CN102911779A - Solid-liquid separation process through plate-frame pressure filtration in cutting fluid recovery - Google Patents

Solid-liquid separation process through plate-frame pressure filtration in cutting fluid recovery Download PDF

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Publication number
CN102911779A
CN102911779A CN2012104279058A CN201210427905A CN102911779A CN 102911779 A CN102911779 A CN 102911779A CN 2012104279058 A CN2012104279058 A CN 2012104279058A CN 201210427905 A CN201210427905 A CN 201210427905A CN 102911779 A CN102911779 A CN 102911779A
Authority
CN
China
Prior art keywords
filter cake
plate
reservoir
clear water
filter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN2012104279058A
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Chinese (zh)
Inventor
方汉春
朱荣兴
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZHEJIANG JINGSHENG SILICON MATERIALS CO Ltd
Original Assignee
ZHEJIANG JINGSHENG SILICON MATERIALS CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZHEJIANG JINGSHENG SILICON MATERIALS CO Ltd filed Critical ZHEJIANG JINGSHENG SILICON MATERIALS CO Ltd
Priority to CN2012104279058A priority Critical patent/CN102911779A/en
Publication of CN102911779A publication Critical patent/CN102911779A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a solid-liquid separation process through plate-frame pressure filtration in cutting fluid recovery. The process comprises the steps as follows: firstly pouring waste mortar into a reservoir I and adding a certain proportion of clear water, stirring and diluting, warming the mixture in a reaction kettle, feeding the mixture to a plate-frame filter press for primary filtering, separating primary filtrate and a filter cake I, feeding the clear water into the plate-frame filter press to clean the filter cake I to obtain primary cleaning fluid, allowing the primary filtrate to enter a decoloration procedure for continuous processing, and recycling the primary cleaning fluid into the reservoir I as dilution water; secondly, placing the filter cake I into a reservoir II and adding a certain proportion of clear water, stirring and diluting, and then conducting secondary plate-frame filtration, separating secondary filtrate and a filter cake II, then feeding clear water into the plate-frame filter press to clean the filter cake II to obtain secondary cleaning fluid, recycling the secondary filtrate and the secondary cleaning fluid into the reservoir I as dilution water, and bagging the filter cake II. According to the process, the cutting fluid remained in the filter cakes can be washed out, the residual amount of the cutting fluid in the filter cakes is reduced, and the recovery rate of the cutting fluid can be increased.

Description

Filter press solid-liquid separation process during a kind of cutting liquid reclaims
 
Technical field
The present invention relates to the filter press solid-liquid separation process in a kind of cutting liquid recovery.
Background technology
Filter press solid-liquid separation process during the cutting liquid that adopts at present reclaims is: pour waste mortar in the reservoir one a certain proportion of clear water of adding, through agitation and dilution, enter and squeeze into plate-and-frame filter press after reactor is heated and once filter, be separated into first-time filtrate and filter cake one, first-time filtrate enters bleaching process and continues processing, filter cake adds a certain proportion of clear water once again in reservoir two, through agitation and dilution, carry out again the secondary Plate Filtration, be separated into secondary filtrate and filter cake two, as diluting water, second filter cake packs and gets final product the secondary filtrate recycle to reservoir one.In aforesaid method, the filter cake two behind the secondary filtration is still residual to have more cutting liquid not to be extracted, and therefore, causes the rate of recovery of cutting liquid lower.
Summary of the invention
The purpose of this invention is to provide the filter press solid-liquid separation process in a kind of cutting liquid recovery that can improve the rate of recovery.
The technical scheme that the present invention takes is: the filter press solid-liquid separation process during a kind of cutting liquid reclaims, it is characterized in that at first, pour waste mortar in the reservoir one a certain proportion of clear water of adding, through agitation and dilution, enter and squeeze into plate-and-frame filter press after reactor is heated and once filter, be separated into first-time filtrate and filter cake one, afterwards clear water is squeezed into plate-and-frame filter press filter cake one is cleaned to get a scavenging solution, above-mentioned first-time filtrate enters bleaching process and continues processing, and one time scavenging solution is back to use reservoir one as diluting water; Secondly, filter cake adds a certain proportion of clear water once in the reservoir two and carries out agitation and dilution again, carry out again the secondary Plate Filtration, be separated into secondary filtrate and filter cake two, afterwards clear water is squeezed into plate-and-frame filter press filter cake two is cleaned to get secondary cleaning liquid, above-mentioned secondary filtrate and secondary cleaning liquid are back to use reservoir one in the lump as diluting water, and second filter cake packs and get final product.
Adopt the present invention, can reduce the residual quantity of the cutting liquid in the filter cake remaining in cutting liquid in the filter cake to coming out, just can improve the rate of recovery of cutting liquid.
Embodiment
Below in conjunction with specific embodiment invention is described further.Its operation is as follows:
At first, pour waste mortar in the reservoir one a certain proportion of clear water of adding, through agitation and dilution, enter and utilize impeller pump to squeeze into plate-and-frame filter press after reactor is heated once to filter, be separated into first-time filtrate and filter cake one, afterwards clear water is utilized impeller pump to squeeze into plate-and-frame filter press filter cake one is cleaned to get a scavenging solution, above-mentioned first-time filtrate enters bleaching process and continues processing, and one time scavenging solution is back to use reservoir one as diluting water.
Secondly, filter cake adds a certain proportion of clear water once in the reservoir two and carries out agitation and dilution again, carry out again the secondary Plate Filtration, be separated into secondary filtrate and filter cake two, afterwards clear water is utilized impeller pump to squeeze into plate-and-frame filter press filter cake two is cleaned to get secondary cleaning liquid, above-mentioned secondary filtrate and secondary cleaning liquid are back to use reservoir one in the lump as diluting water, and second filter cake packs and get final product.

