CN102972858A - Preparation method for plant filler of paper-making process reconstituted tobacco and application of plant filler - Google Patents
Preparation method for plant filler of paper-making process reconstituted tobacco and application of plant filler Download PDFInfo
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- CN102972858A CN102972858A CN2012105544099A CN201210554409A CN102972858A CN 102972858 A CN102972858 A CN 102972858A CN 2012105544099 A CN2012105544099 A CN 2012105544099A CN 201210554409 A CN201210554409 A CN 201210554409A CN 102972858 A CN102972858 A CN 102972858A
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Abstract
The invention discloses a preparation method for plant filler of a paper-making process reconstituted tobacco, and an application of the plant filler. The preparation method comprises the steps as follows: roughly grinding different plant shells respectively to obtain different monomer shell particles; and placing 1 part of various monomer shell particles into a washing and hydrolyzing tank with a stirrer, adding 7 parts of water, stirring and heating to be 80-900 DEG C for washing and hydrolyzing reaction, filtering various monomer shell particles by a sieve with the aperture of 12 mm and a cyclone separator respectively to remove impurities, entering into a dewatering machine for solid-liquid separation, drying the separated shell particles until the water content is 4-6%, finely grinding into powder, filtering by a 60-mesh sieve to obtain finished monomer shell powder, and uniformly mixing two or more of various monomer shell powder filtered by the 60-mesh sieve at last to obtain the plant filler as a finished product. The paper-making process reconstituted tobacco with the plant filler is prepared by the following steps: adding the plant filler into tobacco slurry for making a substrate of the reconstituted tobacco according to 4-8% of the oven dry weight of the substrate of the reconstituted tobacco in percentage by weight, uniformly mixing, feeding to a paper-making machine for making and forming.
Description
Technical field
The invention belongs to the papermaking-method reconstituted tobaccos production technical field, relate to the additive that a kind of reconstituted tobacco is produced, be specifically related to effectively to improve preparation method and the application thereof of the filler of papermaking-method reconstituted tobaccos absorbency.
Background technology
In present papermaking-method reconstituted tobaccos production technology, for the absorbency (also claiming absorbability) that improves the reconstituted tobacco substrate, normally in the production of substrate, adopt the inorganic filler of classes such as adding precipitated calcium carbonate, powdered whiting to realize, to guarantee that reconstituted tobacco has certain absorbency, but the inorganic filler of these interpolations and the affinity of slurry is low, it is all relatively poor to adhere to binding ability, inorganic filler easily precipitates, more with current mistake off the net in the process of manufacturing paper with pulp of substrate, low at on-chip retention.Therefore, the absorbency of substrate is poor, the absorption of unfavorable follow-up workshop section coating fluid, and then have influence on the suction quality of reconstituted tobacco.The inorganic filler of one class such as precipitated calcium carbonate, powdered whiting is many crystallizations entity structure of aciculiform, spindle, sheet shape etc., can not guarantee effectively that the reconstituted tobacco substrate has preferably absorbency, affects to a certain extent the suction quality of reconstituted tobacco.
Summary of the invention
Purpose of the present invention is the shortcoming for existing paper-process reconstituted tobacco absorbency deficiency, a kind of papermaking-method reconstituted tobaccos absorbency that improves is provided, and then can more absorption coating fluids in follow-up coating station, the preparation method of the papermaking-method reconstituted tobaccos plant stuffing that spreading rate can obviously improve, the present invention also provide the application process of this plant stuffing in papermaking-method reconstituted tobaccos.
Purpose of the present invention is achieved through the following technical solutions.
A kind of preparation method of papermaking-method reconstituted tobaccos plant stuffing may further comprise the steps:
(1) shell of different plants is roughly ground respectively, obtained the monomer shell comminutions of different plants; Described shell includes walnut shell, shuck, Yugan sub-seed benevolence shell, peach benevolence shell, cocoanut shell;
(2) above corase grind is obtained 1 part of washing hydrolytic tanks of putting into belt stirrer of various monomer shell comminutions of different plants, add 7 parts of water and stir and be heated to 80～90
0C washs and hydrolysis, and washing and hydrolysis time are 20-30 minute;
(3) will finish washing and the various monomer shell comminutions of hydrolysis crosses respectively 12mm aperture sieve and cyclone separator and carries out removal of impurities, removal impurity and sand grains;
(4) the shell comminutions after screening and cyclonic separation advances dewaterer and carries out Separation of Solid and Liquid, is that to be dried to moisture content be 4～6% to the shell comminutions with isolated solid;
(5) dried monomer shell comminutions is finish-ground to powder and cross 60 mesh sieves, the monomer shell powder by 60 mesh sieves is finished product, can not return by the part of 60 mesh sieves and regrind;
(6) will cross in the various monomer shell of the 60 purposes powder two or more and mix, obtain the plant stuffing finished product.
