CN102898863A - Highland barley red yeast pigment and preparation method thereof and application of highland barley red yeast pigment in food - Google Patents
Highland barley red yeast pigment and preparation method thereof and application of highland barley red yeast pigment in food Download PDFInfo
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- CN102898863A CN102898863A CN2012103800495A CN201210380049A CN102898863A CN 102898863 A CN102898863 A CN 102898863A CN 2012103800495 A CN2012103800495 A CN 2012103800495A CN 201210380049 A CN201210380049 A CN 201210380049A CN 102898863 A CN102898863 A CN 102898863A
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- highland barley
- barley monascus
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Abstract
The invention discloses a highland barley red yeast pigment and a preparation method thereof and application of the highland barley red yeast pigment in food, belongs to the technical field of biochemical products, and in particular relates to a red yeast pigment, an extraction method for the red yeast pigment and application of the red yeast pigment. The highland barley red yeast pigment is prepared by the following steps of: crushing highland barley red yeast, extracting with ethanol, concentrating and drying. The highland barley red yeast pigment has the advantages that the highland barley red yeast pigment extracted by using the method mainly contains six pigments, namely rubropunctatin, monascorabrin, monascin, ankaflavin, rubropunctamine and fmoc-allo-thr-oh by detection and analysis, the color value of the highland barley red yeast pigment reaches over 6000U/g and is improved by over 6 times compared with the color value (800u/g) of the highland barley red yeast raw material, and the highland barley red yeast pigment has good coloring capability. The highland barley red yeast pigment also contains multiple substances with health-care effect such as Monacolin K, gamma-aminobutyric acid, beta-glucan, fatty acid and ergosterol, so not only the highland barley red yeast pigment has the coloring effect, but also the health-care effect of the highland barley red yeast pigment is increased.
Description
Technical field
The invention belongs to the biological biochemistry product technique field, be specifically related to the extraction preparation method of monascorubin, monascorubin, and the purposes of monascorubin.
Background technology
Red colouring agent for food, also used as a Chinese medicine is widely used in food color, food fermentation and the Chinese materia medica as a kind of microbial fermentation product.Monascorubin is a kind of good natural pigment, it has stable in properties, thermotolerance strong (the high temperature tone at 100 ℃ remains unchanged) reaches characteristics such as protein strong coloring forces, simultaneously monascorubin security also is recognized, edible monascorubin safety non-toxic is the edible natural tinting material that is worth promoting.
The patent No. 2009103077555 discloses a kind of " highland barley monascus tea and preparation method thereof ", wherein discloses the source of a kind of " highland barley monascus ":
1) preparation Monascus anka Nakazawa et sato suspension: the red colouring agent for food, also used as a Chinese medicine bacterial classification is transferred on the substratum activates, at the in-built substratum of seed bottle, make the wedge inclined-plane, Monascus anka Nakazawa et sato after the activation is inoculated on the wedge inclined-plane and cultivates, sterilized water is joined length to be had in the seed bottle of Monascus anka Nakazawa et sato, scrapes Monascus anka Nakazawa et sato, makes the Monascus anka Nakazawa et sato suspension;
2) boiling: get highland barley, add 4-5 times of water gaging boiling 50-60 minute;
3) airing: the highland barley of boiling is drained away the water cooling;
4) fermentation: by inoculum size be 80mL-100mL/kg with the highland barley top fermentation of Monascus anka Nakazawa et sato suspension inoculation to boiling, make highland barley monascus;
5) oven dry: with highland barley monascus 40--50 ℃ oven dry.
The patent No. 200810046199.6 discloses a kind of " highland barley monascus and preparation method thereof ", by the preparation of the preparation sort of quyi, raw material, raw material inoculation with cultivate, go out finished product and make highland barley monascus.
Highland barley monascus is used for food color, food fermentation, and the effect that has not only had pigment colored has also increased the health-care effect effect of highland barley monascus pigment.But highland barley monascus unit's look valency is low, and the look valency is generally at 800u/g, and it is water-soluble not high yet, brings many inconveniences at product utilization.
