CN112843761A (en) * 2021-03-10 2021-05-28 郑州博大浓缩干燥设备有限公司 Lees protein production fodder is with lees filter liquor evaporation concentration system

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Inventor after: Wang Dai

Inventor after: Zhang Xiaojie

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Inventor after: Wang Yan

Inventor after: Wang Qian

Inventor after: Xie Dengyu

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Denomination of invention: A concentration production process of grape sugar liquid

Effective date of registration: 20211224

Granted publication date: 20140917

Pledgee: Agricultural Development Bank of China Zouping sub branch

Pledgor: XIWANG PHARMACEUTICAL Co.,Ltd.

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Denomination of invention: A process for concentrating glucose feed solution

Effective date of registration: 20221027

Granted publication date: 20140917

Pledgee: Agricultural Development Bank of China Zouping sub branch

Pledgor: XIWANG PHARMACEUTICAL Co.,Ltd.

Registration number: Y2022980019930