CN102980837A - Device and measuring method for hydrocarbon diffusion coefficient in rocks under high temperature and high pressure - Google Patents
Device and measuring method for hydrocarbon diffusion coefficient in rocks under high temperature and high pressure Download PDFInfo
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- CN102980837A CN102980837A CN2012104658957A CN201210465895A CN102980837A CN 102980837 A CN102980837 A CN 102980837A CN 2012104658957 A CN2012104658957 A CN 2012104658957A CN 201210465895 A CN201210465895 A CN 201210465895A CN 102980837 A CN102980837 A CN 102980837A
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Claims (8)
- Under the high-temperature and high-pressure conditions in the rock hydro carbons coefficient of diffusion measure and use experimental facilities, it is characterized in that this equipment comprises rock diffusion coefficient analyzer, vacuum pump, confined pressure force (forcing) pump, hydro carbons source of the gas, N 2Source of the gas, left piston container, right piston container, Self-pressurizing agri pump, chromatogram detector, computing machine, drying unit and rock saturation water device;Described rock diffusion coefficient analyzer comprises constant temperature oven, core holding unit and temperature controller;Described core holding unit is positioned at described constant temperature oven, is used for placing sample, and is separated into left diffuser casing and right diffuser casing by sample;Described temperature controller is connected with described constant temperature oven;Described confined pressure force (forcing) pump is connected with described core holding unit;Described chromatogram detector is connected with described right diffuser casing with described left diffuser casing respectively by pipeline, and the pipeline that described left diffuser casing is connected with the chromatogram detector is provided with left sample valve, and the pipeline that described right diffuser casing is connected with the chromatogram detector is provided with right sample valve;Described computing machine is connected with described chromatogram detector;Described vacuum pump links to each other with two ends, the described rock diffusion coefficient analyzer left and right sides respectively by pipeline, is provided with the vacuum pump operation valve at described pipeline;Described left piston container and described right piston container dimensional size be connected identically, the two-piston container includes piston, liquid pressurized cylinder and cylinder;The cylinder of described left piston container is connected with described left diffuser casing by pipeline, is provided with left piston container operation valve and left diffuser casing operation valve at described pipeline; The cylinder of described right piston container is connected with right diffuser casing by pipeline, is provided with right piston container operation valve and right loose chamber operation valve at described pipeline;Described hydro carbons source of the gas is connected by the side of pipeline with the cylinder of described left piston container, is provided with left air source control valve at described pipeline; Described N 2Source of the gas is connected by the side of pipeline with the cylinder of described right piston container, is provided with right air source control valve at described pipeline;Described Self-pressurizing agri pump is connected with the liquid pressurized cylinder of described right piston container with described left piston container respectively by pipeline.
- 2. hydro carbons coefficient of diffusion assay method in the rock under the high-temperature and high-pressure conditions, it may further comprise the steps:A. rock sample being made diameter is that 2.5cm, length are the small cylinder of 0.5-0.6cm, and sample is carried out conventional factor of porosity, permeability detection;B. described sample is put into drying unit, more than the oven dry 8h, until constant weight;C. actual formation water data is prepared the simulated formation aqueous solution per sample, and abundant saturated local water until overflow without bubble, took out the fully sample of saturation water more than 8 hours to utilize rock saturation water device to vacuumize then to sample;D. the saturation water sample is put into the core holding unit of rock diffusion coefficient analyzer, utilized the confined pressure under the confined pressure force (forcing) pump simulation stratum condition that loading is set to core holding unit;E. utilize pipeline that vacuum pump links to each other with right piston container to left diffuser casing, right diffuser casing, its two ends and left piston container, with and two ends vacuumize with the pipeline that the chromatogram detector is connected, close successively left diffuser casing operation valve, right diffuser casing operation valve, left piston container operation valve, right piston container operation valve, left sample valve, right sample valve, vacuum