Summary of the invention
The problem to be solved in the present invention is exactly that a kind of unit look valency height, water-soluble height are provided for above deficiency, and has the monascorubin of health-care effect, and the extraction preparation method of monascorubin.Its technical scheme is as follows:
Highland barley monascus pigment of the present invention makes according to the following steps:
1) select highland barley monascus to pulverize;
2) add 80% ethanolic soln of 3-4 times of amounts of highland barley monascus weight in the highland barley monascus of pulverizing to 100-120 part for the first time, concussion was extracted 1-2 hours under temperature 35-40 ℃ condition, filtered; Filter residue adds 70% ethanolic soln of 3-4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1-2 hours under temperature 25-30 ℃ condition, filtered; Filter residue adds 75% ethanolic soln of 2-3 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 0.5-1 hour under temperature 35-40 ℃ condition, filtered; Filter residue is at 60% ethanolic soln of 2-3 times of amounts of the 4th adding highland barley monascus weight, and concussion was extracted 0.5-1 hour under temperature 25-30 ℃ condition, filtered, and collected four times filtrate;
3) filtrate is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract was obtained the highland barley monascus pigment in dry 2-3 hour under-70 ℃～-55 ℃ conditions.
The preparation method of highland barley monascus pigment of the present invention may further comprise the steps:
1) select highland barley monascus to pulverize;
2) add 80% ethanolic soln of 3-4 times of amounts of highland barley monascus weight in the highland barley monascus of pulverizing to 100-120 part for the first time, concussion was extracted 1-2 hours under temperature 35-40 ℃ condition, filtered; Filter residue adds 70% ethanolic soln of 3-4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1-2 hours under temperature 25-30 ℃ condition, filtered; Filter residue adds 75% ethanolic soln of 2-3 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 0.5-1 hour under temperature 35-40 ℃ condition, filtered; Filter residue is at 60% ethanolic soln of 2-3 times of amounts of the 4th adding highland barley monascus weight, and concussion was extracted 0.5-1 hour under temperature 25-30 ℃ condition, filtered, and collected four times filtrate;
3) filtrate is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract was obtained the highland barley monascus pigment in dry 2-3 hour under-70 ℃～-55 ℃ conditions.
Compared with prior art the present invention has following beneficial effect:
1, the highland barley monascus pigment that utilizes this technique to extract, mainly contain rubropunctatin, red allusion quotation red pigment, Monascin, ankaflavin, Rubropunctamine, 6 kinds of pigments of monascorubramine by detecting to analyze, its look valency reaches more than the 6000U/g, look valency than raw material highland barley monascus 800u/g has improved more than 6 times, has preferably tinting strength.The highland barley monascus pigment also contains Monacolin K, γ-aminobutyric acid, the multiple materials with health-care effect such as beta-glucan, lipid acid, ergosterol, therefore, the highland barley monascus pigment not only has the effect of pigment colored, has also increased the health-care effect effect of highland barley monascus pigment.
2, the highland barley monascus pigment is the secondary metabolite of monascus, and other natural pigment has better thermostability, protein tinting strength relatively, and tone is soft, to soda acid and light and oxygen is more stable, nontoxic, without mutagenesis, safe.Can be used in the meat product as tinting material and sanitas; Also can be used for the food cake, soy sauce, nectar, candy etc. painted has lovely luster, edible and healthy effect.
3, this technological operation is simple, and more than highland barley monascus pigment extraction rate reached to 65%, the ethanol rate of recovery reaches more than 75%, and well Recycled ethanol recycles.
