CN102865723B - A kind of drying means of Minton dryer - Google Patents
A kind of drying means of Minton dryer Download PDFInfo
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- CN102865723B CN102865723B CN201110189819.3A CN201110189819A CN102865723B CN 102865723 B CN102865723 B CN 102865723B CN 201110189819 A CN201110189819 A CN 201110189819A CN 102865723 B CN102865723 B CN 102865723B
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- tank body
- horizontal tank
- charging aperture
- discharging opening
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Abstract
The invention discloses a kind of Minton dryer and utilize this Minton dryer to carry out dry method to material.The main points of its technical scheme are, a kind of Minton dryer, comprise horizontal tank body, charging aperture, discharging opening, charging aperture separation valve door, discharging opening separation valve door, vavuum pump and heater, described horizontal tank body and described charging aperture, discharging opening, vavuum pump connects respectively, described charging aperture separation valve door, horizontal tank body and charging aperture and discharging opening are isolated by discharging opening separation valve door respectively, described horizontal tank body has heating jacket, described heating jacket is connected with described heater, it is characterized in that, also involving vibrations device, described vibrating device is connected with described horizontal tank body.Main application of the present invention is by material low temperature drying under vacuum conditions, material is made to be liquefaction by mechanical oscillation, the material by heating and vacuumizing, the drying efficiency of material and degree of drying being improved again, being specially adapted to heat sensitive material, hate oxygenate material or have special drying to require.
Description
Technical field
The present invention relates to the drying means of a kind of Minton dryer to material, particularly a kind of vacuum vibration drying device carries out dry method to material.
Background technology
Vacuum drying has been widely used in the drying of the industries such as chemical industry, medicine, food for additives such as heat sensitive materials at present.Vacuum drying can under lower temperature (40 DEG C to 75 DEG C) dried material, can ensure like this material in dry run can not Yin Wendu too high and variable color, the problem such as rotten occur.But because material in vacuum drying container is not easy to stir, therefore rate of drying is lower, and container contents can produce caking phenomenon, the degree of dry materials is caused to reach technological standards.Prior art adopts gas fluidized way to solve this problem usually, but gas cannot be utilized goods fluid under vacuum higher strip part.Utilizing mechanical forces to carry out turning over materials is also a kind of method, but inside and outside this method, material exchanges very slow, and some is positioned at the material of container center, may be in centre all the time, there is uneven drying equally in stirring, the problem that degree of drying cannot be up to standard.
Summary of the invention
For the deficiencies in the prior art, the present invention proposes a kind of Minton dryer and utilize the drying means of this device, material can be made to heat in vacuum tank and be vibrated to fluidized state, in dry run, material can fully stir, the steam produced constantly is taken away by vavuum pump, to reach dry object.
In order to achieve the above object, the present invention proposes a kind of Minton dryer, comprise horizontal tank body, charging aperture, discharging opening, charging aperture separation valve door, discharging opening separation valve door, vavuum pump and heater, described horizontal tank body and described charging aperture, discharging opening, vavuum pump connects respectively, described charging aperture separation valve door, horizontal tank body and charging aperture and discharging opening are isolated by discharging opening separation valve door respectively, described horizontal tank body has heating jacket, described heating jacket is connected with described heater, it is characterized in that, also involving vibrations device, described vibrating device is connected with described horizontal tank body.
Preferred as technique scheme, also comprise condensing unit, described condensing unit is connected with vavuum pump.
Preferred as technique scheme, also comprise cleaning device, described cleaning device is connected with horizontal tank body.
Preferred as technique scheme, the heat conduction media in described heating jacket are any one of hot water, conduction oil and low-pressure steam.
Preferred as technique scheme, described horizontal tank body is provided with vacuum degree measuring equipment.
Preferred as technique scheme, also comprises the heat source recovery device be connected with described heating jacket with described condensing unit.
The invention allows for a kind of drying means of material, it comprises the following steps:
A material to be dried is loaded in charging aperture by (), open charging aperture separation valve door, the material in charging aperture enters horizontal tank body, closes charging aperture separation valve door;
B () vavuum pump is evacuated to vacuum state to horizontal tank body;
C () heater is subscribed temperature with one and is started to heat the heating jacket of horizontal tank body, vibrating device starts simultaneously, material is liquefaction under the effect of vibrating device, by the effect of heater, in material, contained humidity forms steam and constantly rolls to the surface of liquefied mass, and steam constantly extracts in condenser by vavuum pump;
D () vacuum degree measuring equipment is monitored described horizontal tank body vacuum, when described low vacuum is in a certain preset value, heater stop is to described horizontal tank body heating, described vavuum pump continues to carry out vacuum pumping to described horizontal tank body, until described tank body vacuum exceedes described preset value, heater starts to continue heating to described horizontal tank body;
E () dry run, after a ticket reserving time completes, closes heater and vavuum pump, open discharging opening separation valve door, material enters discharging opening, closes discharging opening separation valve door, closes vibrating device.
Preferred as technique scheme, described step (c) is further comprising the steps of:
Heat is passed to the heating jacket of horizontal tank body by condensing unit in condensation process by heat source recovery device.