The application of plant stuffing in papermaking-method reconstituted tobaccos, by weight percentage plant stuffing to be added in the tobacco slurry of the reconstituted tobacco substrate of manufacturing paper with pulp according to 4～8% of the substrate oven dry weight of reconstituted tobacco and mix, the moulding of manufacturing paper with pulp of upper paper machine namely obtains containing the papermaking-method reconstituted tobaccos of plant stuffing.
Because plant stuffing is the pure natural plant of powdery, and has stronger affinity after tobacco slurry mixes, and adsorb easily and be attached on the tobacco slurry.In addition, plant stuffing and have many spaces cytoplasm structure of protophyte has preferably absorbency, is applied to can overcome in the papermaking-method reconstituted tobaccos deficiency of adding class inorganic fillers such as precipitated calcium carbonate, powdered whiting in the existing production technology.In the substrate of the reconstituted tobacco after moulding because the multiple-void structure that has of plant stuffing makes the reconstituted tobacco substrate have stronger absorbency, and then can more absorption coating fluids in follow-up coating station, spreading rate improves comparatively obvious.In addition, plant stuffing peculiar banksia rose flavor when burning has preferably hamony with this perfume (or spice) of tobacco, thereby effectively improves the suction quality of reconstituted tobacco.Plant stuffing preparation method of the present invention is easy, and raw material obtains easily, and cost of manufacture is low, has good market application foreground.
Description of drawings
Fig. 1 is the flow chart of the inventive method.
The specific embodiment
Embodiment 1
As shown in Figure 1, the preparation method of papermaking-method reconstituted tobaccos plant stuffing of the present invention may further comprise the steps:
(1) the shell raw material of the different plants of selection such as walnut shell, shuck, Yugan sub-seed benevolence shell, peach benevolence shell, cocoanut shell, is roughly ground the monomer shell comminutions that obtains different plants with the one-level grinding machine respectively with various shells,
(2) above corase grind is obtained 1 part of washing hydrolytic tanks of putting into belt stirrer of various monomer shell comminutions of different plants, add 7 parts of water and stir and be heated to 80～90
0C washs and hydrolysis, and washing and hydrolysis time are 20-30 minute;
(3) then will finish washing and the various monomer shell comminutions of hydrolysis crosses respectively 12mm aperture sieve and cyclone separator and carries out removal of impurities, removal impurity and sand grains;
(4) the shell comminutions after screening and cyclonic separation advances dewaterer and carries out Separation of Solid and Liquid, and isolated liquid enters centralized pool and processes reuse, is that the shell comminutions is 4～6% with drier to moisture content with isolated various solids;
(5) dried various monomer shell comminutions are finish-ground to powder and cross 60 mesh sieves with the secondary grinding machine respectively, the monomer shell powder by 60 mesh sieves is finished product, can not return by the part of 60 mesh sieves and regrind;
(6) will cross the various monomer shell of 60 purposes powder is that in walnut shell powder, shuck powder, Yugan sub-seed benevolence shell powder, peach benevolence shell powder, the coconut shell powder two or more carries out the different proportion collocation and mix, and obtains the plant stuffing finished product.
The plant stuffing finished product that obtains is added in the tobacco slurry of the substrate of manufacturing paper with pulp according to 4～8% of the substrate oven dry weight of reconstituted tobacco and after mixing, the moulding of manufacturing paper with pulp of upper paper machine, namely obtain containing the papermaking-method reconstituted tobaccos of plant stuffing.
Embodiment 2
Walnut shell and shuck are prepared respectively walnut shell powder and shuck powder according to the method for embodiment 1, and each 50% mixes with walnut shell powder and shuck powder by weight percentage, obtains the plant stuffing finished product.By weight percentage the substrate over dry of reconstituted tobacco is weighed 4% plant stuffing join mix in the tobacco pulp after, manufacture paper with pulp into 60g/m at sheet forming apparatus
2Substrate, substrate is dried to moisture content 8～10% back balance certain hours.Be coated with after finishing water balance, observe simultaneously imbibition effect (absorbability).Carry out drying and carry out water balance after the substrate coating, make reconstituted tobacco moisture content after being coated with 11～12%, then weigh and calculate coating weight.
