CN102863811A - Underwater luminous master batch and preparation process thereof - Google Patents
Underwater luminous master batch and preparation process thereof Download PDFInfo
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- CN102863811A CN102863811A CN2012103204463A CN201210320446A CN102863811A CN 102863811 A CN102863811 A CN 102863811A CN 2012103204463 A CN2012103204463 A CN 2012103204463A CN 201210320446 A CN201210320446 A CN 201210320446A CN 102863811 A CN102863811 A CN 102863811A
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Abstract
The invention relates to an underwater luminous master batch and a preparation process thereof, belonging to the technical fields of the master batch and the preparation process of the master batch. The underwater luminous master batch contains a carrier, wherein a luminous layer which is prepared from energy storage luminous powder covers the carrier. The preparation process comprises the following steps: 1) preparing; 2) heating; 3) mixing; 4) performing extrusion granulation; and 5) drying. The underwater luminous master batch has a reasonable structural design; as the luminous layer prepared from the energy storage luminous powder covers the carrier, the prepared master batch can absorb, store and give out light and meet the requirements of the industry; and the preparation process of the underwater luminous master batch is simple and fast, the preparation cost is low and the application prospect is broad.
Description
Technical field
The present invention relates to Masterbatch and fabricating technology field thereof, specifically, relate to a kind of underwater light-emitting Masterbatch and preparation technology thereof.
Background technology
Masterbatch is painted to be the coloring plastic method that the most generally adopts now, Masterbatch generally is comprised of three parts, be tinting material, carrier and dispersion agent, after mixing by the high speed muller, broken, extrude and pull into grain, Masterbatch has the remarkable advantages such as concentration height, good dispersity, cleaning in the plastic working process.
Existing Masterbatch can't absorb, store, distribute light source, can't adapt under water sign and fishery job requirements under water.
Summary of the invention
The object of the invention is to solve the weak point that above-mentioned prior art exists, a kind of underwater light-emitting Masterbatch that can absorb, store, distribute light source is provided, preparation technology is simple and direct for this Masterbatch, and preparation cost is cheap.
For addressing the above problem, the technical solution adopted in the present invention is:
A kind of underwater light-emitting Masterbatch is characterized in that: comprise carrier, the outside of carrier is coated with the luminescent layer of being made by the photo-induced energy storage luminescent powder.
Say further:
The thickness of described luminescent layer is the 0.6-1.2 millimeter.
Being shaped as of described underwater light-emitting Masterbatch is circular, cylindrical, in the rectangle any one.
The preparation technology of described underwater light-emitting Masterbatch may further comprise the steps:
1, modulation
Photo-induced energy storage luminescent powder and water are (5-7) in mass ratio: (3-5) mix;
2, mix
The mixture of step 1 gained and carrier dropped in the high speed amalgamator carry out combination treatment;
3, extruding pelletization
The mixture of step 2 gained is delivered in the screw extrusion press, and the temperature in the screw extrusion press is controlled at 200-300 ℃, and rotating speed is the 250-350r/min extruding pelletization;
4, drying
The Masterbatch that step 3) is obtained carries out drying treatment in drying machine, dried Masterbatch water content is controlled at 5%-7%.
Say further:
Also have heating steps between described step 1 and the step 2, be specially:
The mass transport of step 1 gained is heated to cooking-vessel, and heating and temperature control heated 20-30 minute at 50-70 ℃.
The time of combination treatment described in the step 2 is 40-50 minute.
Screw extrusion press described in the step 3 is any one in twin screw extruder or the single screw extrusion machine.
Drying temperature in the drying machine described in the step 4 is controlled at 30-40 ℃.
Compared with prior art, underwater light-emitting Masterbatch of the present invention, reasonable in design is because the outside of carrier is coated with the luminescent layer of being made by the photo-induced energy storage luminescent powder, therefore, the Masterbatch of preparing can absorb, store, distribute light source, adapt to industry requirement, and underwater light-emitting Masterbatch preparation technology of the present invention is simple and direct, preparation cost is cheap, has broad application prospects.
Description of drawings
Accompanying drawing is the structural representation of a kind of embodiment of underwater light-emitting Masterbatch of the present invention.
Embodiment
For technique means, creation characteristic that the present invention is realized, reach purpose and effect is easy to understand, further set forth the present invention below in conjunction with concrete diagram.
With reference to accompanying drawing, the described underwater light-emitting Masterbatch of present embodiment is circular, comprises carrier 1, and the outside of carrier 1 is coated with the luminescent layer 2 of being made by the photo-induced energy storage luminescent powder, and the thickness of luminescent layer 2 is 0.6 millimeter,
The preparation technology of above-mentioned underwater light-emitting Masterbatch may further comprise the steps:
1, modulation
Photo-induced energy storage luminescent powder and water are mixed for 5:3 in mass ratio.
2, heating
The mass transport of step 1 gained is heated to cooking-vessel, and heating and temperature control heated 20 minutes at 50 ℃.
3, mix
The mixture of step 2 gained and carrier dropped in the high speed amalgamator carry out combination treatment, the time of processing is 40 minutes.
4, extruding pelletization
The mixture of step 3 gained is delivered in the twin screw extruder, and the temperature in the twin screw extruder is controlled at 200 ℃, and rotating speed is the 250r/min extruding pelletization.
5, drying
The Masterbatch that step 4 is obtained carries out drying treatment in drying machine, the drying temperature in the drying machine is controlled at 30 ℃, and dried Masterbatch water content is controlled at 5%.
The described underwater light-emitting Masterbatch of present embodiment is cylindrical, comprises carrier, and the outside of carrier is coated with the luminescent layer of being made by the photo-induced energy storage luminescent powder, and the thickness of luminescent layer is 1.2 millimeters.
