CN102942819A - Edible printing ink containing nano materials and preparation method of edible printing ink - Google Patents
Edible printing ink containing nano materials and preparation method of edible printing ink Download PDFInfo
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- CN102942819A CN102942819A CN2012104841971A CN201210484197A CN102942819A CN 102942819 A CN102942819 A CN 102942819A CN 2012104841971 A CN2012104841971 A CN 2012104841971A CN 201210484197 A CN201210484197 A CN 201210484197A CN 102942819 A CN102942819 A CN 102942819A
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Abstract
The invention provides an edible printing ink containing nano materials and a preparation method of the edible printing ink and belongs to the technical field of printing ink manufacture. The edible printing ink containing the nano materials is characterized by comprising the following components of, by weight, 10-35 parts of food colouring toner, 20-85 parts of edible connection materials, 0-1 part of edible auxiliaries and 0.5-5 parts of the edible nano materials; and the preparation method includes weighing each component according to a claim 1, adding the food colouring toner and the edible auxiliaries to water, continuously stirring the food colouring toner and the edible auxiliaries until the food colouring toner and the edible auxiliaries are completely dissolved to obtain a solution a, adding the edible connection materials to the solution a, continuously stirring the mixture to be even to obtain an evenly mixed solution b, adding the edible nano materials to the solution b to be ground for 1-3.5 hours, and performing filling to obtain finished products after the mixture is up to the standards. The edible printing ink is good in flowability and lubricity, small in using quantity, good in shielding forces and luster, fine in granularity, thin in film and clear in printed images.
Description
Technical field
The present invention relates to edible ink, especially relate to a kind of edible ink that contains nano material and preparation method thereof, belong to printing ink manufacturing technology field.
Background technology
The printing-ink technical development so far, the printing ink of various new functions is developed out each field that is applied in, such as microcapsule shell printing ink, gold and silver color ink, fluorescent ink, magnetic ink, anti-counterfeiting printing ink, electrically conductive ink, carbon ink, supervision printing ink, temperature indication printing ink, developing ink, edible ink, ignition printing ink etc.Wherein, edible ink is as printing ink a kind of not only edible but also that can print, can not only satisfy the printability requirement of common ink, can show again the characteristics of its " edible ", be applied in and the more closely-related aspect of people's life with its safety and environmental protection, green harmless advantage.Many scientific research institutions and strong company have all released oneself more ripe ink formulations and application apparatus, and are successfully applied in many consumer products companies.But because its development time is shorter, be developed the technological deficiency that the edible ink of developing all exists some to comply with one's wishes not to the utmost.The application of edible printing ink is less in the market, mainly still print on the medicine surface, and dull coloring, image is simple, major cause is because present edible ink technology also is not very ripe, believe along with going deep into that edible ink is studied, the development of technology, it will be applied to widely field.
Fineness and the purity of edible ink have a significant impact quality product.Print out work of high quality, must have fineness, edible ink that purity is high to guarantee.The fineness of printing ink refers to that the size of pigment (the comprising stopping composition) particle in the printing ink and pigment, stopping composition are distributed in the uniformity coefficient in the low-melting ink vehicle.
Nanotechnology is the science and technology that belongs to emerging, and its research object mainly is nano material.Nowadays nano material has begun to permeate every field, and the world of medicine is the emphasis direction of China's Application of micron.Moreover, nano material also should be well worth doing in the research and development application of medicinal printing ink auxiliary material.Many characteristics of nano material are that we select the compound important reason of itself and edible ink, and it neither damages raw-material performance, gives again starting material a series of new functions.The size of nanometer material structure unit is between 1 nanometer～100 nanometer range.Because its size, adds that it has the special effects on large surface near the coherence length of electronics, it shows special character at aspects such as fusing point, magnetic, optics, heat conduction, conductive characteristics.