Embodiment 3
Yugan sub-seed benevolence shell, peach benevolence shell, cocoanut shell are prepared respectively Yugan sub-seed benevolence shell powder, peach benevolence shell powder and coconut shell powder according to the method for embodiment 1, and by weight percentage Yugan sub-seed benevolence shell powder 30%, peach benevolence shell powder 30% and coconut shell powder 40% are mixed, obtain the plant stuffing finished product.By weight percentage the substrate over dry of reconstituted tobacco is weighed 6% plant stuffing join mix in the tobacco pulp after, manufacture paper with pulp into 60g/m at sheet forming apparatus
2Substrate, substrate is dried to moisture content 8～10% back balance certain hours.Be coated with after finishing water balance, observe simultaneously imbibition effect (absorbability).Carry out drying and carry out water balance after the substrate coating, make reconstituted tobacco moisture content after being coated with 11～12%, then weigh and calculate coating weight.
Embodiment 4
Walnut shell, Yugan sub-seed benevolence shell, peach benevolence shell, cocoanut shell are prepared respectively walnut shell powder, Yugan sub-seed benevolence shell powder, peach benevolence shell powder and coconut shell powder according to the method for embodiment 1, and by weight percentage walnut shell powder 20%, Yugan sub-seed benevolence shell powder 20%, peach benevolence shell powder 25% and coconut shell powder 35% are mixed, obtain the plant stuffing finished product.By weight percentage the substrate over dry of reconstituted tobacco is weighed 8% plant stuffing join mix in the tobacco pulp after, manufacture paper with pulp into 60g/m at sheet forming apparatus
2Substrate, substrate is dried to moisture content 8～10% back balance certain hours.Be coated with after finishing water balance, observe simultaneously imbibition effect (absorbability).Carry out drying and carry out water balance after the substrate coating, make reconstituted tobacco moisture content after being coated with 11～12%, then weigh and calculate coating weight.
Embodiment 5
Walnut shell, shuck, Yugan sub-seed benevolence shell, peach benevolence shell, cocoanut shell are prepared respectively walnut shell powder, shuck powder, Yugan sub-seed benevolence shell powder, peach benevolence shell powder and coconut shell powder according to the method for embodiment 1, and by weight percentage walnut shell powder 15%, shuck powder 15%, Yugan sub-seed benevolence shell powder 30%, peach benevolence shell powder 20% and coconut shell powder 20% are mixed, obtain the plant stuffing finished product.By weight percentage the substrate over dry of reconstituted tobacco is weighed 10% plant stuffing join mix in the tobacco pulp after, manufacture paper with pulp into 60g/m at sheet forming apparatus
2Substrate, substrate is dried to moisture content 8～10% back balance certain hours.Be coated with after finishing water balance, observe simultaneously imbibition effect (absorbability).Carry out drying and carry out water balance after the substrate coating, make reconstituted tobacco moisture content after being coated with 11～12%, then weigh and calculate coating weight.
Do not add any filler and add the experiment of inorganic filler by above-described embodiment 2,3,4,5 method and step, and gather the sample coating result of calculation that embodiment 2,3,4,5 produces as shown in the table:
| Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Do not add any filler substrate spreading rate (%) | 5.8 | 6 | 5.9 | 5.85 |
| Add inorganic filler substrate spreading rate (%) | 44.5 | 45.2 | 46 | 45.7 |
| Add the substrate spreading rate (%) of plant stuffing | 47.5 | 50.2 | 52.4 | 54.3 |
Experimental data can find out that it is unchanged not add any filler substrate spreading rate from table, add inorganic filler substrate spreading rate change not obvious, substantially in a certain scope.Add plant stuffing of the present invention along with usage ratio increases, it is in rising trend that the substrate absorbency obviously strengthens its spreading rate, and surpass 10% it is influential to substrate intensity owing to add plant stuffing consumption of the present invention.Therefore, best plant stuffing consumption is more suitable 4-8%.Evidence, plant stuffing effect of the present invention is good.