pump operation valve after complete;F. utilize leak detection liquid that vacuum leak hunting is carried out in pipeline junction and each valve, the discovery seepage is in time tightened and is repeatedly hunted leak and guarantee that there is not seepage in pipeline;G. the actual ground temperature data of sampling horizon per sample is set as actual ground temperature with the temperature controller of rock diffusion coefficient analyzer, as experimental temperature;H. when the pipeline of rock diffusion coefficient analyzer and valve do not leak gas, open respectively left air source control valve, right air source control valve, left piston container operation valve, right piston container operation valve, utilize hydro carbons source of the gas, N 2Source of the gas fills respectively quantitative hydro carbons and N to left piston container, right piston container 2Serve as balanced gas, start the Self-pressurizing agri pump, set experiment and carry out required final gas injection equalized pressure and constant supercharging flow velocity, by the Self-pressurizing agri pump to the left piston container, the liquid pressurized cylinder constant speed of right piston container is injected the supercharging of pressurized liquid pushing piston pressure gas, when the cylinder of final left piston container and right piston container reaches the gas injection equalized pressure of setting, the Self-pressurizing agri pump stops supercharging, with this as the experiment zero hour, then close left piston container operation valve, right piston container operation valve, left diffuser casing operation valve, right diffuser casing operation valve is at identical gas injection equalized pressure bottom left diffuser casing, only there is concentration gradient in gas and does not exist the gas of pressure gradient to spread in the right diffuser casing;I. opened left sample valve, right sample valve after the experiment beginning made respectively the gas of a small amount of left diffuser casing, right diffuser casing send into the chromatogram detector to measure and record hydro carbons and N in the left diffuser casing every 0.5-2 hour 2Concentration, right diffuser casing in hydro carbons and N 2Concentration, utilize Computer Storage and record the gas concentration data of each two diffuser casings;J. ought be checked through hydro carbons concentration reduction in the left diffuser casing, the increase of hydro carbons concentration can judge that then hydrocarbon gas diffuses into right diffuser casing by sample from left diffuser casing in the right diffuser casing, and with these data as the 1st group of left diffuser casing, right diffuser casing hydro carbons concentration change data, then above left diffuser casings of 8 groups of continuous recordings, after the right diffuser casing hydro carbons concentration change data, experiment finishes, close left piston container operation valve, right piston container operation valve, and left diffuser casing operation valve, right diffuser casing operation valve, left sample valve, right sample valves etc. take out sample from core holding unit;All raw data of K. computer recording being preserved are brought Fick's second law into, utilize following formula to calculate hydro carbons coefficient of diffusion in the High Temperature High Pressure rock:D=ln(ΔC 0/ΔC i)/[E(t i-t 0)],E=A (1/V wherein 1+ 1/V 2)/L, t 0Be initial time, t iBe the i moment, Δ C iBe i moment hydro carbons concentration difference in two diffuser casings, Δ C 0Be initial time hydro carbons concentration difference in two diffuser casings, A is the sectional area of rock sample, and L is the length of rock sample, V 1, V 2Be respectively the volume of left diffuser casing, right diffuser casing, analyze the relation between itself and gas injection equalized pressure, the experimental temperature.
- 3. method as claimed in claim 2, wherein, described rock sample is mud shale, sandstone or gypsum-salt rock.
- 4. method as claimed in claim 2, wherein, in step D, described confined pressure is 3-50MPa.
- 5. method as claimed in claim 2, wherein, in step G, described actual ground temperature is palaeogeothermal or ground temperature now, described experimental temperature is room temperature-150 ℃.
- 6. method as claimed in claim 2, wherein, in step H, described gas injection equalized pressure is 0.2-10MPa; Described constant supercharging flow velocity is 0.5mL/min-20mL/min.
- 7. method as claimed in claim 2, wherein, in step H, described gas injection equalized pressure is 3MPa; Described constant supercharging flow velocity is 5mL/min.
- 8. such as each described method of claim 2-7, it also comprises according to described steps A-K a plurality of samples is detected, calculate respectively hydro carbons coefficient of diffusion in their the High Temperature High Pressure rock, analyze respectively the relation between itself and gas injection equalized pressure, the experimental temperature.
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