CN102919799A - Cream enzymolysis composition and preparation method thereof - Google Patents
Cream enzymolysis composition and preparation method thereof Download PDFInfo
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- CN102919799A CN102919799A CN2012104406227A CN201210440622A CN102919799A CN 102919799 A CN102919799 A CN 102919799A CN 2012104406227 A CN2012104406227 A CN 2012104406227A CN 201210440622 A CN201210440622 A CN 201210440622A CN 102919799 A CN102919799 A CN 102919799A
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Abstract
The invention discloses a cream enzymolysis composition. The composition is characterized by comprising, by weight, 0.3-0.8 part of acetic acid, 4-6 parts of butyric acid, 2-3 parts of caprylic acid, 6-8 parts of decylic acid, 4-7 parts of dodecanoic acid, 3-5 parts of myristic acid, 6-8 parts of palmitic acid, 0.1-0.2 part of s-methyl butyrate, 1-2 parts of ethyl lactate, 0.3-0.6 part of ethyl caprate, 1-3 parts of ethyl laurate, 1-3 parts of gamma-decalactone, 1-2.4 parts of gamma-onalactone, 6-8 parts of delta-decalactone, 1-3 parts of gamma-unsecalactone, 0.3-1 part of butanedione, 1-2 parts of butanone alcohol, 6-8 parts of MHT, 3-4 parts of methyl-5-thiazoleethanol acetate, 2-3 parts of vanillin, 1-2 parts of ethyl vanillin and 20-50 parts of propylene glycol. According to the composition and a preparation method thereof, an alternative solution is provided for equipment and conditions required by producing natural enzymolysis cream products, the problem of unstable aroma of the natural enzymolysis cream products is solved, the production process is simple, the raw materials are easy to acquire, batch production can be achieved, requirements for mass production are satisfied, and the applicability is high.
Description
Technical field
The present invention relates to food flavor and field of perfumery, be specifically related to a kind of prescription and compound method of cream enzymolysis composition.
Background technology
Breast and dairy products occupy critical role in food, feedstuff industry, higher nutritive value is not only arranged, and mouthfeel and fragrance are also very catchy.Dairy products essence is one of essence that developmental research enlivens the most in the essence and flavoring agent field.Dairy products essence of the prior art generally adopts cream enzymolysis flavouring technology to prepare, yet this cream enzymolysis essence is widely used certainly because of with rich flavor, milk.Yet the preparation of cream enzymolysis product needs a large amount of natural creams and the input on the equipment, and the fragrance stability of the product that makes is also relatively poor, and is subjected to the impact of the cream place of production, lipase and enzymatic hydrolysis condition very large; These defectives have all restricted the development of adopting enzymolysis cream product to prepare frankincense essence.
Summary of the invention
The object of the invention is to overcome the deficiency of the required condition of preparation of existing enzymolysis cream product and the defective of product fragrance poor stability, a kind of steady quality, raciness, the raw material that analysis makes according to the enzymolysis butter aroma is easy to get and cream enzymolysis composition that can large-scale production.
Another object of the present invention is to provide the preparation method of the above-mentioned enzymolysis cream composition of a kind of production technology is simple, application is strong preparation.
In order to reach first purpose of foregoing invention, the technical solution used in the present invention is: a kind of cream enzymolysis composition is provided, it is characterized in that: it is comprised of the raw material of following weight portion:
Acetic acid 0.3-0.8 part, butyric acid 4.0-6.0 part, sad 2.0-3.0 part, capric acid 6.0-8.0 part, dodecoic acid 4.0-7.0 part, tetradecylic acid 3.0-5.0 part, hexadecylic acid 6.0-8.0 part, methyl thiobutyrate 0.1-0.2 part, ethyl lactate 1.0-2.0 part, ethyl caprate 0.3-0.6 part, ethyl laurate 1.0-3.0 part, gamma decalactone 1.0-3.0 part, third nonalactone 1.0-2.4 part, fourth position decalactone 6.0-8.0 part, third undecalactone 1.0-3.0 part, diacetyl 0.3-1.0 part, butanone alcohol 1.0-2.0 part, thiazole sulfur 6.0-8.0 part, acetic acid thiazole sulfur 3.0-4.0 part, vanillic aldehyde 2.0-3.0 part, Ethyl vanillin 1.0-2.0 part and propane diols 20.0-50.0 part.
