CN102861547B - Reaction kettle - Google Patents

Reaction kettle Download PDF

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Publication number
CN102861547B
CN102861547B CN201210363496.XA CN201210363496A CN102861547B CN 102861547 B CN102861547 B CN 102861547B CN 201210363496 A CN201210363496 A CN 201210363496A CN 102861547 B CN102861547 B CN 102861547B
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China
Prior art keywords
storage tank
temporary storage
kettle
control system
feed pipe
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Expired - Fee Related
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CN201210363496.XA
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Chinese (zh)
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CN102861547A (en
Inventor
胡晓东
朱兰兰
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Codexis Inc
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SUZHOU ENZYMEWORKS Inc
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Priority to CN201210363496.XA priority Critical patent/CN102861547B/en
Publication of CN102861547A publication Critical patent/CN102861547A/en
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Publication of CN102861547B publication Critical patent/CN102861547B/en
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Abstract

The invention relates to a reaction kettle. The reaction kettle comprises a kettle body, a stirring device and an automatic feeding system, wherein the kettle body comprises a kettle and a kettle cover in sealing connection with the kettle; the automatic feeding system comprises a temporary storage tank with a metering device, an inlet pipe, a feed pipe, a first control valve and a second control valve; one end of the inlet pipe and one end of the feed pipe are respectively communicated with the temporary storage tank; the first control valve and the second control valve are respectively arranged on the inlet pipe and the feed pipe; the other end of the inlet pipe is communicated with the kettle; and the metering device comprises a metering scale arranged on the temporary storage tank, an inductor which is used for inducing materials inside the temporary storage tank, and a control system capable of receiving information of the inductor. According to the reaction kettle, materials can be automatically added into the reaction kettle discontinuously, the whole material adding process is performed in a closed state to prevent harmful bacteria from entering the reaction kettle, and the quality and efficiency of the product after reaction can be improved.