The preparation technology of above-mentioned underwater light-emitting Masterbatch may further comprise the steps:
1, modulation
Photo-induced energy storage luminescent powder and water are mixed for 7:5 in mass ratio.
2, heating
The mass transport of step 1 gained is heated to cooking-vessel, and heating and temperature control heated 30 minutes at 70 ℃.
3, mix
The mixture of step 2 gained and carrier dropped in the high speed amalgamator carry out combination treatment, the time of combination treatment is 50 minutes.
4, extruding pelletization
The mixture of step 3 gained is delivered in the twin screw extruder, and the temperature in the twin screw extruder is controlled at 300 ℃, and rotating speed is the 350r/min extruding pelletization.
5, drying
The Masterbatch that step 4 is obtained carries out drying treatment in drying machine, the drying temperature in the drying machine is controlled at 40 ℃, and dried Masterbatch water content is controlled at 7%.
Embodiment 3
The described underwater light-emitting Masterbatch of present embodiment is rectangle, comprises carrier, and the outside of carrier is coated with the luminescent layer of being made by the photo-induced energy storage luminescent powder, and the thickness of luminescent layer is 1.0 millimeters.
The preparation technology of above-mentioned underwater light-emitting Masterbatch may further comprise the steps:
1, modulation
Photo-induced energy storage luminescent powder and water are mixed for 6:4 in mass ratio.
2, heating
The mass transport of step 1 gained is heated to cooking-vessel, and heating and temperature control heated 25 minutes at 60 ℃.
3, mix
The mixture of step 2 gained and carrier dropped in the high speed amalgamator carry out combination treatment, the time of combination treatment is 45 minutes.
4, extruding pelletization
The mixture of step 3 gained is delivered in the single screw extrusion machine, and the temperature in the single screw extrusion machine is controlled at 250 ℃, and rotating speed is the 300r/min extruding pelletization.
5, drying
The Masterbatch that step 4 is obtained carries out drying treatment in drying machine, the drying temperature in the drying machine is controlled at, and 35 ℃, dried Masterbatch water content is controlled at 6%.
More than show and described ultimate principle of the present invention, principal character and advantage.The technician of the industry should understand; the present invention is not restricted to the described embodiments; that describes in above-described embodiment and the specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (8)
1. underwater light-emitting Masterbatch, it is characterized in that: comprise carrier (1), the outside of carrier (1) is coated with the luminescent layer (2) of being made by the photo-induced energy storage luminescent powder.
2. underwater light-emitting Masterbatch according to claim 1, it is characterized in that: the thickness of described luminescent layer (2) is the 0.6-1.2 millimeter.
3. underwater light-emitting Masterbatch according to claim 1 and 2 is characterized in that: being shaped as of described underwater light-emitting Masterbatch is circular, cylindrical, in the rectangle any one.
4. the preparation technology of a underwater light-emitting Masterbatch is characterized in that: may further comprise the steps:
1) modulation
Photo-induced energy storage luminescent powder and water are (5-7) in mass ratio: (3-5) mix;
2) mix
The mixture of step 1) gained and carrier dropped in the high speed amalgamator carry out combination treatment;
3) extruding pelletization
With step 2) mixture of gained is delivered in the screw extrusion press, and the temperature in the screw extrusion press is controlled at 200-300 ℃, and rotating speed is the 250-350r/min extruding pelletization;
4) drying
The Masterbatch that step 3) is obtained carries out drying treatment in drying machine, dried Masterbatch water content is controlled at 5%-7%.
5. the preparation technology of underwater light-emitting Masterbatch according to claim 4 is characterized in that: described step 1) and step 2) between also have heating steps, be specially:
The mass transport of step 1) gained is heated to cooking-vessel, and heating and temperature control heated 20-30 minute at 50-70 ℃.
6. the preparation technology of underwater light-emitting Masterbatch according to claim 4 is characterized in that: step 2) described in time of combination treatment be 40-50 minute.
7. the preparation technology of underwater light-emitting Masterbatch according to claim 4, it is characterized in that: screw extrusion press described in the step 3) is any one in twin screw extruder or the single screw extrusion machine.
8. the preparation technology of underwater light-emitting Masterbatch according to claim 4 is characterized in that: the drying temperature in the drying machine described in the step 4) is controlled at 30-40 ℃.
Priority Applications (1)
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CN2012103204463A CN102863811A (en) | 2012-08-31 | 2012-08-31 | Underwater luminous master batch and preparation process thereof |
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CN2012103204463A CN102863811A (en) | 2012-08-31 | 2012-08-31 | Underwater luminous master batch and preparation process thereof |
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CN102863811A true CN102863811A (en) | 2013-01-09 |
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CN2012103204463A Pending CN102863811A (en) | 2012-08-31 | 2012-08-31 | Underwater luminous master batch and preparation process thereof |
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1224735A (en) * | 1998-12-09 | 1999-08-04 | 吴国祥 | Night luminous plastic material |
CN101070392A (en) * | 2007-06-18 | 2007-11-14 | 济南朗星科技有限公司 | Method for preparing luminous thermoplastic plastic parent particles |
-
2012
- 2012-08-31 CN CN2012103204463A patent/CN102863811A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1224735A (en) * | 1998-12-09 | 1999-08-04 | 吴国祥 | Night luminous plastic material |
CN101070392A (en) * | 2007-06-18 | 2007-11-14 | 济南朗星科技有限公司 | Method for preparing luminous thermoplastic plastic parent particles |
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Application publication date: 20130109 |