Claims (1)

1. the filter press solid-liquid separation process during a cutting liquid reclaims, it is characterized in that at first, pour waste mortar in the reservoir one a certain proportion of clear water of adding, through agitation and dilution, enter and squeeze into plate-and-frame filter press after reactor is heated and once filter, be separated into first-time filtrate and filter cake one, afterwards clear water is squeezed into plate-and-frame filter press filter cake one is cleaned to get a scavenging solution, above-mentioned first-time filtrate enters bleaching process and continues processing, and one time scavenging solution is back to use reservoir one as diluting water; Secondly, filter cake adds a certain proportion of clear water once in the reservoir two and carries out agitation and dilution again, carry out again the secondary Plate Filtration, be separated into secondary filtrate and filter cake two, afterwards clear water is squeezed into plate-and-frame filter press filter cake two is cleaned to get secondary cleaning liquid, above-mentioned secondary filtrate and secondary cleaning liquid are back to use reservoir one in the lump as diluting water, and second filter cake packs and get final product.
CN2012104279058A 2012-11-01 2012-11-01 Solid-liquid separation process through plate-frame pressure filtration in cutting fluid recovery Pending CN102911779A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012104279058A CN102911779A (en) 2012-11-01 2012-11-01 Solid-liquid separation process through plate-frame pressure filtration in cutting fluid recovery

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012104279058A CN102911779A (en) 2012-11-01 2012-11-01 Solid-liquid separation process through plate-frame pressure filtration in cutting fluid recovery

Publications (1)

Publication Number Publication Date
CN102911779A true CN102911779A (en) 2013-02-06

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2012104279058A Pending CN102911779A (en) 2012-11-01 2012-11-01 Solid-liquid separation process through plate-frame pressure filtration in cutting fluid recovery

Country Status (1)

Country Link
CN (1) CN102911779A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103601199A (en) * 2013-10-14 2014-02-26 浙江晶盛硅晶材料有限公司 Method for preparing silica sol by using waste mortar produced by cutting wafers
CN105481938A (en) * 2016-01-22 2016-04-13 竹山县鑫源皂素有限责任公司 Acid cleaning method for hydrolyzed dioscoreae zingiberensis filter residues

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102108317A (en) * 2011-01-12 2011-06-29 陕西德盛新能源有限公司 Separation and purification method of silicon wafer cutting waste mortar
CN102259863A (en) * 2010-05-31 2011-11-30 溧阳汉达电子材料有限公司 Method for processing used cutting mortar
CN102557031A (en) * 2011-12-27 2012-07-11 双流新源圣光科技有限公司 Method for recycling silicon carbide in waste silicon slice cutting mortar

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102259863A (en) * 2010-05-31 2011-11-30 溧阳汉达电子材料有限公司 Method for processing used cutting mortar
CN102108317A (en) * 2011-01-12 2011-06-29 陕西德盛新能源有限公司 Separation and purification method of silicon wafer cutting waste mortar
CN102557031A (en) * 2011-12-27 2012-07-11 双流新源圣光科技有限公司 Method for recycling silicon carbide in waste silicon slice cutting mortar

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103601199A (en) * 2013-10-14 2014-02-26 浙江晶盛硅晶材料有限公司 Method for preparing silica sol by using waste mortar produced by cutting wafers
CN105481938A (en) * 2016-01-22 2016-04-13 竹山县鑫源皂素有限责任公司 Acid cleaning method for hydrolyzed dioscoreae zingiberensis filter residues

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Application publication date: 20130206