Preferably, described cream enzymolysis composition is comprised of the raw material of following weight portion: 0.5 part of acetic acid, 5.0 parts of butyric acid, sad 2.5 parts, 6.5 parts of capric acid, 5.0 parts of dodecoic acids, 3.5 parts of tetradecylic acids, 7.0 parts of hexadecylic acids, 0.1 part of methyl thiobutyrate, 1.0 parts of ethyl lactates, 0.4 part of ethyl caprate, 1.5 parts of ethyl laurates, 2.0 parts of gamma decalactones, 1.5 parts of third nonalactones, 7.0 parts of fourth position decalactones, 2.0 parts of third undecalactones, 0.5 part of diacetyl, 1.5 parts of butanone alcohol, 7.0 parts of thiazole sulfurs, 3.5 parts of acetic acid thiazole sulfurs, 2.5 parts of vanillic aldehydes, 38.5 parts of 1.0 parts of Ethyl vanillins and propane diols.
In order to reach second purpose of foregoing invention, the technical solution used in the present invention is: the preparation method that a kind of cream enzymolysis composition is provided, it is characterized in that, may further comprise the steps: with vanillic aldehyde, Ethyl vanillin, capric acid, dodecoic acid, tetradecylic acid, hexadecylic acid and propane diols place container to mix, then container is carried out heating water bath under 50-90 ℃, after being stirred to fully dissolving, container is naturally cooled to 20-30 ℃, add again thiazole sulfur, the acetic acid thiazole sulfur, ethyl laurate, gamma decalactone, third nonalactone, fourth position decalactone, third undecalactone, acetic acid, butyric acid, sad, ethyl lactate, methyl thiobutyrate, ethyl caprate, diacetyl and butanone alcohol, mix, namely get cream enzymolysis composition.
In sum, cream enzymolysis composition provided by the invention compared with prior art has following beneficial effect:
1) the cream enzymolysis composition that adopts specific formulated to go out provides the replacement scheme of producing the natural needed equipment of enzymolysis cream product and condition, has solved the unsettled problem of natural enzymolysis cream product fragrance;
2) the present invention utilizes volatile compound that enzymolysis cream produces and the aroma compound of butterfat mouthfeel, and draft cream enzymolysis composition that prescription institute prepares out as food, feed addictive use in corresponding ratio, not only guaranteed the natural attribute of said composition fragrance, and for product brings the mouthfeel of natural fragrance and butterfat, make simultaneously the heat resistance of product, the fragrance remaining time of fragrance be higher than the level of domestic like product.
3) production technology of the present invention is simple, and raw material is easy to get, and can manufacture, and satisfies the needs of large-scale production, and application is strong.
The specific embodiment
The below does describing in detail to produce 100kg cream enzymolysis composition as example to the specific embodiment of the present invention:
Embodiment 1
The proportioning of producing 100kg cream enzymolysis composition is:
Acetic acid 0.5kg, butyric acid 5.0kg, sad 2.5kg, capric acid 6.5kg, dodecoic acid 5.0kg, tetradecylic acid 3.5kg, hexadecylic acid 7.0kg, methyl thiobutyrate 0.1kg, ethyl lactate 1.0kg, ethyl caprate 0.4kg, ethyl laurate 1.5kg, gamma decalactone 2.0kg, third nonalactone 1.5kg, fourth position decalactone 7.0kg, third undecalactone 2.0kg, diacetyl 0.5kg, butanone alcohol 1.5kg, thiazole sulfur 7.0kg, acetic acid thiazole sulfur 3.5kg, vanillic aldehyde 2.5kg, Ethyl vanillin 1.0kg and propane diols 38.5kg.
Its preparation method is: first with vanillic aldehyde 2.5 kg, Ethyl vanillin 1.0 kg, capric acid 6.5 kg, dodecoic acid 4.0 kg, tetradecylic acid 3.5 kg, hexadecylic acid 7.0 kg and propane diols 38.5 kg place in the rustless steel container and mix, then rustless steel container being put into 80 ℃ of water-baths heats, after strong stirring dissolves extremely fully, rustless steel container is shifted out water-bath naturally cool to 30 ℃, add again thiazole sulfur 7.0 kg, acetic acid thiazole sulfur 3.5 kg, ethyl laurate 1.5 kg, gamma decalactone 2.0 kg, third nonalactone 1.5 kg, fourth position decalactone 7.0 kg, third undecalactone 2.0 kg, acetic acid 0.5 kg, butyric acid 5.0 kg, sad 2.5 kg, ethyl lactate 1.0 kg, methyl thiobutyrate 0.1 kg, ethyl caprate 0.4 kg, diacetyl 0.5 kg and butanone alcohol 1.5 kg, mix again, can the packing warehouse-in.
