CN102898949A - Production process for colorless water-soluble capsicum oleoresin - Google Patents
Production process for colorless water-soluble capsicum oleoresin Download PDFInfo
- Publication number
- CN102898949A CN102898949A CN2012103339827A CN201210333982A CN102898949A CN 102898949 A CN102898949 A CN 102898949A CN 2012103339827 A CN2012103339827 A CN 2012103339827A CN 201210333982 A CN201210333982 A CN 201210333982A CN 102898949 A CN102898949 A CN 102898949A
- Authority
- CN
- China
- Prior art keywords
- oleoresin capsicum
- water
- soluble
- capsicum
- oleoresin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Abstract
The invention discloses a production process for a colorless water-soluble capsicum oleoresin, which belongs to the field of further processing of capsicum. According to the invention, an oil-dissolvable capsicum oleoresin is used as a raw material and undergoes short path distillation, and then sodium hydroxide is used for partial alkali refining for removal of dissociated aliphatic acid so as to obtain the colorless water-soluble capsicum oleoresin.
Description
Technical field
The invention belongs to capsicum deep processing field, particularly oleoresin capsicum modified technique.
Background technology
Oleoresin capsicum is through in recent years development, and in the time of output increased, product applications also enlarges immediately.Be accompanied by the expansion of Application Areas, product category has had new demand.Mainly concentrate on oil dissolving and water dissolution two large classes.The water dissolution product mainly carried out emulsification by adding a large amount of emulsifying agents in the past, such water-soluble oleoresin capsicum is not only with high costs, and the edible safety of product also can not get ensureing, so the phenomenons such as various additives exceed standard can occur, simultaneously also because contain a large amount of capsanthin, do not satisfy the customer demand of single use capsaicine, had a strong impact on the expansion of product competitiveness and range of application.
Summary of the invention
For overcoming defects, the invention discloses the production technique of colourless water-soluble oleoresin capsicum, capsaicine in the separating pepper oleo-resinous and capsanthin, then the molten capsicum resin of water white oil is carried out the part alkali refining, produce colourless water-soluble oleoresin capsicum with extremely low price, can also realize the value of capsanthin simultaneously.
The technical solution adopted in the present invention is: oily molten oleoresin capsicum is through the short-path distillation still, under 150 ℃, 50 handkerchief conditions, distill out the molten oleoresin capsicum of the higher water white oil of capsaicin content, add sodium hydroxide in the ratio of the molten oleoresin capsicum 8% of water white oil and carry out the part alkali refining, thereby remove free fatty acids, then through obtaining colourless water-soluble oleoresin capsicum after the water dilution.
The invention has the beneficial effects as follows in the leaching process, the oleoresin capsicum of process short-path distillation keeps its effective constituent fully and is not destroyed, and then removes free fatty acids through the part alkali refining, thereby obtains the water-soluble oleoresin capsicum; Capsanthin after the distillation is applied to painted field also by complete remaining simultaneously, has realized doulbe-sides' victory.
Embodiment
Embodiment 1, take the oily solvability oleoresin capsicum of capsaicin content 3.5% as raw material, oil solvability oleoresin capsicum drops into the short-path distillation still, under 150 ℃, 50 handkerchief pressure, distill out water white oil solvability oleoresin capsicum, through behind the short-path distillation, obtain the molten oleoresin capsicum of water white oil of capsaicin content 15%, the sodium hydroxide that then adds in the ratio of colourless oleoresin capsicum 8% carries out the part alkali refining, remove free shape lipid acid, obtain colourless water-soluble oleoresin capsicum.
Embodiment 2, take the oily solvability oleoresin capsicum of capsaicin content 5% as raw material, through behind the short-path distillation, after obtain the molten oleoresin capsicum of water white oil of capsaicin content 26%, then use sodium hydroxide to carry out the part alkali refining, remove free fatty acids, thereby obtain colourless water-soluble oleoresin capsicum.Concrete steps are: oily solvability oleoresin capsicum drops into the short-path distillation still, under 150 ℃, 50 handkerchief pressure, distill out water white oil solvability oleoresin capsicum, then the sodium hydroxide that adds in the ratio of oleoresin capsicum 8% carries out the part alkali refining, remove free shape lipid acid, obtain colourless water-soluble oleoresin capsicum.
Embodiment 3, take the oily solvability oleoresin capsicum of capsaicin content 4% as raw material, through behind the short-path distillation, after obtain the molten oleoresin capsicum of water white oil of capsaicin content 21%, then use sodium hydroxide to carry out the part alkali refining, remove free fatty acids, thereby obtain the water-soluble oleoresin capsicum.Concrete steps are: oily solvability oleoresin capsicum drops into the short-path distillation still, under 150 ℃, 50 handkerchief pressure, distill out water white oil solvability oleoresin capsicum, then the sodium hydroxide that adds in the ratio of oleoresin capsicum 8% carries out the part alkali refining, remove free shape lipid acid, obtain colourless water-soluble oleoresin capsicum.
