CN102886154A - System for extracting chorionic gonadotrophin through alcohol cycle refrigeration - Google Patents
System for extracting chorionic gonadotrophin through alcohol cycle refrigeration Download PDFInfo
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- CN102886154A CN102886154A CN2012104496238A CN201210449623A CN102886154A CN 102886154 A CN102886154 A CN 102886154A CN 2012104496238 A CN2012104496238 A CN 2012104496238A CN 201210449623 A CN201210449623 A CN 201210449623A CN 102886154 A CN102886154 A CN 102886154A
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Abstract
The invention relates to a system for extracting chorionic gonadotrophin through alcohol cycle refrigeration, which comprises a heating device and an alcohol recovery tower connected with the heating device, wherein the alcohol recovery tower is communicated with a purified alcohol storage bin through a pipeline; the purified alcohol storage bin is communicated with a refrigeration box through a pipeline; the refrigeration box is communicated with an agitation vat through a pipeline; the agitation vat is communicated with a settling vat through a pipeline; the settling vat is communicated with an agitation settling vat through a pipeline; the agitation settling vat is communicated with a separation device through a pipeline; the separation device is respectively communicated with an alcohol recycling bin and a product collecting device through pipelines; the alcohol recycling bin is communicated with the alcohol recovery tower through a pipeline; and a pipeline pump is arranged on a pipeline communicated between the alcohol recycling bin and the alcohol recovery tower. According to the system, after alcohol is used up, waste alcohol can be recycled for use so that the system cyclicity is realized.
Description
Technical field
The present invention relates to a kind of system that utilizes alcohol that material is purified, be specifically related to the system that a kind of alcohol circularly cooling extracts chorionic gonadotrophin.
Background technology
The Diluted Alcohol that alcohol distillation column is applicable to the industries such as pharmacy, food, light industry, chemical industry reclaims.Also be applicable to the distillation of other molten products of coal such as methyl alcohol.The alcohol distillation column operation principle utilizes the alcohol boiling point to be lower than the principle of too late other solution boiling point, temperature with a little higher than alcohol boiling point, the Diluted Alcohol solution that need are reclaimed carries out heated volatile, behind tower body essence gold-plating, separate out absolute alcohol gas, improve the concentration of alcoholic solution, reach the purpose of recovered alcohol.
Contain chorionic gonadotrophin in the urine of pregnant women, urine of pregnant women is after collection, at first utilize Sodium Benzoate that urine of pregnant women is adsorbed, form cake mass after the absorption, contain the chorionic gonadotrophin that contains in the urine of pregnant women that the impurity that adsorbs and needs extract in this cake mass from urine of pregnant women, further extract chorionic gonadotrophin, just need to decompose adsorbing the cake mass that forms behind the urine of pregnant women through Sodium Benzoate, remove impurity, isolate chorionic gonadotrophin.This just need to carry out resolution process with alcohol, and the alcohol that uses in the tradition needed to buy originally, and its cost is higher, and can not recycle after using, and has caused the waste of resource.
Therefore, produce a kind of simple in structurely, easy to operate, save raw material, the alcohol circularly cooling of high-efficiency environment friendly extracts the system of chorionic gonadotrophin, has widely market prospects.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of simple in structurely, easy to operate, save raw material, the alcohol circularly cooling of high-efficiency environment friendly extracts the system of chorionic gonadotrophin.
Technical scheme of the present invention is such realization: a kind of alcohol circularly cooling extracts the system of chorionic gonadotrophin, comprise heater, the alcohol distillation column that is connected with heater, described alcohol distillation column is connected with purification alcohol storage bin by pipeline, purification alcohol storage bin is connected with refrigeration case by pipeline, refrigeration case is connected with agitator by pipeline, agitator is connected with settling box by pipeline, settling box is connected with the stirring settling box by pipeline, stirring settling box is connected with separator by pipeline, separator is connected with alcohol recycling bin and product collecting device respectively by pipeline, the alcohol recycling bin is connected with alcohol distillation column by pipeline, is provided with tubing pump at the pipeline that is communicated with between alcohol recycling bin and the alcohol distillation column.
