CN102978035A - Nutritional nano-loess transparent soap and preparation method thereof - Google Patents

Nutritional nano-loess transparent soap and preparation method thereof Download PDF

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Publication number
CN102978035A
CN102978035A CN 201110259900 CN201110259900A CN102978035A CN 102978035 A CN102978035 A CN 102978035A CN 201110259900 CN201110259900 CN 201110259900 CN 201110259900 A CN201110259900 A CN 201110259900A CN 102978035 A CN102978035 A CN 102978035A
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parts
loess
nano
sodium
tensio
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CN 201110259900
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赵殿栋
朱国华
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Yancheng City Huzheng Nano Material Science & Technology Co Ltd
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Yancheng City Huzheng Nano Material Science & Technology Co Ltd
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Priority to CN 201110259900 priority Critical patent/CN102978035A/en
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Abstract

The invention relates to a skin-care and washing product, and specifically relates to a nutritional nano-loess transparent soap and a preparation method thereof. The nutritional nano-loess transparent soap comprises a modified nano-loess solution, a surfactant and a cellulose thickening amendment and is prepared according to the following weight parts: 5-15 parts of glycerol, 5-10 parts of propylene glycol, 10-25 parts of sodium palmitoleate, 8-12 parts of sodium cocoate, 5-12 parts of sodium stearate, 10-20 parts of sodium myristate, 8-15 parts of stearic acid, 2-6 parts of EDTA-4Na, 1-6 parts of the modified nano-loess solution, 10.5-26.5 parts of a mixed soluble surfactant, 6-18 parts of the cellulose thickening amendment and 1-5 parts of essence. The soap has pure quality, mild property, rich and meticulous foam and strong decontamination capability, has the function of antisepsis and anti-inflammation, and has very good nutrition and protection effects for human skins.