Nanotechnology is applied to make nano level starting material in the preparation of edible ink by new and high technology, this printing ink will be applied in food, the pharmaceutical packing, especially in the medicine on the surface printing of tablet, capsule shell.Because the fine and intrinsic characteristic of its height own, can demonstrate higher absorption and the ability of shielding ultraviolet rays, good chemical stability and thermostability, special colour-change, excellent is dispersed and transparent, fabulous gloss and opacifying power, well mobile, and excellent ink absorption and high drying property.Thereby can show pleasing candle light and ceramic texture true to nature, so that the oleophylic of printing ink and wettability raising, and allow the solid, liquid structure of printing ink reach stable; Strong coloring force, high, the high light part of glossiness is complete and whole printing is clear full; Improve the printing ink wear resistance.
Summary of the invention
For the problems referred to above, the purpose of this invention is to provide a kind of edible ink that contains nano material, this edible ink has good flowability and oilness, can reach better dispersion suspension and stable.
Last technical scheme of the present invention is such: the edible ink that this contains nano material comprises the component of following weight parts: food dye toner 10-35 part; Edible binder 20-85 part; Edible auxiliary agent 0-1 part; Edible nano material 0.5-5 part;
Wherein, described nano material is the nano level titanium oxide, nano level silicon oxide, Nano-class zinc oxide, nano level magnesium oxide, nanometer grade calcium carbonate one of them or several mixtures.
The above-mentioned edible ink that contains nano material, described food dye toner is the food grade carbon black, food grade capsanthin, beet red, Monascus color, iron oxide red, food grade Gardenia Yellow, curcumine, food grade gardenia blue, indigo wherein one of them or arbitrary combination.
Further, the above-mentioned edible ink that contains nano material, described edible binder comprises the component of following weight parts: water 20-80 part; Oil 20-80 part; Sweetener 0-20 part; Emulsifying agent 0-20 part.
Further, the above-mentioned edible ink that contains nano material, described edible auxiliary agent is ethanol, Microcrystalline Cellulose, Virahol, oleum lini, calcium stearate, magnesium palmitate, linseed oil fatty acid, pectin, cera alba, methylcellulose gum, sodium alginate, vitamin-E, vitamins C, silicon-dioxide, calcium lactate, Magnesium Stearate, the fatty acid ester compounded thing of higher alcohols, Tenox PG, phosphatide, SODIUM PHOSPHATE, MONOBASIC, glycerine, potassium primary phosphate, a kind of or arbitrary combination of chitin.
Further, the above-mentioned edible ink that contains nano material, described oil are soybean oil, glycerine, hydrogenated soybean oil, one of them of hydrogenated castor oil, refined maize oil or sweet oil or arbitrary combination.
Further, the above-mentioned edible ink that contains nano material, described sweetener are sorbyl alcohol, Xylitol, glucose, maltose, fructose, lactose, simple syrup, one of them of sucrose or arbitrary combination.
Further, the above-mentioned edible ink that contains nano material, described emulsifier lecithin, xanthan gum, one of them of Polysorbate 80 or gum arabic or arbitrary combination.
A technical scheme is such after of the present invention: the preparation method that this contains the edible ink of nano material comprises the steps: successively
1) takes by weighing the component of following weight parts: food dye toner 10-35 part; Edible binder 20-85 part; Edible auxiliary agent 0-1 part; Edible nano material 0.5-5 part;
2) food dye toner, edible auxiliary agent are added to the water, constantly are stirred to fully dissolving, get solution a;
3) binder be will eat and solution a, the solution b that constantly stirs and obtain mixing added;
4) will eat nano material and add solution b, grind 1 ~ 3.5h;
5) can finished product after the assay was approved.
Compared with prior art, the present invention has the following advantages: 1, edible ink provided by the invention has good flowability and oilness, can reach better dispersion suspension and stable, and consumption is few, the power of covering is good, gloss is excellent, granularity is fine and smooth, film forming is continuous, uniform and smooth, rete is thin, printed images is clear, printing adaptability is good; Select 2, that " Chinese pharmacopoeia is included raw material, meets edible fully and medicinal standard; 3, adhesivity is good, can be used for the lettering on the edible substrates such as most of capsule shell and tablet, and the scope of application is extensive; 4, this product corrodibility is little, and is nontoxic; 5, this product oil resistant acid resistance, fixing property is good.