Arranging of described purification alcohol storage bin highly is not less than arranging highly of refrigeration case, arranging of refrigeration case highly is not less than arranging highly of agitator, arranging of agitator highly is not less than arranging highly of settling box, arranging of settling box highly is not less than the height that arranges that stirs settling box, stirs settling box the height that arranges that highly is not less than separator is set.
Arranging of described purification alcohol storage bin highly is not less than arranging highly of refrigeration case, agitator, settling box, stirring settling box and separator.
Described tubing pump is one-way pump.
The cryogenic temperature of described refrigeration case is-10 degrees centigrade to-18 degrees centigrade.
The volumetric concentration ratio of the alcohol that described alcohol distillation column makes is 99.5 ﹪.
The present invention has following good effect: at first, the present invention is simple in structure, easy to operate, comprise heater, the alcohol distillation column that is connected with heater, described alcohol distillation column is connected with purification alcohol storage bin by pipeline, purification alcohol storage bin is connected with refrigeration case by pipeline, refrigeration case is connected with agitator by pipeline, agitator is connected with settling box by pipeline, settling box is connected with the stirring settling box by pipeline, stirring settling box is connected with separator by pipeline, separator is connected with alcohol recycling bin and product collecting device respectively by pipeline, the alcohol recycling bin is connected with alcohol distillation column by pipeline, be provided with tubing pump at the pipeline that is communicated with between alcohol recycling bin and the alcohol distillation column, alcohol of the present invention is after finishing using, and discarded alcohol can be recycled utilization, has realized systemic circulation; Secondly, arranging of purification alcohol storage bin highly is not less than arranging highly of refrigeration case, arranging of refrigeration case highly is not less than arranging highly of agitator, arranging of agitator highly is not less than arranging highly of settling box, arranging of settling box highly is not less than the height that arranges that stirs settling box, stir settling box the height that arranges that highly is not less than separator is set, arranging of purification alcohol storage bin highly is not less than refrigeration case, agitator, settling box, stir the height that arranges of settling box and separator, utilize the height fall refrigeration of finishing alcohol rapidly and efficiently, transportation and the purification operation that utilizes alcohol to finish, reduced the time of alcohol transportation, minimizing has improved the operating efficiency of alcohol purification material because the alcohol transportation has caused the cold energy loss.
Description of drawings
Fig. 1 is structural representation of the present invention.
The specific embodiment
As shown in Figure 1, a kind of alcohol circularly cooling extracts the system of chorionic gonadotrophin, comprise heater 1, the alcohol distillation column 2 that is connected with heater, described alcohol distillation column 2 is connected with purification alcohol storage bin 3 by pipeline, purification alcohol storage bin 3 is connected with refrigeration case 4 by pipeline, refrigeration case 4 is connected with agitator 5 by pipeline, agitator 5 is connected with settling box 6 by pipeline, settling box 6 is connected with stirring settling box 7 by pipeline, stirring settling box 7 is connected with separator 8 by pipeline, separator 8 is connected with alcohol recycling bin 9 and product collecting device 10 respectively by pipeline, alcohol recycling bin 9 is connected with alcohol distillation column 2 by pipeline, is provided with tubing pump 11 at the pipeline that is communicated with between alcohol recycling bin 9 and the alcohol distillation column 2.
Arranging of described purification alcohol storage bin 3 highly is not less than arranging highly of refrigeration case 4, arranging of refrigeration case 4 highly is not less than arranging highly of agitator 5, arranging of agitator 5 highly is not less than arranging highly of settling box 6, arranging of settling box 6 highly is not less than the height that arranges that stirs settling box 7, stirs settling box 7 height that arranges that highly is not less than separator 8 is set.Arranging of described purification alcohol storage bin 3 highly is not less than refrigeration case 4, agitator 5, settling box 6, stirs arranging highly of settling box 7 and separator 8.Described tubing pump 11 is one-way pump.The cryogenic temperature of described refrigeration case 4 is-10 degrees centigrade to-18 degrees centigrade.The volumetric concentration ratio of the alcohol that described alcohol distillation column 2 makes is 99.5 ﹪.