Description

A kind of nutrition nano-loess transparent toilet soap and preparation method thereof
Technical field
What the present invention relates to is the skin care articles for washing, is specially a kind of nutrition nano-loess transparent toilet soap and preparation method thereof.
Background technology
Perfumed soap is a kind of traditional articles for washing, also is the necessary articles for use of life that consumers in general almost will use every day, and its quality and quality and human consumer's quality of life quality is closely bound up.Detergent industry has become trend to superior, functionalization development both at home and abroad.The production of nutrition nano-loess perfumed soap, crucial preparation and application at functional ingredient, many high-quality animals and plants elite are extracted and prepared and use all needs high-tech means, crucial in soapmaking process also some science and technology.Its security of the employed functional ingredient of perfumed soap and environment-friendly type require stricter, the continuous increase of realizing along with health of people at present.And this kind perfumed soap possesses very large price advantage with respect to high-grade cosmetics, also use when taking a shower of human consumer with good conditionsi.Loess is a kind of pure natural substance, is wherein comprising a lot of nutritional mineral matter, and it not only can cut off electromagnetic radiation, can also be releasing far infrared, have the effect of particularly preferred nutrition skin.
Summary of the invention
The object of the present invention is to provide a kind of nutritive ingredient of using to be nutrition nano-loess transparent toilet soap of nano-loess and preparation method thereof, thereby prepare a kind of transparent nano loess perfumed soap with effects such as nutrition skin-protection, releasing far infrared and negative ions.
Technical scheme of the present invention is: a kind of nutrition nano-loess transparent toilet soap comprises modification, tensio-active agent and the Mierocrystalline cellulose thickening agent of nano-loess solution, and presses following parts by weight preparation:
5~15 parts of glycerine; 5~10 parts of propylene glycol; 10~25 parts in Zoomeric acid sodium; 8~12 parts in cocinic acid sodium; 5~12 parts of sodium stearate; 10~20 parts of Sodium tetradecanoates; 8~15 parts of stearic acid; EDTA-4Na2~6 part; 1~6 part of modified Nano loess solution; 6~18 parts of compatibility tensio-active agent 10.5~26.5, Mierocrystalline cellulose thickening agents; 1~5 part in essence;
The method of modifying of described modified Nano loess solution is: the effective concentration of nano-loess is in the former nano-loess solution: 35%.Method of modifying is: get 60~100 parts of the nano-loess solution of 35% effective constituent in container, low whipping speed is in 600~800 rev/mins the situation, add 8~12 parts of dehydrated alcohols, stir after 10 minutes, add 8~12 parts of buffer reagents, under same stirring velocity, stir after 8~12 minutes, with 2.5 times of deionized water dilutions (namely diluting with 2.5 times deionized water), stirring velocity is reduced to 200~400 rev/mins, stir and got final product in 10~20 minutes;
A kind of nutrition nano-loess transparent toilet soap preparation method, preparation process is:
1) modification of nano-loess solution: by above-mentioned method of modifying, prepare modified Nano loess solution, stand-by;
2) preparation of compatibility tensio-active agent: take by weighing tea saponin, dehydrated alcohol, deionized water by said components, and prepare as stated above the compatibility tensio-active agent, stand-by;
3) allotment of perfumed soap composition: according to the method described above, take by weighing 5~15 parts of glycerine; 5~10 parts of propylene glycol; 10~25 parts in Zoomeric acid sodium; 8~12 parts in cocinic acid sodium; 5~12 parts of sodium stearate; 10~20 parts of Sodium tetradecanoates; 8~15 parts of stearic acid; EDTA-4Na2~6 part; 1~6 part of modified Nano loess solution; 10.5~26.5 parts in compatibility tensio-active agent; 6~18 parts of Mierocrystalline cellulose thickening agents; 1~5 part in essence.Preparation method: in container, low whipping speed is in 200~400 rev/mins the situation, add successively glycerine, propylene glycol, Zoomeric acid sodium, cocinic acid sodium, sodium stearate, Sodium tetradecanoate, EDTA-4Na, stearic acid etc., be warming up to gradually 70 ℃, add the compatibility tensio-active agent after stirring, dissolving.Then add thickening material under the constant temperature, mix, after about 40 minutes, be cooled to gradually 35 ℃, add essence, nano-loess solution and deionized water, rear cooling stirs.In whipping process, spray a small amount of defoamer, can enter film after stirring;
4) moulding of perfumed soap: before perfumed soap enters film, mould should be cleaned up, the a small amount of defoamer of rear sprinkling to be dried, then the perfumed soap that melts is slowly poured in the mould, with the bubble on defoamer cancellation surface, room temperature cooling or acceleration cooling in refrigerator, after band cools off fully, perfumed soap is deviate from from mould, with the preservative film parcel, be into soap.