Embodiment
Embodiment one:
Present embodiment highland barley monascus pigment makes according to the following steps:
1) select the look valency to be crushed to 20 orders greater than the highland barley monascus of 800u/g;
2) adding 4 times of amounts of highland barley monascus weight for the first time in the highland barley monascus of pulverizing to 100g is 80% ethanolic soln of 400g, and concussion was extracted 2 hours under 35 ℃ of conditions of temperature, filtered; It is 70% ethanolic soln of 300g that filter residue adds 3 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1 hour under 30 ℃ of conditions of temperature, filtered; It is 75% ethanolic soln of 300g that filter residue adds 3 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 1 hour under 35 ℃ of conditions of temperature, filtered; It is 60% ethanolic soln of 200g that filter residue adds 2 times of amounts of highland barley monascus weight at the 4th time, and concussion was extracted 0.5 hour under 30 ℃ of conditions of temperature, filtered, and collected four times filtrate;
3) filtrate reduced vacuum under 59 ℃ of temperature, the negative 0.8Pa condition of pressure is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract drying under-70 ℃ of conditions was obtained the highland barley monascus pigment in 3 hours.
The preparation method of present embodiment highland barley monascus pigment may further comprise the steps:
1) select the look valency to be crushed to 20 orders greater than the highland barley monascus of 800u/g;
2) adding 4 times of amounts of highland barley monascus weight for the first time in the highland barley monascus of pulverizing to 100g is 80% ethanolic soln of 400g, and concussion was extracted 2 hours under 35 ℃ of conditions of temperature, filtered; It is 70% ethanolic soln of 300g that filter residue adds 3 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1 hour under 30 ℃ of conditions of temperature, filtered; It is 75% ethanolic soln of 300g that filter residue adds 3 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 1 hour under 35 ℃ of conditions of temperature, filtered; It is 60% ethanolic soln of 200g that filter residue adds 2 times of amounts of highland barley monascus weight at the 4th time, and concussion was extracted 0.5 hour under 30 ℃ of conditions of temperature, filtered, and collected four times filtrate;
3) filtrate reduced vacuum under 59 ℃ of temperature, the negative 0.8Pa condition of pressure is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract drying under-70 ℃ of conditions was obtained the highland barley monascus pigment in 3 hours.
Embodiment two:
Present embodiment highland barley monascus pigment makes according to the following steps:
1) select the look valency to be crushed to 80 orders greater than the highland barley monascus of 800u/g;
2) adding 3 times of amounts of highland barley monascus weight for the first time in the highland barley monascus of pulverizing to 120g is 80% ethanolic soln of 360g, and concussion was extracted 1 hour under 40 ℃ of conditions of temperature, filtered; It is 70% ethanolic soln of 480g that filter residue adds 4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 2 hours under 25 ℃ of conditions of temperature, filtered; It is 75% ethanolic soln of 240g that filter residue adds 2 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 0.5 hour under 40 ℃ of conditions of temperature, filtered; It is 60% ethanolic soln of 360g that filter residue adds 3 times of amounts of highland barley monascus weight at the 4th time, and concussion was extracted 1 hour under 25 ℃ of conditions of temperature, filtered, and collected four times filtrate;
3) filtrate reduced vacuum under 61 ℃ of temperature, the negative 0.7Pa condition of pressure is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract was obtained the highland barley monascus pigment in dry 2-3 hour under-70 ℃～-55 ℃ conditions.
The preparation method of present embodiment highland barley monascus pigment may further comprise the steps:
1) select the look valency to be crushed to 80 orders greater than the highland barley monascus of 800u/g;
2) adding 3 times of amounts of highland barley monascus weight for the first time in the highland barley monascus of pulverizing to 120g is 80% ethanolic soln of 360g, and concussion was extracted 1 hour under 40 ℃ of conditions of temperature, filtered; It is 70% ethanolic soln of 480g that filter residue adds 4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 2 hours under 25 ℃ of conditions of temperature, filtered; It is 75% ethanolic soln of 240g that filter residue adds 2 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 0.5 hour under 40 ℃ of conditions of temperature, filtered; It is 60% ethanolic soln of 360g that filter residue adds 3 times of amounts of highland barley monascus weight at the 4th time, and concussion was extracted 1 hour under 25 ℃ of conditions of temperature, filtered, and collected four times filtrate;
3) filtrate reduced vacuum under 61 ℃ of temperature, the negative 0.7Pa condition of pressure is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract was obtained the highland barley monascus pigment in dry 2-3 hour under-70 ℃～-55 ℃ conditions.