The present invention is after collecting urine of pregnant women, utilize Sodium Benzoate absorption urine of pregnant women, form cake mass after the absorption, contain the chorionic gonadotrophin that contains in the urine of pregnant women of the impurity that from urine of pregnant women, adsorbs and needs extraction in this cake mass, to further extract chorionic gonadotrophin, just need to the cake mass that form behind Sodium Benzoate absorption urine of pregnant women be decomposed, remove impurity, isolate chorionic gonadotrophin.This just need to carry out resolution process with alcohol, the volumetric concentration ratio of the alcohol that alcohol distillation column 2 of the present invention makes is 99.5 ﹪, directly collect in the purification alcohol storage bin 3, then rely on Action of Gravity Field to flow directly in the refrigeration case 4, then by refrigeration case 4 the alcohol temperature is reduced to-10 degrees centigrade to-18 degrees centigrade, alcohol after the cooling is fed directly to and is used for stirring and decomposing the cake mass that dilution forms in the agitator 5 behind Sodium Benzoate absorption urine of pregnant women, the time of stirring in agitator 5 is 2 hours, the rotating speed of agitating device per minute is 200 to turn, then entering settling box 6 stirred 30 to 60 minutes again, and precipitate 20 hours, and then stir settling box 7 and stirred 30 minutes, material is fully dissolved, inflow separation device 8 after the natural sedimentation, isolate the products material that needs by separator 8 and flow into product collecting device 10.Isolate the alcohol that contains impurity through separator 8 and be diverted to alcohol recycling bin 9, and be withdrawn into alcohol distillation column 2 through tubing pump 11 and recycle.
Claims (6)
1. an alcohol circularly cooling extracts the system of chorionic gonadotrophin, comprise heater (1), the alcohol distillation column that is connected with heater (2), it is characterized in that: described alcohol distillation column (2) is connected with purification alcohol storage bin (3) by pipeline, purification alcohol storage bin (3) is connected with refrigeration case (4) by pipeline, refrigeration case (4) is connected with agitator (5) by pipeline, agitator (5) is connected with settling box (6) by pipeline, settling box (6) is connected with stirring settling box (7) by pipeline, stirring settling box (7) is connected with separator (8) by pipeline, separator (8) is connected with alcohol recycling bin (9) and product collecting device (10) respectively by pipeline, alcohol recycling bin (9) is connected with alcohol distillation column (2) by pipeline, is provided with tubing pump (11) at the pipeline that is communicated with between alcohol recycling bin (9) and the alcohol distillation column (2).
2. alcohol circularly cooling according to claim 1 extracts the system of chorionic gonadotrophin, it is characterized in that: arranging of described purification alcohol storage bin (3) highly is not less than arranging highly of refrigeration case (4), arranging of refrigeration case (4) highly is not less than arranging highly of agitator (5), arranging of agitator (5) highly is not less than arranging highly of settling box (6), arranging of settling box (6) highly is not less than the height that arranges that stirs settling box (7), stirs settling box (7) height that arranges that highly is not less than separator (8) is set.
3. alcohol circularly cooling according to claim 1 extracts the system of chorionic gonadotrophin, it is characterized in that: arranging of described purification alcohol storage bin (3) highly is not less than refrigeration case (4), agitator (5), settling box (6), stirs arranging highly of settling box (7) and separator (8).
4. alcohol circularly cooling according to claim 1 extracts the system of chorionic gonadotrophin, and it is characterized in that: described tubing pump (11) is one-way pump.
5. alcohol circularly cooling according to claim 1 extracts the system of chorionic gonadotrophin, and it is characterized in that: the cryogenic temperature of described refrigeration case (4) is-10 degrees centigrade to-18 degrees centigrade.