Implement the present invention and have following beneficial effect:
1, nutrition transparent toilet soap of the present invention allocates forming take other plant oil such as glycerine, palmitinic acids as basic raw material in the situation of stirring at low speed, and preparation is simple for this, and cost is lower, and the blending technology that is suitable for suitability for industrialized production is provided for transparent toilet soap.The perfumed soap of preparing not only quality is pure, and character is gentle, and foam is careful abundant, and the dirty ability of dispelling is strong, also has nutrition skin, emitting far-infrared effect, to promoting cutaneous circulation, strengthening the epidermic cell activity and have good effect.
2, nano-loess has adsorption, and the adsorbable cutin of skin and the refuse in the skin pore of dispelling plays the effect that cleans skin, makes skin delicate, smooth, play to the skin toxin expelling, and sterilization and oxidation resistant effect, recovery is full of the skin of elastic force gloss.
3, nano-loess contains the multiple nutrients mineral substance, after these nutritional mineral matter are absorbed by the skin, can significantly increase the physiologically active of skin, improves the metabolism of skin, thus make skin more healthy, more activity arranged.
4, nano-loess can be releasing far infrared, far infrared rays acts on the human skin cell, can activate water molecules in the skin, improve the oxygen level of health, far-infrared engergy makes water molecules produce resonance, become independent water molecules, improve the oxygen level of health, make the cellular-restoring vigor, independent water molecules can freely be come in and gone out between the cell in addition, again by resonance, be converted into heat energy, make the temperature of subcutaneous deep rise a little, blood flow rate is accelerated, and can effectively prevent and the symptoms such as assisting therapy sacroiliitis, cold limbs paralysis; Far-infrared engergy purifies the blood, and improves skin matter pigment, can prevent the bone network arthropathy that causes because of uric acid.
5, nano-loess energy anion releasing uses the nano-loess perfumed soap in the shower, can increase negative ion concentration on every side, plays the effect of refreshment.
6, the rapid Ginseng Extract of nano-loess is alleviated and is discharged dermopathic side effect and makeup poison, and allergic skin inflammation etc. is had better auxiliary curative effect.Special in the Ms who likes making up, before cosmetic and after the makeup removing, use respectively the nano-loess perfumed soap to wash one's face, can play the dermopathic effect of fabulous prevention.
7, the nutrition nano-loess transparent toilet soap of the present invention preparation washing that not only the possesses general perfumed soap dirty function of dispelling also has the function of nutrition skin, anion releasing and far infrared rays, and common people use the effect that can play health care, nutrition skin.
Embodiment
Embodiment 1:
(1) modification of nano-loess solution: the nano-loess solution 80 of getting 35% effective constituent restrains in container, low whipping speed is in 600 rev/mins the situation, add dehydrated alcohol 10 grams, stir after 10 minutes, add ethylene glycol 10 grams, under same stirring velocity, stir after 10 minutes, be diluted to 2.5 times (namely with the dilutions of 2.5 times deionized water) with deionized water, stirring velocity is reduced to 200 rev/mins, stirred 10 minutes, stand-by.Because the modification of nano-loess solution has a best proportioning, be the proportioning of this example, will no longer narrate the method for modifying of nano-loess solution in the example below, only according to different situations, change the consumption of nano-loess solution.
(2) preparation of compatibility tensio-active agent: claim accurately to take by weighing tea saponin 1 gram, dehydrated alcohol 6 grams, deionized water 8 grams by said components, after dehydrated alcohol and deionized water mixed, add tensio-active agent, under 600~800 rev/mins stirring velocity, stirred 1~3 minute, both got the compatibility tensio-active agent, stand-by.
(3) allotment of perfumed soap composition: according to the method described above, take by weighing 10 parts of glycerine; 6 parts of propylene glycol; 12 parts in Zoomeric acid sodium; 10 parts in cocinic acid sodium; 6 parts of sodium stearate; 12 parts of Sodium tetradecanoates; 8 parts of stearic acid; EDTA-4Na3 part; 2 parts of modified Nano loess solution; 15 parts in compatibility tensio-active agent; 8 parts of Mierocrystalline cellulose thickening agents; 2 parts in essence.Blending means: in container, low whipping speed is in 200~400 rev/mins the situation, add successively glycerine, propylene glycol, Zoomeric acid sodium, cocinic acid sodium, stearic acid, Sodium tetradecanoate, EDTA-4Na, be warming up to gradually 70 ℃, add the compatibility tensio-active agent after stirring, dissolving.Then add thickening material under the constant temperature, mix, after about 40 minutes, be cooled to gradually 35 ℃, nano-loess solution after adding essence, the modification, deionized water sprays a small amount of defoamer in whipping process, can enter film after stirring.