Embodiment 2
The proportioning of producing 100kg cream enzymolysis composition is:
Acetic acid 0.3kg, butyric acid 4.0kg, sad 2.0kg, capric acid 6.0kg, dodecoic acid 4.0kg, tetradecylic acid 3.0kg, hexadecylic acid 6.0kg, methyl thiobutyrate 0.15kg, ethyl lactate 1.5kg, ethyl caprate 0.3kg, ethyl laurate 3.0kg, gamma decalactone 3.0kg, third nonalactone 1.0kg, fourth position decalactone 6.0kg, third undecalactone 3.0kg, diacetyl 0.3kg, butanone alcohol 1.0kg, thiazole sulfur 6.0kg, acetic acid thiazole sulfur 3.0kg, vanillic aldehyde 2.0kg, Ethyl vanillin 2.0kg and propane diols 42.45kg.
Its preparation method is: first with vanillic aldehyde 2.0 kg, Ethyl vanillin 2.0 kg, capric acid 6.0 kg, dodecoic acid 4.0 kg, tetradecylic acid 3.0 kg, hexadecylic acid 6.0 kg and propane diols 42.45 kg place in the rustless steel container and mix, then rustless steel container being put into 50 ℃ of water-baths heats, after strong stirring dissolves extremely fully, rustless steel container is shifted out water-bath naturally cool to 30 ℃, add again thiazole sulfur 6.0 kg, acetic acid thiazole sulfur 3.0kg, ethyl laurate 3.0 kg, gamma decalactone 3.0 kg, third nonalactone 1.0 kg, fourth position decalactone 6.0 kg, third undecalactone 3.0kg, acetic acid 0.3 kg, butyric acid 4.0 kg, sad 2.0 kg, ethyl lactate 1.5kg, methyl thiobutyrate 0.15 kg, ethyl caprate 0.3 kg, diacetyl 0.3kg and butanone alcohol 1.0 kg, mix again, can the packing warehouse-in.
Embodiment 3
The proportioning of producing 100kg cream enzymolysis composition is:
Acetic acid 0.8kg, butyric acid 6.0kg, sad 3.0kg, capric acid 8.0kg, dodecoic acid 7.0kg, tetradecylic acid 5.0kg, hexadecylic acid 8.0kg, methyl thiobutyrate 0.2kg, ethyl lactate 2.0kg, ethyl caprate 0.5kg, ethyl laurate 1.0kg, gamma decalactone 1.0kg, third nonalactone 2.4kg, fourth position decalactone 8.0kg, third undecalactone 1.0kg, diacetyl 1.0kg, butanone alcohol 2.0kg, thiazole sulfur 8.0kg, acetic acid thiazole sulfur 4.0kg, vanillic aldehyde 3.0kg, Ethyl vanillin 1.0kg and propane diols 34.3kg.
Its preparation method is: first with vanillic aldehyde 3.0 kg, Ethyl vanillin 1.0kg, capric acid 8.0 kg, dodecoic acid 7.0 kg, tetradecylic acid 5.0 kg, hexadecylic acid 8.0 kg and propane diols 34.3kg place in the rustless steel container and mix, then rustless steel container being put into 90 ℃ of water-baths heats, after strong stirring dissolves extremely fully, rustless steel container is shifted out water-bath naturally cool to 20 ℃, add again thiazole sulfur 8.0 kg, acetic acid thiazole sulfur 4.0kg, ethyl laurate 1.0 kg, gamma decalactone 1.0 kg, third nonalactone 2.4kg, fourth position decalactone 8.0kg, third undecalactone 1.0kg, acetic acid 0.8 kg, butyric acid 6.0kg, sad 3.0kg, ethyl lactate 2.0kg, methyl thiobutyrate 0.2 kg, ethyl caprate 0.5 kg, diacetyl 1.0kg and butanone alcohol 2.0 kg, mix again, can the packing warehouse-in.
Although in conjunction with specific embodiments the specific embodiment of the present invention is described in detail, be not to be restriction to this patent protection domain.In claims limited range, various modifications that those skilled in the art can make without creative work or adjust the protection that still is subjected to this patent.
Claims (3)
1. cream enzymolysis composition is characterized in that: it is comprised of the raw material of following weight portion:
Acetic acid 0.3-0.8 part, butyric acid 4.0-6.0 part, sad 2.0-3.0 part, capric acid 6.0-8.0 part, dodecoic acid 4.0-7.0 part, tetradecylic acid 3.0-5.0 part, hexadecylic acid 6.0-8.0 part, methyl thiobutyrate 0.1-0.2 part, ethyl lactate 1.0-2.0 part, ethyl caprate 0.3-0.6 part, ethyl laurate 1.0-3.0 part, gamma decalactone 1.0-3.0 part, third nonalactone 1.0-2.4 part, fourth position decalactone 6.0-8.0 part, third undecalactone 1.0-3.0 part, diacetyl 0.3-1.0 part, butanone alcohol 1.0-2.0 part, thiazole sulfur 6.0-8.0 part, acetic acid thiazole sulfur 3.0-4.0 part, vanillic aldehyde 2.0-3.0 part, Ethyl vanillin 1.0-2.0 part and propane diols 20.0-50.0 part.