Embodiment three:
Present embodiment highland barley monascus pigment makes according to the following steps:
1) select the look valency to be crushed to 50 orders greater than the highland barley monascus of 800u/g;
2) adding 3 times of amounts of highland barley monascus weight for the first time in the highland barley monascus of pulverizing to 110g is 80% ethanolic soln of 330g, and concussion was extracted 1.5 hours under 37 ℃ of conditions of temperature, filtered; It is 70% ethanolic soln of 440g that filter residue adds 4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1.5 hours under 28 ℃ of conditions of temperature, filtered; It is 75% ethanolic soln of 220g that filter residue adds 2 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 1 hour under 37 ℃ of conditions of temperature, filtered; It is 60% ethanolic soln of 330g that filter residue adds 3 times of amounts of highland barley monascus weight at the 4th time, and concussion was extracted 0.5 hour under 28 ℃ of conditions of temperature, filtered, and collected four times filtrate;
3) filtrate reduced vacuum under temperature 60 C, the negative 0.75Pa condition of pressure is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract drying under-60 ℃ of conditions was obtained the highland barley monascus pigment in 2.5 hours.
The preparation method of present embodiment highland barley monascus pigment may further comprise the steps:
1) select the look valency to be crushed to 50 orders greater than the highland barley monascus of 800u/g;
2) adding 3 times of amounts of highland barley monascus weight for the first time in the highland barley monascus of pulverizing to 110g is 80% ethanolic soln of 330g, and concussion was extracted 1.5 hours under 37 ℃ of conditions of temperature, filtered; It is 70% ethanolic soln of 440g that filter residue adds 4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1.5 hours under 28 ℃ of conditions of temperature, filtered; It is 75% ethanolic soln of 220g that filter residue adds 2 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 1 hour under 37 ℃ of conditions of temperature, filtered; It is 60% ethanolic soln of 330g that filter residue adds 3 times of amounts of highland barley monascus weight at the 4th time, and concussion was extracted 0.5 hour under 28 ℃ of conditions of temperature, filtered, and collected four times filtrate;
3) filtrate reduced vacuum under temperature 60 C, the negative 0.75Pa condition of pressure is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract drying under-60 ℃ of conditions was obtained the highland barley monascus pigment in 2.5 hours.
Embodiment one to three used highland barley monascus is the described patent No. 2009103077555 of above-mentioned background technology or the patent No. 200810046199.6 disclosed highland barley monascus.
Embodiment four:
Present embodiment discloses the purposes of highland barley monascus pigment in meat product, is used for the painted of meat product, has the stable and rot-resistant effect of color and luster.The consumption of highland barley monascus pigment is 0.1-0.3% of meat product weight.
Embodiment five:
Present embodiment discloses the purposes of highland barley monascus pigment in the food cake, is used for the painted of food cake, has lovely luster, functional health effect.The consumption of highland barley monascus pigment is 0.01-0.1% of food cake weight.
Embodiment six:
Present embodiment discloses the purposes of highland barley monascus pigment in soy sauce or nectar, is used for the painted of soy sauce or nectar, has lovely luster, edible and healthy effect.The consumption of highland barley monascus pigment is 0.01-0.1% of soy sauce or nectar weight.