(4) moulding of perfumed soap: before perfumed soap enters film, mould should be cleaned up, the a small amount of defoamer of rear sprinkling to be dried, then the perfumed soap that melts is slowly poured in the mould, with the bubble on defoamer cancellation surface, room temperature cooling or acceleration cooling in refrigerator, after band cools off fully, perfumed soap is deviate from from mould, with the preservative film parcel, be into soap.
Embodiment 2:
(1) preparation of compatibility tensio-active agent: claim accurately to take by weighing tea saponin 0.8 gram, dehydrated alcohol 8 grams, deionized water 12 grams by said components, after dehydrated alcohol and deionized water mixed, add tensio-active agent, under 600~800 rev/mins stirring velocity, stirred 1~3 minute, both got the compatibility tensio-active agent, stand-by.The modification of nano-loess solution is with embodiment 1.
(2) allotment of perfumed soap composition: according to the method described above, take by weighing 10 parts of glycerine; 6 parts of propylene glycol; 12 parts in Zoomeric acid sodium; 10 parts in cocinic acid sodium; 6 parts of sodium stearate; 12 parts of Sodium tetradecanoates; 8 parts of stearic acid; EDTA-4Na3 part; 4 parts of modified Nano loess solution; 20.8 parts in compatibility tensio-active agent; 8 parts of Mierocrystalline cellulose thickening agents; 3 parts in essence.Blending means: in container, low whipping speed is in 200~400 rev/mins the situation, add successively glycerine, propylene glycol, Zoomeric acid sodium, cocinic acid sodium, stearic acid, Sodium tetradecanoate, EDTA-4Na, be warming up to gradually 70 ℃, add the compatibility tensio-active agent after stirring, dissolving.Then add thickening material under the constant temperature, mix, after about 40 minutes, be cooled to gradually 35 ℃, nano-loess solution after adding essence, the modification, deionized water sprays a small amount of defoamer in whipping process, can enter film after stirring.
(3) moulding of perfumed soap: before perfumed soap enters film, mould should be cleaned up, the a small amount of defoamer of rear sprinkling to be dried, then the perfumed soap that melts is slowly poured in the mould, with the bubble on defoamer cancellation surface, room temperature cooling or acceleration cooling in refrigerator, after band cools off fully, perfumed soap is deviate from from mould, with the preservative film parcel, be into soap.
Embodiment 3:
(1) preparation of compatibility tensio-active agent: claim accurately to take by weighing tea saponin 0.8 gram, dehydrated alcohol 8 grams, deionized water 12 grams by said components, after dehydrated alcohol and deionized water mixed, add tensio-active agent, under 600~800 rev/mins stirring velocity, stirred 1~3 minute, both got the compatibility tensio-active agent, stand-by.
(2) allotment of perfumed soap composition: according to the method described above, take by weighing 12 parts of glycerine; 9 parts of propylene glycol; 10 parts in Zoomeric acid sodium; 10 parts in cocinic acid sodium; 5 parts of sodium stearate; 12 parts of Sodium tetradecanoates; 8 parts of stearic acid; EDTA-4Na3 part; 4 parts of modified Nano loess solution; 20.8 parts in compatibility tensio-active agent; 6 parts of Mierocrystalline cellulose thickening agents; 3 parts in essence.Blending means: in container, low whipping speed is in 200~400 rev/mins the situation, add successively glycerine, propylene glycol, Zoomeric acid sodium, cocinic acid sodium, stearic acid, Sodium tetradecanoate, EDTA-4Na, be warming up to gradually 70 ℃, add the compatibility tensio-active agent after stirring, dissolving.Then add thickening material under the constant temperature, mix, after about 40 minutes, be cooled to gradually 35 ℃, nano-loess solution after adding essence, the modification, deionized water sprays a small amount of defoamer in whipping process, can enter film after stirring.
(3) moulding of perfumed soap: before perfumed soap enters film, mould should be cleaned up, the a small amount of defoamer of rear sprinkling to be dried, then the perfumed soap that melts is slowly poured in the mould, with the bubble on defoamer cancellation surface, room temperature cooling or acceleration cooling in refrigerator, after band cools off fully, perfumed soap is deviate from from mould, with the preservative film parcel, be into soap.
Below in conjunction with the embodiments the present invention is had been described in detail; but within the protection domain of spirit of the present invention and claim; those skilled in the art can also make multiple remodeling and modification; the functional materials composition that perhaps adds other; should say that some such remodeling and modification are all within protection scope of the present invention.