By adopting technique scheme, Minton dryer provided by the invention and drying means are owing to have employed horizontal tank body, and material effective drying surface can be made obviously to increase, and rate of drying is improved; Material is low temperature drying under vacuum conditions, the material being specially adapted to heat sensitive material, hating oxygenate material or have special drying to require; Heat transfer type is mainly heat transfer by heat conduction, and under the effect of vibrating device and heater, material is fluidized state, and heating surface constantly rolls renewal, and the thermal efficiency and dry materials degree are improved; Organic solvent in material can be reclaimed by condensing unit, effectively reduces production cost; The heat that condensing unit is absorbed by vavuum pump can pass to heater again by heat source recovery device, saves the energy; By the vacuum pumping of vavuum pump to charging aperture and discharging opening, can vacuum feed be realized, vibration discharging, easy to operate, and can prevent material from luming; Horizontal tank body installs cleaning device, and cleaning very convenient, inner tank wall can be kept smooth, is that dry run meets GMP relevant requirements.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
Detailed description of the invention
Below in conjunction with accompanying drawing, the specific embodiment of the present invention is described in further detail.For person of ordinary skill in the field, from detailed description of the invention, above and other object of the present invention, feature and advantage will be apparent.
Be below the preferred embodiment of a kind of Minton dryer of the present invention's proposition, as shown in Figure 1,
In Fig. 1, horizontal tank body 1 is provided with heating jacket 2, horizontal tank body 1 is connected respectively with vavuum pump 3, vibrating device 4, charging aperture 5, discharging opening 6, horizontal tank body 1 is isolated with charging aperture 5 by charging aperture separation valve door 12, horizontal tank body 1 is isolated with discharging opening 6 by discharging opening separation valve door 13, is in closed condition before these two separation valve door work.Heater 7 is connected with heating jacket 2, and thermal source wherein can be hot water, conduction oil or low-pressure steam, the conduction material that can certainly be applicable to for other, thus can make the heating-up temperature that inner tank wall keeps certain.This thermal source can adopt guiding flowing to increase reflow's cycle, enlargement discharge space, improves the thermal efficiency.
Horizontal tank body 1 is arranged a vacuum degree measuring equipment 11, after dry run starts, vacuum degree measuring equipment constantly measures the vacuum in tank body, if vacuum does not reach a certain preset value, heater 7 stops heating automatically, lumps to prevent material.Condensing unit 8 is connected with vavuum pump 3, and in dry run, the steam that vavuum pump 3 is extracted out and solvent transfer in this condenser, can recycle through condensation to solvent.
Heat source recovery device 9 is connected respectively with condensing unit 8, heating jacket 2, in condensing unit 8 course of work, the heat of steam and solvent is flowed to heating interlayer 2 again by heat source recovery device, to play the object that energy regenerating utilizes, can production cost be reduced and save the energy.Cleaning device 10 is connected with horizontal tank body 1, utilizes high-temperature steam to clean inner tank wall after work completes, and reaches the object of dedusting and sterilization.
During work, material to be dried is filled in charging aperture 5, opens the charging aperture separation valve door 12 between charging aperture 5 and horizontal tank body 1, by material transferring in tank body, and close this separation valve door 12.Vavuum pump 3 is started working, and horizontal tank body 1 is evacuated to vacuum state.
Vibrating device 4 and heater 7 start simultaneously, vibrating device 4 is arranged on the base of horizontal tank body 1, its mechanical exciting force produced drives horizontal tank body 1 to produce and is synchronized with the movement, make material in tank body under vacuum conditions, through secondary ballistic fluidisation, in suspended state, simultaneously because tank body produces exciting force by mechanical exciting, making in tank body each position by 900---1800UPM vibrates, and produces the amplitude of 15-35mm.Material in tank body becomes fluidized state under the effect of vibrating device, and fully contact with the inwall of horizontal tank body 1, realize heat transmission and constantly update the area of heating surface, storeroom lamellar spacing is increased, heat exchange is carried out by the hot media in heating jacket 2, the temperature of material is constantly raised, and the hydrone in material or solvent gasify rapidly disengaging, and the hydrone gasified and solvent rise rapidly and to be taken away by vavuum pump 3.
In the process, the vacuum of vacuum degree measuring equipment 11 to horizontal tank body 1 inside is monitored, when this low vacuum is in a certain preset value, heater 7 stops heating horizontal tank body 1, vavuum pump 3 continues to carry out vacuum pumping to horizontal tank body 1, until this tank body vacuum meets or exceeds described preset value, heater 7 starts to continue heating to horizontal tank body and reaches drying purpose.
After a scheduled time, vavuum pump 3 stops vacuum pumping, heater 7 stops heating, open the discharging opening separation valve door 13 between horizontal tank body 1 and discharging opening 6, dried material is taken out to discharging opening 6, close this separation valve door 13, then close vibrating device 4, whole dry run completes.
The foregoing is only preferred embodiment of the present invention, be not used for limiting practical range of the present invention; If do not depart from the spirit and scope of the present invention, the present invention is modified or equivalent to replace, in the middle of the protection domain that all should be encompassed in claim of the present invention.