Claims (5)
1. highland barley monascus pigment is characterized in that making according to the following steps:
1) select highland barley monascus to pulverize;
2) add 80% ethanolic soln of 3-4 times of amounts of highland barley monascus weight in the highland barley monascus of pulverizing to 100-120 part for the first time, concussion was extracted 1-2 hours under temperature 35-40 ℃ condition, filtered; Filter residue adds 70% ethanolic soln of 3-4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1-2 hours under temperature 25-30 ℃ condition, filtered; Filter residue adds 75% ethanolic soln of 2-3 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 0.5-1 hour under temperature 35-40 ℃ condition, filtered; Filter residue is at 60% ethanolic soln of 2-3 times of amounts of the 4th adding highland barley monascus weight, and concussion was extracted 0.5-1 hour under temperature 25-30 ℃ condition, filtered, and collected four times filtrate;
3) filtrate is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract was obtained the highland barley monascus pigment in dry 2-3 hour under-70 ℃～-55 ℃ conditions.
2. the preparation method of the described highland barley monascus pigment of claim 1 is characterized in that may further comprise the steps:
1) select highland barley monascus to pulverize;
2) add 80% ethanolic soln of 3-4 times of amounts of highland barley monascus weight in the highland barley monascus of pulverizing to 100-120 part for the first time, concussion was extracted 1-2 hours under temperature 35-40 ℃ condition, filtered; Filter residue adds 70% ethanolic soln of 3-4 times of amounts of highland barley monascus weight for the second time, and concussion was extracted 1-2 hours under temperature 25-30 ℃ condition, filtered; Filter residue adds 75% ethanolic soln of 2-3 times of amounts of highland barley monascus weight for the third time, and concussion was extracted 0.5-1 hour under temperature 35-40 ℃ condition, filtered; Filter residue is at 60% ethanolic soln of 2-3 times of amounts of the 4th adding highland barley monascus weight, and concussion was extracted 0.5-1 hour under temperature 25-30 ℃ condition, filtered, and collected four times filtrate;
3) filtrate is concentrated into medicinal extract, Recycled ethanol;
4) medicinal extract was obtained the highland barley monascus pigment in dry 2-3 hour under-70 ℃～-55 ℃ conditions.
3. the purposes of the described highland barley monascus pigment of claim 1 in food is characterized in that the purposes in meat product.
4. the purposes of the described highland barley monascus pigment of claim 1 in food is characterized in that the purposes in the food cake.
5. the purposes of the described highland barley monascus pigment of claim 1 in food is characterized in that the purposes in soy sauce or nectar.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105146496A (en) * | 2015-09-24 | 2015-12-16 | 李志兵 | Pigment special for compound soybean sauce and preparing technology of pigment |
| CN105707895A (en) * | 2016-01-25 | 2016-06-29 | 朱喜艳 | Hulless barley enzyme beta-glucan and hulless barley enzyme beta-glucan propagation method |
| CN106318775A (en) * | 2016-08-24 | 2017-01-11 | 西藏月王生物技术有限公司 | Preparing technology of red yeast rice highland barley wine |
| CN111803597A (en) * | 2020-08-20 | 2020-10-23 | 西藏月王药诊生态藏药科技有限公司 | Highland barley monascus granules and preparation method thereof |
| CN115812832A (en) * | 2022-11-28 | 2023-03-21 | 青海华实科技投资管理有限公司 | Highland barley soft sweet and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105146496A (en) * | 2015-09-24 | 2015-12-16 | 李志兵 | Pigment special for compound soybean sauce and preparing technology of pigment |
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| CN111803597B (en) * | 2020-08-20 | 2022-04-29 | 西藏月王药诊生态藏药科技有限公司 | Highland barley monascus granules and preparation method thereof |
| CN115812832A (en) * | 2022-11-28 | 2023-03-21 | 青海华实科技投资管理有限公司 | Highland barley soft sweet and preparation method thereof |
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Address after: 850000 Lhasa economic and Technological Development Zone, Tibet City, Lhasa Road, No. 9 Patentee after: TIBET YUEWANG DRUGSTORE ECOLOGICAL TIBETAN MEDICINE TECHNOLOGY Co.,Ltd. Address before: Lhasa City, Tibet autonomous region 850000 empty road No. 1 cefn Druids District Patentee before: TIBET YUEWANG BIOLOGIC TECHNETRONIC Co.,Ltd. |
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