2. cream enzymolysis composition according to claim 1 is characterized in that: it is comprised of the raw material of following weight portion: 0.5 part of acetic acid, 5.0 parts of butyric acid, sad 2.5 parts, 6.5 parts of capric acid, 5.0 parts of dodecoic acids, 3.5 parts of tetradecylic acids, 7.0 parts of hexadecylic acids, 0.1 part of methyl thiobutyrate, 1.0 parts of ethyl lactates, 0.4 part of ethyl caprate, 1.5 parts of ethyl laurates, 2.0 parts of gamma decalactones, 1.5 parts of third nonalactones, 7.0 parts of fourth position decalactones, 2.0 parts of third undecalactones, 0.5 part of diacetyl, 1.5 parts of butanone alcohol, 7.0 parts of thiazole sulfurs, 3.5 parts of acetic acid thiazole sulfurs, 2.5 parts of vanillic aldehydes, 38.5 parts of 1.0 parts of Ethyl vanillins and propane diols.
3. the preparation method of a cream enzymolysis composition, it is characterized in that, may further comprise the steps: with vanillic aldehyde, Ethyl vanillin, capric acid, dodecoic acid, tetradecylic acid, hexadecylic acid and propane diols place container to mix, then container is carried out heating water bath under 50-90 ℃, after being stirred to fully dissolving, container is naturally cooled to 20-30 ℃, add again thiazole sulfur, the acetic acid thiazole sulfur, ethyl laurate, gamma decalactone, third nonalactone, fourth position decalactone, third undecalactone, acetic acid, butyric acid, sad, ethyl lactate, methyl thiobutyrate, ethyl caprate, diacetyl and butanone alcohol, mix, namely get cream enzymolysis composition.
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Cited By (6)
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| CN104256490A (en) * | 2014-07-11 | 2015-01-07 | 杭州艾菲曼普香精香料有限公司 | Condensed milk essence containing natural cream enzymatic hydrolysate |
| CN105410363A (en) * | 2015-11-17 | 2016-03-23 | 成都大帝汉克生物科技有限公司 | Milk favored paste used as dog food |
| CN106387834A (en) * | 2016-03-04 | 2017-02-15 | 广州市恒裕香料有限公司 | Xiangnaiwang essence and preparation method thereof |
| CN108713645A (en) * | 2018-05-15 | 2018-10-30 | 成都大帝汉克生物科技有限公司 | A kind of special fatty acid product improving beef cattle growth performance |
| CN112293715A (en) * | 2019-11-29 | 2021-02-02 | 内蒙古伊利实业集团股份有限公司 | Composition for endowing food with milk-flavor, enzymatic flavored milk fat and product and preparation method thereof |
| CN114831299A (en) * | 2022-03-30 | 2022-08-02 | 浙江澳杰生物技术有限公司 | Butter essence and production process thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104256490A (en) * | 2014-07-11 | 2015-01-07 | 杭州艾菲曼普香精香料有限公司 | Condensed milk essence containing natural cream enzymatic hydrolysate |
| CN105410363A (en) * | 2015-11-17 | 2016-03-23 | 成都大帝汉克生物科技有限公司 | Milk favored paste used as dog food |
| CN105410363B (en) * | 2015-11-17 | 2019-03-22 | 成都大帝汉克生物科技有限公司 | A kind of dog food milk taste slurry |
| CN106387834A (en) * | 2016-03-04 | 2017-02-15 | 广州市恒裕香料有限公司 | Xiangnaiwang essence and preparation method thereof |
| CN108713645A (en) * | 2018-05-15 | 2018-10-30 | 成都大帝汉克生物科技有限公司 | A kind of special fatty acid product improving beef cattle growth performance |
| CN112293715A (en) * | 2019-11-29 | 2021-02-02 | 内蒙古伊利实业集团股份有限公司 | Composition for endowing food with milk-flavor, enzymatic flavored milk fat and product and preparation method thereof |
| CN112293715B (en) * | 2019-11-29 | 2023-12-05 | 内蒙古伊利实业集团股份有限公司 | Composition for endowing food with milk flavor, enzymolysis aroma-enhancing milk fat and product and preparation method thereof |
| CN114831299A (en) * | 2022-03-30 | 2022-08-02 | 浙江澳杰生物技术有限公司 | Butter essence and production process thereof |
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| CN102919799B (en) | 2014-06-25 |
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