6. alcohol circularly cooling according to claim 1 extracts the system of chorionic gonadotrophin, and it is characterized in that: the volumetric concentration ratio of the alcohol that described alcohol distillation column (2) makes is 99.5 ﹪.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2012104496238A CN102886154A (en) | 2012-11-12 | 2012-11-12 | System for extracting chorionic gonadotrophin through alcohol cycle refrigeration |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012104496238A CN102886154A (en) | 2012-11-12 | 2012-11-12 | System for extracting chorionic gonadotrophin through alcohol cycle refrigeration |
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| CN102886154A true CN102886154A (en) | 2013-01-23 |
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| CN2012104496238A Pending CN102886154A (en) | 2012-11-12 | 2012-11-12 | System for extracting chorionic gonadotrophin through alcohol cycle refrigeration |
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Citations (8)
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|---|---|---|---|---|
| US4517298A (en) * | 1981-05-08 | 1985-05-14 | Georgia Tech Research Corporation | Process for producing fuel grade ethanol by continuous fermentation, solvent extraction and alcohol separation |
| US5064623A (en) * | 1988-04-11 | 1991-11-12 | Mobil Oil Corporation | Integrated system for extraction of crude alcohol and co-conversion raffinate with olefin |
| CN1302818A (en) * | 2000-12-12 | 2001-07-11 | 上海惠海生化制品厂 | Human chorionic gonadotropin and its preparing process |
| EP1746074A1 (en) * | 2005-02-10 | 2007-01-24 | Tioxide Europe S.R.L. | Process for making iron sulphate |
| CN1982271A (en) * | 2006-06-19 | 2007-06-20 | 张志伟 | Alcohol recovery device |
| CN201182917Y (en) * | 2008-03-12 | 2009-01-21 | 甘肃效灵生物开发有限责任公司 | Continuous extracting device |
| CN101792482A (en) * | 2010-03-12 | 2010-08-04 | 丽珠医药集团股份有限公司 | Method for purifying gonadotropins |
| CN203002015U (en) * | 2012-11-12 | 2013-06-19 | 常军强 | System for extracting chorionic gonadotrophin through alcohol cycle refrigeration |
-
2012
- 2012-11-12 CN CN2012104496238A patent/CN102886154A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4517298A (en) * | 1981-05-08 | 1985-05-14 | Georgia Tech Research Corporation | Process for producing fuel grade ethanol by continuous fermentation, solvent extraction and alcohol separation |
| US5064623A (en) * | 1988-04-11 | 1991-11-12 | Mobil Oil Corporation | Integrated system for extraction of crude alcohol and co-conversion raffinate with olefin |
| CN1302818A (en) * | 2000-12-12 | 2001-07-11 | 上海惠海生化制品厂 | Human chorionic gonadotropin and its preparing process |
| EP1746074A1 (en) * | 2005-02-10 | 2007-01-24 | Tioxide Europe S.R.L. | Process for making iron sulphate |
| CN1982271A (en) * | 2006-06-19 | 2007-06-20 | 张志伟 | Alcohol recovery device |
| CN201182917Y (en) * | 2008-03-12 | 2009-01-21 | 甘肃效灵生物开发有限责任公司 | Continuous extracting device |
| CN101792482A (en) * | 2010-03-12 | 2010-08-04 | 丽珠医药集团股份有限公司 | Method for purifying gonadotropins |
| CN203002015U (en) * | 2012-11-12 | 2013-06-19 | 常军强 | System for extracting chorionic gonadotrophin through alcohol cycle refrigeration |
Non-Patent Citations (2)
| Title |
|---|
| 罗金华等: "人工流产物中提取绒促性素新工艺研究", 《中国生化药物杂志》 * |
| 魏经建等: "人绒促性素粗品制备新工艺", 《中国生化药物杂志》 * |
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Application publication date: 20130123 |