Embodiment
The present invention is described in detail below in conjunction with specific embodiment, but do not consist of any limitation of the invention, and the modification of the limited number of time that anyone makes in claim scope of the present invention is still in claim protection domain of the present invention.
Embodiment 1
The preparation method is:
(a) the food grade capsanthin is added in the purified water, constantly be stirred to fully dissolving, get solution a;
(b) soybean oil, Xylitol, Yelkin TTS are added solution a, the solution b that constantly stirs and obtain mixing;
(c) the nano level titanium oxide is added solution b, grind 1 ~ 3.5h;
(d) can finished product after the assay was approved.
Embodiment 2
Embodiment 3
Embodiment 4
Embodiment 5
Embodiment 6
Inspection method
(1) color check
1. with transferring each about 5 g of ink knife label taking sample and sample, place on the sheet glass, respectively it is mixed well.
2. be applied to the upper left side of drawdown sheet with take a sample about 0.5 g of accent ink knife, about 0.5 g of materialsing again is applied to the upper right side of drawdown sheet, and both should adjacently not link to each other.
3. scraping blade is placed the ink sample top that coats, blade body portion is divided with drawdown sheet be 90o.Firmly printing ink is scraped lamellar from top to bottom on drawdown sheet, during 15 mm place, reduce firmly to the black lateral road, make the approximate 25o of the inboard angle of scraping blade, make printing ink paint thicker China ink layer at paper.
4. the printing ink thin layer on the drawdown sheet is called complexion, and the thick layer of ink of drawdown sheet bottom is called mass colour, and the printing ink thin layer on the drawdown sheet is called background color to x ray fluoroscopy x.
5. the ink colors check is complete, and glassine paper is covered on the thick China ink layer.
The result: the complexion of printing ink is similar to, conforms to standard specimen with background color.
(2) fineness check
Measure tested printing ink 0.5ml with 0.l ml suction pipe, add No. 6 solvent oils according to the size of degree of mobilization and dilute.Scope: degree of mobilization adds 18 (or add 0.30 mL with every 0.02 mL) below 24 mm; 25 mm ~ 35 mm add 14 (or 0.28 mL); 36 mm ~ 45 mm add 10 (or 0.20 mL); The above non-refuelling of 46 mm.To transfer the ink knife picking to dilute uniform printing ink, place scraper plate fineness instrument depth of groove 50 μ m places, measure the fineness of printing ink with scraper plate fineness instrument.
The result: the fineness of printing ink is 15 μ m.
(3) degree of mobilization check
1. ink samples and fluidity tester should place constant temperature indoor heat insulating 20 min in advance.
2. get ink samples (2 ~ 3) g with the accent ink knife, transfer (come and go for once) 15 times at sheet glass.Draw sample 0.1 mL with ink tube, residual ink scraped off around the mouth of pipe was reached, and sample is flushed with the mouth of pipe, and printing ink must not contain bubble in the pipe.
3. printing ink in the ink tube is extruded, China ink is scraped the Circular glass sheet center that places in the metal shaft collar with the accent ink knife, and the residual ink of blotting tube core is wiped off, smear in upper Circular glass sheet center.
4. upper Circular glass sheet is placed on the Circular glass in the metal shaft collar, has China ink to overlap in the middle of making, press immediately counterweight, (noticing that the metal shaft collar keeps level) begins to clock.
5. remove counterweight during 15 min, measure printing ink circle diameter with the transparency gage, intersect and measure twice.
The result: the degree of mobilization of printing ink is 30mm.
(4) viscosity check
1. connect instrument power source, regulating constant incubator water temperature to 32 ℃ keeps constant temperature.
2. the instrument speed control lever is placed low-speed position, will synthesize rubber roll and printing ink glue roll-in on metallic roll.
3. start instrument, behind 15 min that turn round, vernier is placed scale " 0 " position.Regulate instrument, make scale be in equilibrium state.