Claims (3)

1. a nutrition nano-loess transparent toilet soap is characterized in that, comprises modification, tensio-active agent and the Mierocrystalline cellulose thickening agent of nano-loess solution, and prepares by following parts by weight:
5~15 parts of glycerine, 5~10 parts of propylene glycol, 10~25 parts in Zoomeric acid sodium, 8~12 parts in cocinic acid sodium, 5~12 parts of sodium stearate, 10~20 parts of Sodium tetradecanoates, 8~15 parts of stearic acid, EDTA-4Na2~6 part, compatibility tensio-active agent 10.5~26.5,1~6 part of modified Nano loess solution, 6~18 parts of Mierocrystalline cellulose thickening agents, 1~5 part in essence.
2. a kind of nutrition nano-loess transparent toilet soap according to claim 1, it is characterized in that, the method of modifying of modified Nano loess solution is: get 60~100 parts of the nano-loess solution of 35% effective constituent in container, low whipping speed is in 600~800 rev/mins the situation, add 8~12 parts of dehydrated alcohols, stir after 10 minutes, add 8~12 parts of buffer reagents, under same stirring velocity, stir after 8~12 minutes, with 2.5 times of deionized water dilutions (namely diluting with 2.5 times deionized water), stirring velocity is reduced to 200~400 rev/mins, stir and got final product in 10~20 minutes;
3. nutrition nano-loess transparent toilet soap preparation method is characterized in that preparation process is:
1) method of modifying of modified Nano loess solution: take by weighing reagent by said components, and press the deployed modified Nano loess of the method for modifying solution of above-mentioned modified Nano loess solution, stand-by;
2) preparation of compatibility tensio-active agent: take by weighing tea saponin, dehydrated alcohol, deionized water by said components, and prepare as stated above the compatibility tensio-active agent, stand-by;
3) allotment of perfumed soap composition: take by weighing 5~15 parts of glycerine, 5~10 parts of propylene glycol, 10~25 parts in Zoomeric acid sodium, 8~12 parts in cocinic acid sodium, 5~12 parts of sodium stearate, 10~20 parts of Sodium tetradecanoates, 8~15 parts of stearic acid; , EDTA-4Na2~6 part, compatibility tensio-active agent 10.5~26.5,0.4~1.2 part of modified Nano loess solution, 6~18 parts of Mierocrystalline cellulose thickening agents, 1~5 part in essence; In container, take stirring velocity as 200~400 rev/mins, add successively glycerine, propylene glycol, Zoomeric acid sodium, cocinic acid sodium, sodium stearate, Sodium tetradecanoate sodium oleate, stearic acid, be warming up to gradually 70 ℃, add the compatibility tensio-active agent after stirring, dissolving, then add thickening material under the constant temperature, mix, after about 40 minutes, be cooled to gradually 35 ℃, nano-loess solution after adding essence, the modification sprays a small amount of defoamer in whipping process, can enter film after stirring;
4) moulding of perfumed soap: before perfumed soap enters film, mould should be cleaned up, the a small amount of defoamer of rear sprinkling to be dried, then the perfumed soap that melts is slowly poured in the mould, with the bubble on defoamer cancellation surface, room temperature cooling or acceleration cooling in refrigerator, after band cools off fully, perfumed soap is deviate from from mould, with the preservative film parcel, be into soap.
CN 201110259900 2011-09-05 2011-09-05 Nutritional nano-loess transparent soap and preparation method thereof Pending CN102978035A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104263559A (en) * 2014-10-14 2015-01-07 福建师范大学 Antibacterial handmade soap containing tea saponin
TWI627270B (en) * 2015-02-17 2018-06-21 Qiu bo chang Negative ion soap process

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104263559A (en) * 2014-10-14 2015-01-07 福建师范大学 Antibacterial handmade soap containing tea saponin
TWI627270B (en) * 2015-02-17 2018-06-21 Qiu bo chang Negative ion soap process

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Application publication date: 20130320