Description

A kind of reactor
Technical field
The present invention relates to a kind of reactor, it is particularly related to a kind of reactor of auto feed.
Background technology
At present, in chemicals experiment or synthetic preparation process, the use of reactor is very common, the fermenting and producing dehalogenase of for example microorganism, during the fermentation, need interval to increase microorganism raw material to sending out in reactor, but, in interpolation microorganism raw material process, great majority are all to adopt manually to add, charging aperture on autoreaction still kettle cover, in kettle, add microorganism raw material, in whole process, not only labour intensity is larger, and dehalogenase in fermentation is contacted with air, a large amount of harmful bacterias enters in kettle, activity and the quality of dehalogenase have directly been affected, the efficiency of simultaneously producing dehalogenase is low.
Summary of the invention
Technical problem to be solved by this invention is to overcome the deficiencies in the prior art, and a kind of reactor of improved auto feed is provided.
For solving above technical problem, the present invention takes following technical scheme:
A kind of reactor, it comprises kettle and agitating device, the kettle cover that this kettle comprises still body and is tightly connected with still body, particularly, reactor also comprises automatic feeding system, described automatic feeding system comprise with the temporary storage tank of metering device, have respectively an end with feed pipe and charge pipe that temporarily storage tank is communicated with, be separately positioned on the first control valve and the second control valve on feed pipe and charge pipe, and be arranged on visor hand hole on kettle cover and stretch into the lamp of looking in kettle, feed pipe and charge pipe are arranged side by side is arranged on temporary storage tank lower end; The other end of charge pipe is communicated with still body; Metering device comprises the metering ruler that arranges on temporary storage tank, for responding to the inductor of temporary tank inside material and can receiving the control system of inductor information, the first control valve comprises the first application valve body and for controlling the first application valve body, opens or closes the first control system of state, and control system is connected with the first control system; The second control valve comprises the second application valve body and for controlling the second application valve body, opens or closes the second control system of state, and control system is connected with the second control system.
According to concrete an enforcement of the present invention, depending on lamp and visor hand hole relative being arranged on described kettle cover respectively, can maximizedly watch like this extent of reaction of the interior material of kettle, depending on lamp, be the anti-riot lamp of looking of corrosion resistant simultaneously, long service life, cost-saving.
Further, automatic feeding system also comprise the feed pipe being communicated with the other end of temporary storage tank and be arranged on feed pipe and kettle cover between the 3rd control valve, described the 3rd control valve comprises the 3rd application valve body and for controlling the 3rd valve body processed, opens or closes the 3rd control system of state, and control system is connected with the second control system.
Further, feed pipe is arranged on temporary storage tank upper end and is communicated with temporary storage tank.
Due to the enforcement of above technical scheme, the present invention compared with prior art tool has the following advantages:
The present invention can realize discontinuously and automatically adding materials in reactor, and whole filling process is all to carry out under air-tight state simultaneously, prevents that harmful bacteria from entering in reactor, improves quality and the efficiency of reaction afterproduct.
Accompanying drawing explanation
Below in conjunction with accompanying drawing and concrete embodiment, the present invention will be further described in detail.
Fig. 1 is the structural representation of the reactor according to the present invention;
Wherein: 1, kettle; 10, still body; 11, kettle cover; 100, discharging opening; 110, charging aperture; 2, agitating device; 3, temporary storage tank; 4, feed pipe; 5, charge pipe; 6, the first control valve; 60, the first application valve body; 7, the second control valve; 70, the second application valve body; 8, metering ruler; 9, visor hand hole; 12, look lamp; 13, feed pipe; 14, the 3rd control valve; 140, the 3rd control valve.
The specific embodiment
As shown in Figure 1, the reactor of the present embodiment, it comprises kettle 1, agitating device 2, visor hand hole 9, depending on lamp 10 and automatic feeding system, the kettle cover 11 that wherein kettle 1 comprises still body 10 and is tightly connected with still body 10, the bottom of still body 10 is provided with discharging opening 100, kettle cover 11 is provided with charging aperture 110, agitating device 2 also adopts those known forms, in this example, do not describing in detail, wherein depending on lamp 12 and visor hand hole 9 relative being arranged on kettle cover 11 respectively, depending on lamp 12, it is the conventional anti-riot lamp of looking of corrosion resistant in this area, improve the service life of looking lamp 12, more convenient observation is in the interior material reaction progress of kettle 1.Automatic feeding system comprises temporary storage tank 3, feed pipe 4, charge pipe 5, the first control valve 6 and the second control valve 7, and concrete structural relation is as follows.
Feed pipe 4 is set up in parallel the bottom at temporary storage tank 3 together with charge pipe 5, and be communicated with temporary storage tank 3, wherein temporarily storage tank 3 is provided with meter scale 8 and for responding to the inductor (not shown) of temporary storage tank 3 materials inside and can receiving the control system of inductor information, as long as when the material in temporary storage tank 3 is encountered inductor, this inductor just sends information, by control system, received, inductor and control system are all those forms that those skilled in the art commonly use, and at this, do not describe in detail.In addition, wherein the first control valve 6 comprises the first application valve body 60 and for controlling the first application valve body 60, opens or closes the first control system of state, and control system is connected with the first control system; The second control valve 7 comprises the second application valve body 70 and for controlling the second application valve body 70, opens or closes the second control system of state, and control system is connected with the second control system;
Automatic feeding system in this example also comprises the feed pipe 13 and the 3rd control valve 14 that are arranged on temporary storage tank 3 upper ends, wherein the two ends of feed pipe 13 are communicated with kettle cover 11 and temporary storage tank 3 respectively, the 3rd control valve 14 comprises the 3rd application valve body 140 being arranged on feed pipe 13 and the 3rd application valve body 140 is opened or the 3rd control system of closure state for controlling, and the 3rd control system is also communicated with the second control system.When the 3rd application valve body is opened, by the gas in kettle 1, will be pressed in kettle 1 in temporary storage tank 3 and the interior material of charge pipe 5, prevent residual in temporarily storage tank 3 and charge pipe 5 of material, improve material and flow into the speed in kettle 1, raise the efficiency.
The specific works process of the present embodiment is as follows:
According to the progress of material in reactor reaction, the temporary storage tank of corresponding large low capacity is set, and on storage tank, be provided with metering ruler and inductor temporarily, now the second application valve body on charge pipe and on feed pipe the 3rd application valve body all in closed condition, and the first application valve body on feed pipe is in open mode, material is in feed pipe flow into temporary storage tank, when the material in temporary storage tank is encountered the inductor in temporary storage tank, by control system, received after the information of inductor, the first application valve body is closed, and open the second application valve body, material flows in reactor from temporary storage tank, can open the 3rd application valve body simultaneously, by the gas in kettle, will in temporary storage tank and charge pipe, be expressed in kettle by material, improve the speed that material enters kettle, prevent residual in temporarily storage tank and charge pipe of material.After the material in temporary storage tank all adds in reactor, again close second and the 3rd application valve body, open the first application valve body, material flows in temporary storage tank from feed pipe again, and by concrete extent of reaction, determine the flow velocity of material, when in temporary storage tank, material contacts with inductor, in reaction kettle body, material reaction completes, then close the first application valve body, open the second application valve body, material flows in reactor from temporary storage tank, can open the 3rd application valve body simultaneously, by the gas in kettle, will in temporary storage tank and charge pipe, be expressed in kettle by material, improve the speed that material enters kettle, prevent residual in temporarily storage tank and charge pipe of material.So, repeatedly carry out this operating process, realize discontinuously and automatically adding materials in phase reaction kettle.
In sum, the present invention can realize discontinuously and automatically adding materials in reactor, and whole filling process is all to carry out under air-tight state simultaneously, prevents that harmful bacteria from entering in reactor, improves quality and the efficiency of reaction afterproduct.
Above the present invention is described in detail, but the invention is not restricted to the embodiments described.The equivalence that all Spirit Essences according to the present invention are done changes or modifies, and all should be encompassed in protection scope of the present invention.