4. after the sample printing ink that mixes up being poured into the metal rocker blotter, again sample printing ink by extruding in the metal rocker blotter, evenly be applied on the synthetic rubber roll.Use the hand rotation motor, China ink is evenly turned be applied on metallic roll and the printing ink glue roller.
5. start instrument, even China ink.30s time shift open brake, moving cursor makes the scale balance, reads the viscosity data during l min.
The result: it is 15 that the viscosity of printing ink detects.
(5) tinting strength check
1. use analytical balance, take by weighing standard chalk 2 g at the Circular glass sheet, sample printing ink 0.2 g.Use same method, same ratio takes by weighing standard chalk and standard specimen printing ink.The black sample that weighs up is fully mixed well with the accent ink knife respectively.
2. with the accent ink knife get the standard mixed well approximately 0.5 g be applied to the upper left side of drawdown sheet, get again the sample mixed well approximately 0.5 g be applied to the upper right side of drawdown sheet, both should be adjacent and do not link to each other.
3. scraping blade is placed the ink sample top that coats, blade body portion is divided vertical with drawdown sheet.Then, printing ink is scraped lamellar from top to bottom on drawdown sheet, when scraping to (35 ~ 45) mm, reduce firmly, make the approximate 25o of the inboard angle of scraping blade, printing ink is painted thicker China ink layer at paper.
4. observe sample whether consistent with complexion, the mass colour of standard specimen, if inconsistent, then change the consumption of sample standard chalk, reach consistent to watering down sample with standard specimen, by formula calculate, draw sample tinting strength percentage ratio.
5. after scraping sample, the mass colour that reflects with observation post in 30 s is as the criterion.
Illustrate: observe and water down when scraping sample, should under the D65 standard illuminants, carry out.
The sample tinting strength, w represents with massfraction, calculates by formula (A-1):
w = m1/m2 （A-1）
In the formula: m2-water down standard chalk consumption, g;
M1-water down sample chalk consumption, g.
The result: it is 96% that the tinting strength of printing ink detects.
Claims (8)
1. an edible ink that contains nano material is characterized in that, comprises the component of following weight parts: food dye toner 10-35 part; Edible binder 20-85 part; Edible auxiliary agent 0-1 part; Edible nano material 0.5-5 part;
Wherein, described nano material is the nano level titanium oxide, nano level silicon oxide, Nano-class zinc oxide, nano level magnesium oxide, nanometer grade calcium carbonate one of them or several mixtures.
2. the edible ink that contains nano material according to claim 1, it is characterized in that, described food dye toner is the food grade carbon black, food grade capsanthin, beet red, Monascus color, iron oxide red, food grade Gardenia Yellow, curcumine, food grade gardenia blue, indigo wherein one of them or arbitrary combination.
3. the edible ink that contains nano material according to claim 1 is characterized in that, described edible binder comprises the component of following weight parts: water 20-80 part; Oil 20-80 part; Sweetener 0-20 part; Emulsifying agent 0-20 part.
4. the edible ink that contains nano material according to claim 1 is characterized in that, described edible auxiliary agent is ethanol, Microcrystalline Cellulose, Virahol, oleum lini, calcium stearate, magnesium palmitate, linseed oil fatty acid, pectin, cera alba, methylcellulose gum, sodium alginate, vitamin-E, vitamins C, silicon-dioxide, calcium lactate, Magnesium Stearate, the fatty acid ester compounded thing of higher alcohols, Tenox PG, phosphatide, SODIUM PHOSPHATE, MONOBASIC, glycerine, potassium primary phosphate, a kind of or arbitrary combination of chitin.
5. the edible ink that contains nano material according to claim 4 is characterized in that, described oil is soybean oil, glycerine, hydrogenated soybean oil, one of them of hydrogenated castor oil, refined maize oil or sweet oil or arbitrary combination.
6. the edible ink that contains nano material according to claim 4 is characterized in that, described sweetener is sorbyl alcohol, Xylitol, glucose, maltose, fructose, lactose, simple syrup, one of them of sucrose or arbitrary combination.
7. the edible ink that contains nano material according to claim 4 is characterized in that, described emulsifier lecithin, xanthan gum, one of them of Polysorbate 80 or gum arabic or arbitrary combination.