Claims (1)
1. the production technique of colourless water-soluble oleoresin capsicum, take oleoresin capsicum as raw material, the molten oleoresin capsicum of oil is through the short-path distillation still, under 150 ℃, 50 handkerchief conditions, distill out the molten oleoresin capsicum of the higher water white oil of capsaicin content, add sodium hydroxide in the ratio of the molten oleoresin capsicum 8% of water white oil and carry out the part alkali refining, thereby remove free fatty acids, then through obtaining colourless water-soluble oleoresin capsicum after the water dilution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103339827A CN102898949A (en) | 2012-09-11 | 2012-09-11 | Production process for colorless water-soluble capsicum oleoresin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012103339827A CN102898949A (en) | 2012-09-11 | 2012-09-11 | Production process for colorless water-soluble capsicum oleoresin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102898949A true CN102898949A (en) | 2013-01-30 |
Family
ID=47571446
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2012103339827A Pending CN102898949A (en) | 2012-09-11 | 2012-09-11 | Production process for colorless water-soluble capsicum oleoresin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102898949A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104351720A (en) * | 2014-11-24 | 2015-02-18 | 青岛大学 | Preparation method of water-soluble capsicum oleoresin |
| CN109874964A (en) * | 2018-12-27 | 2019-06-14 | 晨光生物科技集团股份有限公司 | A kind of production method and its decoloration chilli extract of the chilli extract that decolourizes |
| CN113234332A (en) * | 2021-05-20 | 2021-08-10 | 云南福彻生物科技有限公司 | Method for preparing capsanthin from capsicum oleoresin |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101693854A (en) * | 2009-10-30 | 2010-04-14 | 杨崧 | Method for preparing colorless capsicum oil |
| CN102061130A (en) * | 2009-11-13 | 2011-05-18 | 天津市食品研究所有限公司 | Method for extracting chilli oil resin from chilli |
| CN102603554A (en) * | 2011-12-15 | 2012-07-25 | 武城县英潮经贸有限公司 | New process for extracting capsaicin crystal substances |
| CN102618072A (en) * | 2012-01-12 | 2012-08-01 | 华南理工大学 | Method for refining capsanthin by enzyme catalysis, esterification and molecular distillation |
-
2012
- 2012-09-11 CN CN2012103339827A patent/CN102898949A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101693854A (en) * | 2009-10-30 | 2010-04-14 | 杨崧 | Method for preparing colorless capsicum oil |
| CN102061130A (en) * | 2009-11-13 | 2011-05-18 | 天津市食品研究所有限公司 | Method for extracting chilli oil resin from chilli |
| CN102603554A (en) * | 2011-12-15 | 2012-07-25 | 武城县英潮经贸有限公司 | New process for extracting capsaicin crystal substances |
| CN102618072A (en) * | 2012-01-12 | 2012-08-01 | 华南理工大学 | Method for refining capsanthin by enzyme catalysis, esterification and molecular distillation |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104351720A (en) * | 2014-11-24 | 2015-02-18 | 青岛大学 | Preparation method of water-soluble capsicum oleoresin |
| CN104351720B (en) * | 2014-11-24 | 2015-12-30 | 青岛大学 | A kind of preparation method of water-soluble capsicum oleoresin |
| CN109874964A (en) * | 2018-12-27 | 2019-06-14 | 晨光生物科技集团股份有限公司 | A kind of production method and its decoloration chilli extract of the chilli extract that decolourizes |
| CN113234332A (en) * | 2021-05-20 | 2021-08-10 | 云南福彻生物科技有限公司 | Method for preparing capsanthin from capsicum oleoresin |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103990550B (en) | A kind of collophane direct flotation collecting agent and preparation method thereof and purposes and application process | |
| CN103084276B (en) | Preparation method of plant fatty acid diethanolamide ester soap compound collecting agent | |
| CN105695159B (en) | Solvent-free highly enriched dish washing detergent of one kind and preparation method thereof | |
| CN102898949A (en) | Production process for colorless water-soluble capsicum oleoresin | |
| CN102936610B (en) | Method for highly efficiently extracting protein from walnut dreg | |
| UY33433A (en) | NEW METHOD TO PRODUCE MICROCELLULOSE | |
| MX2021004224A (en) | Industrial preparation method of lutein and marigold flavone. | |
| CN102787037B (en) | Transparent soap | |
| CN106047539A (en) | Camellia seed handmade soap and preparation method thereof | |
| CN102205278A (en) | Collophanite flotation collecting agent prepared from rubber seed oil and method for preparing same | |
| HRP20151432T1 (en) | Process for the preparation of nebivolol | |
| CN103436369B (en) | Method for synchronously preparing biodiesel and glycerol carbonate under acceleration action of methanol | |
| CN104211597B (en) | The preparation method of rosin acid | |
| CN104211596B (en) | The preparation method of rosin acid | |
| CN103710709B (en) | A kind of water-base emulsion type antirust solution and preparation method thereof | |
| CN103360291B (en) | With producing the method that high concentration TGA prepared by the O-alkyl-N-alkyl sulfide tail washings by carbamate | |
| CN102373119A (en) | Machine cleaning agent | |
| CN104593120A (en) | Demulsifier | |
| CN103243554A (en) | Real silk fabric refining agent | |
| CN103897633B (en) | A kind of latex type natural rubber pressure sensitive adhesive | |
| CN103897879A (en) | Powerful detergent | |
| CN102807495A (en) | 3-chlorine-2-hydroxypropyl dimethyl dehydroabietic-base ammonium chloride and preparation method thereof | |
| CN105567391A (en) | Method for preparing electrical discharge machining liquid | |
| CN108854838B (en) | A kind of abietyl lactic acid surfactant and its application | |
| CN103525391A (en) | High-temperature resistant clean fracturing fluid and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20130130 |