Claims (5)

1. a reactor, it comprises kettle (1) and agitating device (2), the kettle cover (11) that this kettle (1) comprises still body (10) and is tightly connected with described still body (10), it is characterized in that: described reactor also comprises automatic feeding system, described automatic feeding system comprises the temporary storage tank (3) with metering device, the feed pipe (4) and the charge pipe (5) that have respectively an end to be communicated with described temporary storage tank (3), be separately positioned on the first control valve (6) and the second control valve (7) on described feed pipe (4) and described charge pipe (5), and be arranged on the visor hand hole (9) on described kettle cover (11) and stretch into and look lamp (12) in described kettle (1), what described feed pipe (4) and charge pipe (5) were arranged side by side is arranged on described temporary storage tank (3) lower end and is communicated with described temporary storage tank (3), the other end of described charge pipe (5) is communicated with described still body (10), described metering device comprises the metering ruler (8) arranging on described temporary storage tank (3), the control system that is used for responding to the inductor of described temporary storage tank (3) materials inside and can receives described inductor information, described the first control valve (6) comprises the first application valve body (60) and for controlling described the first application valve body (60), opens or closes the first control system of state, described control system is connected with the first described control system, described the second control valve (7) comprises the second application valve body (70) and for controlling described the second application valve body (70), opens or closes the second control system of state, described control system is connected with the second described control system.
2. reactor according to claim 1, is characterized in that: described in depending on lamp (12) and described visor hand hole (9) relative being arranged on described kettle cover (11) respectively.
3. reactor according to claim 1 and 2, is characterized in that: described in depending on lamp (12), be the anti-riot lamp of looking of corrosion resistant.
4. reactor according to claim 1, it is characterized in that: described automatic feeding system also comprise the feed pipe (13) being communicated with the other end of described temporary storage tank (3) and be arranged on described feed pipe (13) and described kettle cover (11) between the 3rd control valve (14), the 3rd described control valve (14) comprises the 3rd application valve body (140) and for controlling described the 3rd valve body processed (140), opens or closes the 3rd control system of state, and described control system is connected with the second described control system.
5. reactor according to claim 4, is characterized in that: described feed pipe (13) is arranged on described temporary storage tank (3) upper end and is communicated with described temporary storage tank (3).
CN201210363496.XA 2012-09-26 2012-09-26 Reaction kettle Expired - Fee Related CN102861547B (en)

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Application Number Priority Date Filing Date Title
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CN102861547B true CN102861547B (en) 2014-04-23

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Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103055790A (en) * 2013-01-18 2013-04-24 金伟光 Equipment of preparing anthraquinone by one-kettle method and method of preparing anthraquinone using same
CN106824004A (en) * 2017-01-24 2017-06-13 安徽华晟涂料有限公司 A kind of water paint produces additive feeding system
CN111545131B (en) * 2020-04-29 2021-10-08 北京航空航天大学 Control method of waste heat recovery type sealed hydrothermal reaction kettle
CN114632490A (en) * 2022-02-28 2022-06-17 昆山市冠宝化学有限公司 Polyurethane adhesive preparation device and preparation method thereof
CN114931914A (en) * 2022-06-02 2022-08-23 安徽省谱诺药化设备有限公司 Sealed feeding and discharging type stainless steel reaction kettle and feeding and discharging method thereof

Citations (3)

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Publication number Priority date Publication date Assignee Title
US20030170156A1 (en) * 2002-03-07 2003-09-11 Mionix Corp. Apparatus for mixing acid and base
CN1559660A (en) * 2004-03-02 2005-01-05 浙江大学 Automatic control extreme environment analogue flow reaction experimental device
CN102631878A (en) * 2012-05-02 2012-08-15 浙江华亿工程设计有限公司 Intelligent reaction kettle

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20030170156A1 (en) * 2002-03-07 2003-09-11 Mionix Corp. Apparatus for mixing acid and base
CN1559660A (en) * 2004-03-02 2005-01-05 浙江大学 Automatic control extreme environment analogue flow reaction experimental device
CN102631878A (en) * 2012-05-02 2012-08-15 浙江华亿工程设计有限公司 Intelligent reaction kettle

Non-Patent Citations (2)

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Title
智能控制方法在反应釜温度控制中的运用;谢森林等;《自动化仪表》;20080831;第29卷(第8期);15-18 *
谢森林等.智能控制方法在反应釜温度控制中的运用.《自动化仪表》.2008,第29卷(第8期),15-18.

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Effective date of registration: 20180524

Address after: American California

Patentee after: Codexis, Inc.

Address before: 215600 E-108, pioneer service center, 1 Guotai North Road, Yang Shi Town, Zhangjiagang, Suzhou, Jiangsu

Patentee before: Suzhou EnzymeWorks, Inc.

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140423

Termination date: 20180926