8. the preparation method who contains the edible ink of nano material claimed in claim 1 is characterized in that, comprises the steps: successively
1) takes by weighing each component by weight part claimed in claim 1;
2) food dye toner, edible auxiliary agent are added to the water, constantly are stirred to fully dissolving, get solution a;
3) binder be will eat and solution a, the solution b that constantly stirs and obtain mixing added;
4) will eat nano material and add solution b, grind 1 ~ 3.5h;
5) can finished product after the assay was approved.
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| CN201210484197.1A CN102942819B (en) | 2012-11-23 | 2012-11-23 | Edible printing ink containing nano materials and preparation method of edible printing ink |
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| CN201210484197.1A CN102942819B (en) | 2012-11-23 | 2012-11-23 | Edible printing ink containing nano materials and preparation method of edible printing ink |
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| CN102942819A true CN102942819A (en) | 2013-02-27 |
| CN102942819B CN102942819B (en) | 2015-01-07 |
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Cited By (19)
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| CN103242696A (en) * | 2013-05-24 | 2013-08-14 | 天津天康源生物技术有限公司 | Edible printing ink for printing paper and food packaging material |
| CN103254681A (en) * | 2013-05-24 | 2013-08-21 | 天津天康源生物技术有限公司 | Edible printing ink for plastic food packaging materials |
| CN103275549A (en) * | 2013-05-24 | 2013-09-04 | 天津天康源生物技术有限公司 | Edible printing ink used for chocolate printing and production method thereof |
| CN103351708A (en) * | 2013-07-08 | 2013-10-16 | 苏州凹凸彩印厂 | Edible printing ink |
| CN103408980A (en) * | 2013-07-09 | 2013-11-27 | 吴江市冰心文教用品有限公司 | Stable-color yellow environment-friendly pigment |
| CN104277578A (en) * | 2014-11-11 | 2015-01-14 | 合肥皖为电气设备工程有限责任公司 | Printing ink with good color fixation and no penetration and production method of printing ink |
| CN104831589A (en) * | 2015-04-20 | 2015-08-12 | 重庆黔龙卷烟材料有限公司 | Method used for producing tipping paper |
| CN105086590A (en) * | 2014-05-13 | 2015-11-25 | 内蒙古蒙牛乳业（集团）股份有限公司 | Noctilucent printing ink for food packaging and preparation method thereof |
| CN106036798A (en) * | 2016-06-20 | 2016-10-26 | 浙江旺林生物科技有限公司 | Application of micron-grade bamboo plant carbon black in xylitol |
| CN106046931A (en) * | 2016-06-07 | 2016-10-26 | 吴江市屯村颜料厂 | Method for preparing food-grade water-based ink with bacteriostasis function |
| CN106280705A (en) * | 2016-08-25 | 2017-01-04 | 浙江中域科技股份有限公司 | A kind of edible ink-jet printing-ink and preparation method thereof |
| CN106366766A (en) * | 2016-08-31 | 2017-02-01 | 张文涛 | Anti-counterfeiting waterborne ink for medicine packaging and preparation method of anti-counterfeiting waterborne ink |
| CN106519790A (en) * | 2016-11-18 | 2017-03-22 | 佛山市高明区海帝陶瓷原料有限公司 | Edible ink containing grape skin pigment and preparation method of edible ink |
| CN106519791A (en) * | 2016-11-18 | 2017-03-22 | 佛山市高明区海帝陶瓷原料有限公司 | Edible oil printing ink containing black soybean hull pigment and preparation method thereof |
| CN106752364A (en) * | 2016-12-30 | 2017-05-31 | 英科·卡乐油墨(苏州)有限公司 | A kind of edible water-based ink |
| CN108901131A (en) * | 2018-07-23 | 2018-11-27 | 清华大学 | The production method of printed circuit board and printed circuit board |