Claims (7)
1. a drying means for material, it comprises the following steps:
A material to be dried is loaded in charging aperture by (), open charging aperture separation valve door, the material in charging aperture enters horizontal tank body, closes charging aperture separation valve door;
B () vavuum pump is evacuated to vacuum state to horizontal tank body;
C () heater is subscribed temperature with one and is started to heat the heating jacket of horizontal tank body, vibrating device starts simultaneously, material is liquefaction under the effect of vibrating device, by the effect of heater, in material, contained humidity forms steam and constantly rolls to the surface of liquefied mass, and steam constantly extracts in condenser by vavuum pump;
D () vacuum degree measuring equipment is monitored described horizontal tank body vacuum, when described low vacuum is in a certain preset value, heater stop is to described horizontal tank body heating, described vavuum pump continues to carry out vacuum pumping to described horizontal tank body, until described tank body vacuum exceedes described preset value, heater starts to continue heating to described horizontal tank body;
E () dry run, after a ticket reserving time completes, closes heater and vavuum pump, open discharging opening separation valve door, material enters discharging opening, closes discharging opening separation valve door, closes vibrating device;
For the Minton dryer of described dry materials method, comprise horizontal tank body, charging aperture, discharging opening, charging aperture separation valve door, discharging opening separation valve door, vavuum pump and heater, described horizontal tank body is connected respectively with described charging aperture, discharging opening, vavuum pump, horizontal tank body and charging aperture and discharging opening are isolated by described charging aperture separation valve door, discharging opening separation valve door respectively, described horizontal tank body has heating jacket, described heating jacket is connected with described heater, and described vibrating device is connected with described horizontal tank body.
2. the drying means of material as claimed in claim 1, it is characterized in that, described step (c) is further comprising the steps of:
Heat is passed to the heating jacket of horizontal tank body by condensing unit in condensation process by heat source recovery device.
3. the drying means of material as claimed in claim 1, it is characterized in that, also comprise condensing unit, described condensing unit is connected with vavuum pump.
4. the drying means of the material as described in claim 1 or 3, is characterized in that, also comprises cleaning device, and described cleaning device is connected with horizontal tank body.
5. the drying means of the material as described in claim 1 or 3, is characterized in that, the heat conduction media in described heating jacket are any one of hot water, conduction oil and low-pressure steam.
6. the drying means of the material as described in claim 1 or 3, is characterized in that, described horizontal tank body is provided with vacuum degree measuring equipment.
7. the drying means of material as claimed in claim 3, is characterized in that, also comprise the heat source recovery device be connected with described heating jacket with described condensing unit.
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CN201110189819.3A CN102865723B (en) | 2011-07-07 | 2011-07-07 | A kind of drying means of Minton dryer |
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CN201110189819.3A CN102865723B (en) | 2011-07-07 | 2011-07-07 | A kind of drying means of Minton dryer |
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CN102865723B true CN102865723B (en) | 2015-09-16 |
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CN103968652B (en) * | 2014-04-29 | 2016-05-25 | 李亚光 | A kind of water-bath vacuum oven system and baking method thereof |
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CN105115260A (en) * | 2015-07-20 | 2015-12-02 | 太仓市友联干燥粉碎设备有限公司 | Vibration vacuum drying system |
CN105124021A (en) * | 2015-09-28 | 2015-12-09 | 江苏农林职业技术学院 | Green tea vacuum low temperature drying device |
CN105651007B (en) * | 2016-01-28 | 2019-04-12 | 黄禹铭 | A kind of medicinal material foodstuff seed low-temperature air energy vacuum drying device |
CN114191832A (en) * | 2021-09-30 | 2022-03-18 | 宜宾锂宝新材料有限公司 | Integrated drying and coating equipment for ternary cathode material and using method of integrated drying and coating equipment |
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CN118654450A (en) * | 2024-08-20 | 2024-09-17 | 昆明学院 | Take waste heat recovery's vacuum drying device |
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EP1108967A1 (en) * | 1999-12-15 | 2001-06-20 | Zanchetta & C. S.r.l. | A vibrating vacuum dryer and the related drying method |
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CN201086237Y (en) * | 2007-08-10 | 2008-07-16 | 株洲精工硬质合金有限公司 | Vibration drying mechanism for hard metal mix |
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Patent Citations (6)
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US3733716A (en) * | 1970-06-02 | 1973-05-22 | Matsushita Electric Works Ltd | Lyophilization installation |
CN2083275U (en) * | 1990-08-11 | 1991-08-21 | 浙江省石油化工设计院 | Vacuum vibration drying apparatus |
EP1108967A1 (en) * | 1999-12-15 | 2001-06-20 | Zanchetta & C. S.r.l. | A vibrating vacuum dryer and the related drying method |
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Address after: 215428 Shalu Highway 99, Jungjing Town, Taicang City, Suzhou City, Jiangsu Province Patentee after: Jiangsu Shenjiu (Group) Co.,Ltd. Address before: 215428 Shalu Highway 99, Jungjing Town, Taicang City, Suzhou City, Jiangsu Province Patentee before: JIANGSU SHENJIU CHEMICAL FIBER Co.,Ltd. |
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