Claims (2)
1. the preparation method of a papermaking-method reconstituted tobaccos plant stuffing is characterized in that, may further comprise the steps:
(1) shell of different plants is roughly ground respectively, obtained the monomer shell comminutions of different plants; Described shell includes walnut shell, shuck, Yugan sub-seed benevolence shell, peach benevolence shell, cocoanut shell;
(2) above corase grind is obtained 1 part of washing hydrolytic tanks of putting into belt stirrer of various monomer shell comminutions of different plants, add 7 parts of water and stir and be heated to 80～90
0C washs and hydrolysis, and washing and hydrolysis time are 20～30 minutes;
(3) will finish washing and the various monomer shell comminutions of hydrolysis crosses respectively 12mm aperture sieve and cyclone separator and carries out removal of impurities, removal impurity and sand grains;
(4) the shell comminutions after screening and cyclonic separation advances dewaterer and carries out Separation of Solid and Liquid, is that to be dried to moisture content be 4～6% to the shell comminutions with isolated solid;
(5) dried monomer shell comminutions is finish-ground to powder and cross 60 mesh sieves, the monomer shell powder by 60 mesh sieves is finished product, can not return by the part of 60 mesh sieves and regrind;
(6) will cross in the various monomer shell of the 60 purposes powder two or more and mix, obtain the plant stuffing finished product.
2. the application of plant stuffing in papermaking-method reconstituted tobaccos for preparing such as claim 1, it is characterized in that, by weight percentage plant stuffing is added in the tobacco slurry of the reconstituted tobacco substrate of manufacturing paper with pulp according to 4～8% of the substrate oven dry weight of reconstituted tobacco and mix, the moulding of manufacturing paper with pulp of upper paper machine namely obtains containing the papermaking-method reconstituted tobaccos of plant stuffing.
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| CN201210554409.9A CN102972858B (en) | 2012-12-19 | 2012-12-19 | Preparation method for plant filler of paper-making process reconstituted tobacco and application of plant filler |
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| CN201210554409.9A CN102972858B (en) | 2012-12-19 | 2012-12-19 | Preparation method for plant filler of paper-making process reconstituted tobacco and application of plant filler |
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| CN102972858A true CN102972858A (en) | 2013-03-20 |
| CN102972858B CN102972858B (en) | 2014-08-27 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112971194A (en) * | 2021-04-19 | 2021-06-18 | 云南中烟工业有限责任公司 | Tobacco flavor loading process |
| CN113455692A (en) * | 2020-03-31 | 2021-10-01 | 中烟施伟策（云南）再造烟叶有限公司 | Cocoa-containing auxiliary material for cigarettes and tobacco product |
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| CN102524932A (en) * | 2010-12-21 | 2012-07-04 | 湖北中烟工业有限责任公司 | Method for applying natural solid flavors and fragrances to papermaking-reconstructed tobacco sheets |
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Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3460959A (en) * | 1965-12-04 | 1969-08-12 | Wiederhold Fa Hermann | Covers for tips and filters of tobacco products |
| US3796222A (en) * | 1971-03-17 | 1974-03-12 | Philip Morris Inc | Method of making a smoking product from coffee bean hulls |
| GB1412878A (en) * | 1972-03-02 | 1975-11-05 | Tamag Basel Ag | Process for the manufacture of tobacco substitute by shaping from a paste |
| GB1413177A (en) * | 1972-03-02 | 1975-11-12 | Tamag Basel Ag | Process for the manufacture of regenerated tobacco |
| US3978866A (en) * | 1974-09-03 | 1976-09-07 | R. J. Reynolds Tobacco Company | Smoking compositions |
| CN1218373A (en) * | 1996-03-07 | 1999-06-02 | 英美烟草(投资)有限公司 | Smokable filler material for smoking articles |
| CN1513386A (en) * | 2003-07-07 | 2004-07-21 | 长沙卷烟厂 | Matter for lowering contents of tar and like harmful matter in smoke of cigarette |
| CN102398903A (en) * | 2010-09-10 | 2012-04-04 | 英美烟草(投资)有限公司 | Active carbon material |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113455692A (en) * | 2020-03-31 | 2021-10-01 | 中烟施伟策（云南）再造烟叶有限公司 | Cocoa-containing auxiliary material for cigarettes and tobacco product |
| CN112971194A (en) * | 2021-04-19 | 2021-06-18 | 云南中烟工业有限责任公司 | Tobacco flavor loading process |
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| CN102972858B (en) | 2014-08-27 |
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