| WO2019051751A1 (en) * | 2017-09-14 | 2019-03-21 | 兰木长 | Preparation method for edible ink |
| CN113801515A (en) * | 2021-09-27 | 2021-12-17 | 铜陵天天纸品科技有限公司 | Edible printing ink and printer using same |
| CN114525054A (en) * | 2022-03-18 | 2022-05-24 | 潍坊潍森纤维新材料有限公司 | Preparation method of oxygen-barrier ink and application of oxygen-barrier ink in cellulose casing |
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| CN103242696A (en) * | 2013-05-24 | 2013-08-14 | 天津天康源生物技术有限公司 | Edible printing ink for printing paper and food packaging material |
| CN103254681A (en) * | 2013-05-24 | 2013-08-21 | 天津天康源生物技术有限公司 | Edible printing ink for plastic food packaging materials |
| CN103275549A (en) * | 2013-05-24 | 2013-09-04 | 天津天康源生物技术有限公司 | Edible printing ink used for chocolate printing and production method thereof |
| CN103351708A (en) * | 2013-07-08 | 2013-10-16 | 苏州凹凸彩印厂 | Edible printing ink |
| CN103408980A (en) * | 2013-07-09 | 2013-11-27 | 吴江市冰心文教用品有限公司 | Stable-color yellow environment-friendly pigment |
| CN103408980B (en) * | 2013-07-09 | 2016-01-13 | 南通市乐佳涂料有限公司 | A kind of Yellow environment-friendly pigment of color stability |
| CN105086590A (en) * | 2014-05-13 | 2015-11-25 | 内蒙古蒙牛乳业（集团）股份有限公司 | Noctilucent printing ink for food packaging and preparation method thereof |
| CN104277578A (en) * | 2014-11-11 | 2015-01-14 | 合肥皖为电气设备工程有限责任公司 | Printing ink with good color fixation and no penetration and production method of printing ink |
| CN104831589A (en) * | 2015-04-20 | 2015-08-12 | 重庆黔龙卷烟材料有限公司 | Method used for producing tipping paper |
| CN106046931A (en) * | 2016-06-07 | 2016-10-26 | 吴江市屯村颜料厂 | Method for preparing food-grade water-based ink with bacteriostasis function |
| CN106036798A (en) * | 2016-06-20 | 2016-10-26 | 浙江旺林生物科技有限公司 | Application of micron-grade bamboo plant carbon black in xylitol |
| CN106280705A (en) * | 2016-08-25 | 2017-01-04 | 浙江中域科技股份有限公司 | A kind of edible ink-jet printing-ink and preparation method thereof |
| CN106366766A (en) * | 2016-08-31 | 2017-02-01 | 张文涛 | Anti-counterfeiting waterborne ink for medicine packaging and preparation method of anti-counterfeiting waterborne ink |
| CN106519790A (en) * | 2016-11-18 | 2017-03-22 | 佛山市高明区海帝陶瓷原料有限公司 | Edible ink containing grape skin pigment and preparation method of edible ink |
| CN106519791A (en) * | 2016-11-18 | 2017-03-22 | 佛山市高明区海帝陶瓷原料有限公司 | Edible oil printing ink containing black soybean hull pigment and preparation method thereof |
| CN106752364A (en) * | 2016-12-30 | 2017-05-31 | 英科·卡乐油墨(苏州)有限公司 | A kind of edible water-based ink |
| WO2019051751A1 (en) * | 2017-09-14 | 2019-03-21 | 兰木长 | Preparation method for edible ink |
| CN108901131A (en) * | 2018-07-23 | 2018-11-27 | 清华大学 | The production method of printed circuit board and printed circuit board |
| CN113801515A (en) * | 2021-09-27 | 2021-12-17 | 铜陵天天纸品科技有限公司 | Edible printing ink and printer using same |
| CN114525054A (en) * | 2022-03-18 | 2022-05-24 | 潍坊潍森纤维新材料有限公司 | Preparation method of oxygen-barrier ink and application of oxygen-barrier ink in cellulose casing |
| CN114525054B (en) * | 2022-03-18 | 2022-10-21 | 潍坊潍森纤维新材料有限公司 | Preparation method of oxygen-barrier ink and application of oxygen-barrier ink in cellulose casing |
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